TW200538459A - Purification of n-(phosphonomethyl)glycine - Google Patents

Purification of n-(phosphonomethyl)glycine Download PDF

Info

Publication number: TW200538459A
Authority: TW; Taiwan
Prior art keywords: ala; leu; gly; val; arg
Prior art date: 2004-05-21

Application number

TW094113644A

Other languages

English (en)

Chinese (zh)

Inventor

Jimmy Jui Tai

Herbert Nathan Praay

James William Ringer

Mark Victor Michael Emonds

Original Assignee

Dow Agrosciences Llc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2004-05-21

Filing date

2005-04-28

Publication date

2005-12-01

2005-04-28 Application filed by Dow Agrosciences Llc filed Critical Dow Agrosciences Llc

2005-12-01 Publication of TW200538459A publication Critical patent/TW200538459A/zh

Links

XDDAORKBJWWYJS-UHFFFAOYSA-N glyphosate Chemical compound OC(=O)CNCP(O)(O)=O XDDAORKBJWWYJS-UHFFFAOYSA-N 0.000 title claims abstract description 50
238000000746 purification Methods 0.000 title abstract description 8
239000005562 Glyphosate Substances 0.000 claims abstract description 46
229940097068 glyphosate Drugs 0.000 claims abstract description 46
238000000034 method Methods 0.000 claims abstract description 27
239000000203 mixture Substances 0.000 claims abstract description 26
239000002253 acid Substances 0.000 claims abstract description 22
239000000463 material Substances 0.000 claims abstract description 21
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239000002244 precipitate Substances 0.000 claims abstract description 6
239000012528 membrane Substances 0.000 claims abstract description 5
238000001728 nano-filtration Methods 0.000 claims abstract description 5
DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims description 52
239000000047 product Substances 0.000 claims description 21
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 17
239000002585 base Substances 0.000 claims description 17
239000004471 Glycine Substances 0.000 claims description 15
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
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238000006386 neutralization reaction Methods 0.000 claims description 5
239000000126 substance Substances 0.000 claims description 4
150000001413 amino acids Chemical class 0.000 claims description 2
150000003839 salts Chemical class 0.000 abstract description 21
VPZXBVLAVMBEQI-UHFFFAOYSA-N glycyl-DL-alpha-alanine Natural products OC(=O)C(C)NC(=O)CN VPZXBVLAVMBEQI-UHFFFAOYSA-N 0.000 description 91
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XKUKSGPZAADMRA-UHFFFAOYSA-N glycyl-glycyl-glycine Chemical compound NCC(=O)NCC(=O)NCC(O)=O XKUKSGPZAADMRA-UHFFFAOYSA-N 0.000 description 17
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Classifications

- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/025—Purification; Separation; Stabilisation; Desodorisation of organo-phosphorus compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
- C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y5/00—Nanobiotechnology or nanomedicine, e.g. protein engineering or drug delivery

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General Health & Medical Sciences (AREA)
Biochemistry (AREA)
Molecular Biology (AREA)
Pharmacology & Pharmacy (AREA)
Medicinal Chemistry (AREA)
Epidemiology (AREA)
Animal Behavior & Ethology (AREA)
Public Health (AREA)
Veterinary Medicine (AREA)
Separation Using Semi-Permeable Membranes (AREA)
Agricultural Chemicals And Associated Chemicals (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
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TW094113644A 2004-05-21 2005-04-28 Purification of n-(phosphonomethyl)glycine TW200538459A (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US57325504P	2004-05-21	2004-05-21

Publications (1)

Publication Number	Publication Date
TW200538459A true TW200538459A (en)	2005-12-01

Family

ID=35134799

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
TW094113644A TW200538459A (en)	2004-05-21	2005-04-28	Purification of n-(phosphonomethyl)glycine

Country Status (21)

Country	Link
US (1)	US7683207B2 (de)
EP (1)	EP1756127B1 (de)
JP (1)	JP4896881B2 (de)
KR (1)	KR20070012828A (de)
CN (1)	CN1953986B (de)
AT (1)	ATE417854T1 (de)
AU (1)	AU2005245973B2 (de)
BR (1)	BRPI0511434A (de)
CA (1)	CA2564397A1 (de)
DE (1)	DE602005011797D1 (de)
DK (1)	DK1756127T3 (de)
ES (1)	ES2317251T3 (de)
IL (1)	IL178994A (de)
MX (1)	MXPA06013372A (de)
NZ (1)	NZ550781A (de)
PL (1)	PL1756127T3 (de)
RU (1)	RU2369611C2 (de)
TW (1)	TW200538459A (de)
UA (1)	UA84345C2 (de)
WO (1)	WO2005113567A1 (de)
ZA (1)	ZA200609230B (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US8026389B2 (en) *	2006-12-15	2011-09-27	Ricardo Amaral Remer	Solid and water-soluble active ingredient and herbicide formulation, production process therefor, and process for controlling weeds
CN101434620B (zh) *	2008-12-18	2011-11-09	杭州天创净水设备有限公司	Ida法草甘膦母液取粉系统及取粉工艺
CN104151355A (zh) *	2014-08-06	2014-11-19	四川省乐山市福华通达农药科技有限公司	一种甘氨酸法制备草甘膦的脏粉处理工艺
CN105692960A (zh) *	2016-03-04	2016-06-22	安徽国星生物化学有限公司	一种草甘膦母液的处理方法
CN119660873B (zh) *	2024-12-24	2025-09-09	武汉理工大学	一种吸附分离草甘膦和增甘膦的方法

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* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3799758A (en)	1971-08-09	1974-03-26	Monsanto Co	N-phosphonomethyl-glycine phytotoxicant compositions
GB1436843A (en)	1972-07-21	1976-05-26	Ici Ltd	Preparation of n-phosphonomethyl-glycine
CH647528A5 (fr) *	1978-10-27	1985-01-31	Bcap Biolog Chem Act Pat	Procede pour la preparation de n-phosphonomethylglycine.
HU184601B (en) *	1979-07-09	1984-09-28	Alkaloida Vegyeszeti Gyar	Process for producing n-/phosphono-methyl/-glycine
DE3564115D1 (en) *	1984-06-04	1988-09-08	Stauffer Chemical Co	Method for preparation of n-phosphonomethylglycine
ES2022053T3 (es) *	1989-08-17	1995-04-16	Monsanto Co	Procedimiento de purificacion de n-fosfonometilglicina.
EP0806428B1 (de) *	1994-11-09	2003-01-29	Showa Denko Kabushiki Kaisha	Verfahren zur Abtrennung von N-Phosphonomethylglycin
JP3823330B2 (ja) *	1994-11-09	2006-09-20	昭和電工株式会社	Ｎ−ホスホノメチルグリシンの単離方法
AR027024A1 (es) *	1999-12-23	2003-03-12	Basf Ag	Procedimiento para la preparacion de n-fosfonometilglicina
DE10130136A1 (de)	2001-06-22	2003-01-02	Basf Ag	Verfahren zur Gewinnung von N-Phosphonomethylglycin
AR039201A1 (es) *	2003-03-28	2005-02-09	Atanor S A	Procedimiento para purificar soluciones de glifosato mediante nanofiltracion

2005
- 2005-04-28 TW TW094113644A patent/TW200538459A/zh unknown
- 2005-05-20 CN CN2005800151195A patent/CN1953986B/zh not_active Expired - Fee Related
- 2005-05-20 JP JP2007527533A patent/JP4896881B2/ja not_active Expired - Fee Related
- 2005-05-20 DK DK05753118T patent/DK1756127T3/da active
- 2005-05-20 AT AT05753118T patent/ATE417854T1/de active
- 2005-05-20 DE DE602005011797T patent/DE602005011797D1/de not_active Expired - Lifetime
- 2005-05-20 AU AU2005245973A patent/AU2005245973B2/en not_active Ceased
- 2005-05-20 WO PCT/US2005/017989 patent/WO2005113567A1/en not_active Ceased
- 2005-05-20 MX MXPA06013372A patent/MXPA06013372A/es active IP Right Grant
- 2005-05-20 RU RU2006145439/04A patent/RU2369611C2/ru not_active IP Right Cessation
- 2005-05-20 US US11/133,739 patent/US7683207B2/en not_active Expired - Fee Related
- 2005-05-20 PL PL05753118T patent/PL1756127T3/pl unknown
- 2005-05-20 NZ NZ550781A patent/NZ550781A/en not_active IP Right Cessation
- 2005-05-20 BR BRPI0511434-9A patent/BRPI0511434A/pt not_active IP Right Cessation
- 2005-05-20 EP EP05753118A patent/EP1756127B1/de not_active Expired - Lifetime
- 2005-05-20 UA UAA200613503A patent/UA84345C2/ru unknown
- 2005-05-20 CA CA002564397A patent/CA2564397A1/en not_active Abandoned
- 2005-05-20 ZA ZA200609230A patent/ZA200609230B/en unknown
- 2005-05-20 ES ES05753118T patent/ES2317251T3/es not_active Expired - Lifetime
- 2005-05-20 KR KR1020067024021A patent/KR20070012828A/ko not_active Withdrawn
2006
- 2006-11-01 IL IL178994A patent/IL178994A/en not_active IP Right Cessation

Also Published As

Publication number	Publication date
RU2006145439A (ru)	2008-06-27
MXPA06013372A (es)	2007-03-01
ES2317251T3 (es)	2009-04-16
IL178994A (en)	2010-06-16
WO2005113567A1 (en)	2005-12-01
JP4896881B2 (ja)	2012-03-14
JP2008500395A (ja)	2008-01-10
RU2369611C2 (ru)	2009-10-10
KR20070012828A (ko)	2007-01-29
US7683207B2 (en)	2010-03-23
EP1756127A1 (de)	2007-02-28
UA84345C2 (en)	2008-10-10
BRPI0511434A (pt)	2007-12-26
US20060264655A1 (en)	2006-11-23
CA2564397A1 (en)	2005-12-01
AU2005245973A1 (en)	2005-12-01
ZA200609230B (en)	2008-06-25
CN1953986B (zh)	2011-04-06
DK1756127T3 (da)	2009-03-02
EP1756127B1 (de)	2008-12-17
DE602005011797D1 (de)	2009-01-29
NZ550781A (en)	2009-06-26
IL178994A0 (en)	2007-03-08
PL1756127T3 (pl)	2009-06-30
CN1953986A (zh)	2007-04-25
AU2005245973B2 (en)	2010-09-16
ATE417854T1 (de)	2009-01-15

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