JO3678B1 - عملية ووحدة صناعية لإنتاج حمض الكبريتيك بشكل محسَّن وفعَّال من حيث الطاقة - Google Patents

عملية ووحدة صناعية لإنتاج حمض الكبريتيك بشكل محسَّن وفعَّال من حيث الطاقة

Info

Publication number
JO3678B1
JO3678B1 JOP/2015/0323A JOP20150323A JO3678B1 JO 3678 B1 JO3678 B1 JO 3678B1 JO P20150323 A JOP20150323 A JO P20150323A JO 3678 B1 JO3678 B1 JO 3678B1
Authority
JO
Jordan
Prior art keywords
sulfuric acid
absorption
cooled
plant
efficient production
Prior art date
Application number
JOP/2015/0323A
Other languages
English (en)
Inventor
-Ing Peter Ernst Dipl
-Ing Hannes Storch Dr
-Ing Wolfram Schalk Dipl
-Ing Karl-Heinz Daum Dipl
Original Assignee
Outotec Finland Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outotec Finland Oy filed Critical Outotec Finland Oy
Application granted granted Critical
Publication of JO3678B1 publication Critical patent/JO3678B1/ar

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C01B17/765—Multi-stage SO3-conversion
    • C01B17/7655—Multi-stage SO3-conversion with intermediate absorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1406—Multiple stage absorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1456—Removing acid components
    • B01D53/1481—Removing sulfur dioxide or sulfur trioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1493—Selection of liquid materials for use as absorbents
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C01B17/775—Liquid phase contacting processes or wet catalysis processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/74—Preparation
    • C01B17/76—Preparation by contact processes
    • C01B17/80—Apparatus
    • C01B17/806—Absorbers; Heat exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/10—Inorganic absorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2258/00—Sources of waste gases
    • B01D2258/02—Other waste gases
    • B01D2258/025—Other waste gases from metallurgy plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/48—Sulfur compounds
    • B01D53/50—Sulfur oxides
    • B01D53/507—Sulfur oxides by treating the gases with other liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Treating Waste Gases (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Gas Separation By Absorption (AREA)

Abstract

يصف الاختراع الحالي عملية لإنتاج حمض كبريتيك بواسطة أكسدة حفزية لـ SO2 إلى SO3 وامتصاص لاحق للـ SO3 في حمض الكبريتيك, حيث يدخل الـ SO3 في مرحلة امتصاص أولى (جهاز امتصاص أولي) ويتم امتصاصه جزئياً على الأقل في حمض الكبريتيك المركز, حيث يتم تزويد الـ SO3 غير الممتص في مرحلة الامتصاص الاولى إلى مرحلة الامتصاص الثانية (جهاز الامتصاص الثاني) لامتصاص المزيد في حمض الكبريتيك المركز, و حيث يتم تبريد حمض الكبريتيك بعد مروره خلال مرحلتي الامتصاص. ويتم إجراء التبريد لحمض الكبريتيك في على الأقل المبادلين الحراريين الموصولين على التوازي, حيث يتم تشغيل واحد على الأقل من المبادلين الحراريين كمبخر جزئي ويتم تبريده بواسطة ماء/بخار تغذية المرجل ويتم تبريد الآخر بماء التبريد وتشغيله كمبرِّد للحمض النقي.
JOP/2015/0323A 2014-12-19 2015-12-16 عملية ووحدة صناعية لإنتاج حمض الكبريتيك بشكل محسَّن وفعَّال من حيث الطاقة JO3678B1 (ar)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102014119216 2014-12-19

Publications (1)

Publication Number Publication Date
JO3678B1 true JO3678B1 (ar) 2020-08-27

Family

ID=55066577

Family Applications (1)

Application Number Title Priority Date Filing Date
JOP/2015/0323A JO3678B1 (ar) 2014-12-19 2015-12-16 عملية ووحدة صناعية لإنتاج حمض الكبريتيك بشكل محسَّن وفعَّال من حيث الطاقة

Country Status (12)

Country Link
US (1) US10150671B2 (ar)
EP (1) EP3233723B1 (ar)
CN (1) CN107108210B (ar)
CA (1) CA2968771C (ar)
CL (1) CL2017001412A1 (ar)
DE (1) DE202015106813U1 (ar)
ES (1) ES2722750T3 (ar)
JO (1) JO3678B1 (ar)
MA (1) MA40600B1 (ar)
SA (1) SA517381761B1 (ar)
TR (1) TR201905939T4 (ar)
WO (1) WO2016096867A1 (ar)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2902732C (en) * 2013-03-15 2021-10-26 Ernesto Vera-Castaneda Regenerative recovery of contaminants from effluent gases
DE202015106813U1 (de) * 2014-12-19 2016-01-20 Outotec (Finland) Oy Anlage zur energieeffizienteren Herstellung von Schwefelsäure
BR102016003690B1 (pt) 2016-02-22 2022-08-30 Nc Engenharia, Industria E Comercio Ltda Método e equipamento para resfriar ácido sulfúrico
CN106268179B (zh) * 2016-08-25 2018-09-07 长沙有色冶金设计研究院有限公司 一种综合回收硫酸净化废酸的节能工艺及系统
CN109867267B (zh) * 2019-04-25 2022-01-28 吉林隆源骐化工有限责任公司 一种接触法硫酸生产装置中的转化升温系统
CN111185079B (zh) * 2019-12-04 2022-02-08 大连百傲化学股份有限公司 一种焚烧烟气中酸性气体的资源化处理方法
EP4077212B1 (en) 2019-12-19 2024-02-07 Metso Metals Oy A venturi absorber tube for absorbing sulfur trioxide in sulfuric acid
WO2021254627A1 (en) * 2020-06-18 2021-12-23 Outotec (Finland) Oy Process and plant for the production of sulfuric acid
FR3112536B1 (fr) 2020-07-16 2022-11-25 Ocp Sa Procédé et installation de fabrication d’acide sulfurique
CN113460973A (zh) * 2021-06-30 2021-10-01 内蒙古金陶股份有限公司 一种利用硫精矿制备硫酸的方法
CN113521966A (zh) * 2021-07-26 2021-10-22 浙江大学 基于传质-反应调控的分区多级循环co2捕集浓缩方法
EP4601996A4 (en) * 2022-10-11 2026-08-12 Metso Metals Oy METHOD AND INSTALLATION FOR THE PERMANENT STORAGE OF PHOSPHOGYPSE
CN119575904A (zh) * 2024-11-28 2025-03-07 广东中南钢铁股份有限公司 一种湿法硫酸工艺的故障判断及处理方法、装置及电子设备

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH57886A (de) 1911-09-22 1913-02-01 Siemens Ag Hilfseinrichtung zum Schutz gegen unbeabsichtigtes Ansprechen elektrischer Sicherungsapparate
CH198647A (de) 1935-11-30 1938-07-15 Paul Leistritz Knetmaschine.
CH498647A (de) 1968-02-03 1970-11-15 Metallgesellschaft Ag Vorrichtung zur Behandlung gasförmiger Medien
CH547231A (de) 1970-10-15 1974-03-29 Metallgesellschaft Ag Zwischenabsorber fuer die absorption von so3 und verfahren zum betreiben des zwischenabsorbers.
US4996038A (en) 1983-07-05 1991-02-26 Monsanto Company Heat recovery from concentrated sulfuric acid
US5118490A (en) * 1989-06-21 1992-06-02 Monsanto Company Absorption of wet conversion gas
DE102004012293B4 (de) * 2004-03-12 2016-09-08 Outotec Oyj Verfahren und Anlage zur Herstellung von Schwefelsäure
DE102005008109A1 (de) * 2005-02-21 2006-08-24 Outokumpu Technology Oy Verfahren und Anlage zur Herstellung von Schwefelsäure
MX2010005600A (es) * 2007-11-23 2010-09-07 Outotec Oyj Proceso y planta para producir acido sulfurico.
JO3617B1 (ar) * 2010-01-20 2020-08-27 Mecs Inc استرجاع الطاقة في تصنيع حمض السلفريك
DE102010006541B4 (de) 2010-02-01 2016-03-17 Outotec Oyj Verfahren und Anlage zum Abkühlen von Säure
DE202015106813U1 (de) * 2014-12-19 2016-01-20 Outotec (Finland) Oy Anlage zur energieeffizienteren Herstellung von Schwefelsäure

Also Published As

Publication number Publication date
CA2968771C (en) 2020-05-05
EP3233723A1 (en) 2017-10-25
US20170349437A1 (en) 2017-12-07
SA517381761B1 (ar) 2021-03-07
ES2722750T3 (es) 2019-08-16
MA40600B1 (fr) 2018-11-30
CA2968771A1 (en) 2016-06-23
US10150671B2 (en) 2018-12-11
CN107108210A (zh) 2017-08-29
EP3233723B1 (en) 2019-02-06
MA40600A1 (fr) 2018-05-31
CL2017001412A1 (es) 2018-02-16
WO2016096867A1 (en) 2016-06-23
CN107108210B (zh) 2019-07-16
DE202015106813U1 (de) 2016-01-20
TR201905939T4 (tr) 2019-05-21

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