TR201905939T4 - Gelişmiş enerji tasarruflu sülfürik asit üretimine yönelik proses ve tesis. - Google Patents

Gelişmiş enerji tasarruflu sülfürik asit üretimine yönelik proses ve tesis. Download PDF

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Publication number
TR201905939T4
TR201905939T4 TR2019/05939T TR201905939T TR201905939T4 TR 201905939 T4 TR201905939 T4 TR 201905939T4 TR 2019/05939 T TR2019/05939 T TR 2019/05939T TR 201905939 T TR201905939 T TR 201905939T TR 201905939 T4 TR201905939 T4 TR 201905939T4
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TR
Turkey
Prior art keywords
sulfuric acid
absorber
chamber
plant
acid production
Prior art date
Application number
TR2019/05939T
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English (en)
Inventor
Daum Karl-Heinz
Ernst Peter
Storch Hannes
Schalk Wolfram
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Outotec Finland Oy
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Publication date
Application filed by Outotec Finland Oy filed Critical Outotec Finland Oy
Publication of TR201905939T4 publication Critical patent/TR201905939T4/tr

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C01B17/765—Multi-stage SO3-conversion
    • C01B17/7655—Multi-stage SO3-conversion with intermediate absorption
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C01B17/80—Apparatus
    • C01B17/806—Absorbers; Heat exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1406—Multiple stage absorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1456—Removing acid components
    • B01D53/1481—Removing sulfur dioxide or sulfur trioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1493—Selection of liquid materials for use as absorbents
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C01B17/775—Liquid phase contacting processes or wet catalysis processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/10—Inorganic absorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2258/00—Sources of waste gases
    • B01D2258/02—Other waste gases
    • B01D2258/025—Other waste gases from metallurgy plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/48—Sulfur compounds
    • B01D53/50—Sulfur oxides
    • B01D53/507—Sulfur oxides by treating the gases with other liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Treating Waste Gases (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Gas Separation By Absorption (AREA)

Abstract

SO2 ila SO3?ün katalitik oksidasyonu ve sonrasında sülfürik asitte SO3 soğurumu ile sülfürik asit üretimine yönelik tesis olup, gazlı SO3 ve konsantre sülfürik asidin, sülfürik asitteki SO3'ü soğurması için eklendiği bir birincil soğurucuya (42) sahiptir, birincil soğurucuda (42) soğrulmayan SO3, yani bir ikincil soğurucu (41), sülfürik asitte daha fazla soğurum için tedarik edilmektedir, ve sülfürik asidin, iki soğurucunun (41, 42) bir haznesinden (62, 63) birincil soğurucunun (42) başlığına devridaim ettirilmesine yönelik en bir devridaim kanalına (10, 9, 3) sahiptir. Birinin, kazan besleme suyu/buharı (43) ile soğutma için tasarlandığı ve diğerinin, soğutma suyu (44) ile soğutma için tasarlandığı en az bir devridaim kanalında (10, 9, 3) paralel olarak ve birincil soğurucu (42) haznesini (62), ikincil soğurucu (41) haznesine (63) bağlayan bir bağlantı (61) veya birincil soğurucunun (42) ve ikincil soğurucunun (41) bir ortak haznesi (62) ve/veya bir ortak pompa tankı (46) vasıtasıyla bağlanan en az iki ısı değiştirici (43, 44) ile karakterize edilmektedir.
TR2019/05939T 2014-12-19 2015-12-15 Gelişmiş enerji tasarruflu sülfürik asit üretimine yönelik proses ve tesis. TR201905939T4 (tr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102014119216 2014-12-19

Publications (1)

Publication Number Publication Date
TR201905939T4 true TR201905939T4 (tr) 2019-05-21

Family

ID=55066577

Family Applications (1)

Application Number Title Priority Date Filing Date
TR2019/05939T TR201905939T4 (tr) 2014-12-19 2015-12-15 Gelişmiş enerji tasarruflu sülfürik asit üretimine yönelik proses ve tesis.

Country Status (12)

Country Link
US (1) US10150671B2 (tr)
EP (1) EP3233723B1 (tr)
CN (1) CN107108210B (tr)
CA (1) CA2968771C (tr)
CL (1) CL2017001412A1 (tr)
DE (1) DE202015106813U1 (tr)
ES (1) ES2722750T3 (tr)
JO (1) JO3678B1 (tr)
MA (1) MA40600B1 (tr)
SA (1) SA517381761B1 (tr)
TR (1) TR201905939T4 (tr)
WO (1) WO2016096867A1 (tr)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR112015022004B8 (pt) * 2013-03-15 2022-07-12 Mecs Inc Processos para remoção de gás contaminante da fonte de gás e recuperação do referido gás e para a remoção de dióxido de enxofre de fonte de gás contendo dióxido de enxofre e recuperação do dióxido de enxofre
CN107108210B (zh) * 2014-12-19 2019-07-16 奥图泰(芬兰)公司 用于改进的能量有效生产硫酸的方法和设备
BR102016003690B1 (pt) 2016-02-22 2022-08-30 Nc Engenharia, Industria E Comercio Ltda Método e equipamento para resfriar ácido sulfúrico
CN106268179B (zh) * 2016-08-25 2018-09-07 长沙有色冶金设计研究院有限公司 一种综合回收硫酸净化废酸的节能工艺及系统
CN109867267B (zh) * 2019-04-25 2022-01-28 吉林隆源骐化工有限责任公司 一种接触法硫酸生产装置中的转化升温系统
CN111185079B (zh) * 2019-12-04 2022-02-08 大连百傲化学股份有限公司 一种焚烧烟气中酸性气体的资源化处理方法
EP4077212B1 (en) 2019-12-19 2024-02-07 Metso Metals Oy A venturi absorber tube for absorbing sulfur trioxide in sulfuric acid
EP4168358B1 (en) * 2020-06-18 2024-07-31 Metso Metals Oy Process and plant for the production of sulfuric acid
CN113460973A (zh) * 2021-06-30 2021-10-01 内蒙古金陶股份有限公司 一种利用硫精矿制备硫酸的方法
CN113521966A (zh) * 2021-07-26 2021-10-22 浙江大学 基于传质-反应调控的分区多级循环co2捕集浓缩方法
WO2024079378A1 (en) * 2022-10-11 2024-04-18 Metso Outotec Finland Oy Process and plant for a permanent storage of phosphogypsum
CN119575904A (zh) * 2024-11-28 2025-03-07 广东中南钢铁股份有限公司 一种湿法硫酸工艺的故障判断及处理方法、装置及电子设备

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH57886A (de) 1911-09-22 1913-02-01 Siemens Ag Hilfseinrichtung zum Schutz gegen unbeabsichtigtes Ansprechen elektrischer Sicherungsapparate
CH198647A (de) 1935-11-30 1938-07-15 Paul Leistritz Knetmaschine.
CH498647A (de) 1968-02-03 1970-11-15 Metallgesellschaft Ag Vorrichtung zur Behandlung gasförmiger Medien
CH547231A (de) 1970-10-15 1974-03-29 Metallgesellschaft Ag Zwischenabsorber fuer die absorption von so3 und verfahren zum betreiben des zwischenabsorbers.
US4996038A (en) 1983-07-05 1991-02-26 Monsanto Company Heat recovery from concentrated sulfuric acid
US5118490A (en) * 1989-06-21 1992-06-02 Monsanto Company Absorption of wet conversion gas
DE102004012293B4 (de) * 2004-03-12 2016-09-08 Outotec Oyj Verfahren und Anlage zur Herstellung von Schwefelsäure
DE102005008109A1 (de) * 2005-02-21 2006-08-24 Outokumpu Technology Oy Verfahren und Anlage zur Herstellung von Schwefelsäure
MX2010005600A (es) * 2007-11-23 2010-09-07 Outotec Oyj Proceso y planta para producir acido sulfurico.
JO3617B1 (ar) * 2010-01-20 2020-08-27 Mecs Inc استرجاع الطاقة في تصنيع حمض السلفريك
DE102010006541B4 (de) 2010-02-01 2016-03-17 Outotec Oyj Verfahren und Anlage zum Abkühlen von Säure
CN107108210B (zh) * 2014-12-19 2019-07-16 奥图泰(芬兰)公司 用于改进的能量有效生产硫酸的方法和设备

Also Published As

Publication number Publication date
ES2722750T3 (es) 2019-08-16
CA2968771A1 (en) 2016-06-23
CA2968771C (en) 2020-05-05
MA40600B1 (fr) 2018-11-30
JO3678B1 (ar) 2020-08-27
EP3233723A1 (en) 2017-10-25
SA517381761B1 (ar) 2021-03-07
CN107108210B (zh) 2019-07-16
MA40600A1 (fr) 2018-05-31
DE202015106813U1 (de) 2016-01-20
US20170349437A1 (en) 2017-12-07
EP3233723B1 (en) 2019-02-06
WO2016096867A1 (en) 2016-06-23
US10150671B2 (en) 2018-12-11
CL2017001412A1 (es) 2018-02-16
CN107108210A (zh) 2017-08-29

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