TWI739802B - 黑色粒子及黑色粒子之製造方法 - Google Patents

黑色粒子及黑色粒子之製造方法 Download PDF

Info

Publication number: TWI739802B
Authority: TW; Taiwan
Prior art keywords: black particles; particles; solvent; black; patent application
Prior art date: 2016-02-18

Application number

TW106105444A

Other languages

English (en)

Chinese (zh)

Other versions

TW201733788A (zh

Inventor

孫仁德

野里省二

中壽賀章

伊原隆

高藤誠

桑原穣

村上晶子

Original Assignee

日商積水化學工業股份有限公司

國立大學法人熊本大學

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2016-02-18

Filing date

2017-02-18

Publication date

2021-09-21

2017-02-18 Application filed by 日商積水化學工業股份有限公司, 國立大學法人熊本大學 filed Critical 日商積水化學工業股份有限公司

2017-10-01 Publication of TW201733788A publication Critical patent/TW201733788A/zh

2021-09-21 Application granted granted Critical

2021-09-21 Publication of TWI739802B publication Critical patent/TWI739802B/zh

Links

239000002245 particle Substances 0.000 title claims abstract description 134
238000004519 manufacturing process Methods 0.000 title claims abstract description 16
229920005989 resin Polymers 0.000 claims abstract description 52
239000011347 resin Substances 0.000 claims abstract description 52
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 27
229910052799 carbon Inorganic materials 0.000 claims abstract description 23
229910003481 amorphous carbon Inorganic materials 0.000 claims abstract description 21
238000000034 method Methods 0.000 claims abstract description 21
230000005484 gravity Effects 0.000 claims abstract description 8
238000001069 Raman spectroscopy Methods 0.000 claims abstract description 5
239000002904 solvent Substances 0.000 claims description 29
239000011259 mixed solution Substances 0.000 claims description 18
UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 claims description 12
238000001819 mass spectrum Methods 0.000 claims description 11
NXPPAOGUKPJVDI-UHFFFAOYSA-N naphthalene-1,2-diol Chemical compound C1=CC=CC2=C(O)C(O)=CC=C21 NXPPAOGUKPJVDI-UHFFFAOYSA-N 0.000 claims description 11
ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 10
238000005011 time of flight secondary ion mass spectroscopy Methods 0.000 claims description 10
238000002042 time-of-flight secondary ion mass spectrometry Methods 0.000 claims description 10
238000009835 boiling Methods 0.000 claims description 8
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 7
238000002441 X-ray diffraction Methods 0.000 claims description 6
239000012046 mixed solvent Substances 0.000 claims description 5
WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims description 3
239000011247 coating layer Substances 0.000 claims 2
238000010292 electrical insulation Methods 0.000 abstract description 6
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 52
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 31
238000010438 heat treatment Methods 0.000 description 23
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 22
238000006243 chemical reaction Methods 0.000 description 17
238000005259 measurement Methods 0.000 description 14
230000000052 comparative effect Effects 0.000 description 13
239000000049 pigment Substances 0.000 description 10
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
239000006229 carbon black Substances 0.000 description 8
238000001035 drying Methods 0.000 description 8
239000002994 raw material Substances 0.000 description 8
125000001624 naphthyl group Chemical group 0.000 description 7
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical group C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
QMMFVYPAHWMCMS-UHFFFAOYSA-N Dimethyl sulfide Chemical compound CSC QMMFVYPAHWMCMS-UHFFFAOYSA-N 0.000 description 6
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 6
238000000349 field-emission scanning electron micrograph Methods 0.000 description 6
-1 formaldehyde, amines Chemical class 0.000 description 6
239000000243 solution Substances 0.000 description 6
FRASJONUBLZVQX-UHFFFAOYSA-N 1,4-dioxonaphthalene Natural products C1=CC=C2C(=O)C=CC(=O)C2=C1 FRASJONUBLZVQX-UHFFFAOYSA-N 0.000 description 5
BOKGTLAJQHTOKE-UHFFFAOYSA-N 1,5-dihydroxynaphthalene Chemical compound C1=CC=C2C(O)=CC=CC2=C1O BOKGTLAJQHTOKE-UHFFFAOYSA-N 0.000 description 5
IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 5
238000003763 carbonization Methods 0.000 description 5
239000000126 substance Substances 0.000 description 5
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 4
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 4
239000003738 black carbon Substances 0.000 description 4
239000006185 dispersion Substances 0.000 description 4
239000011261 inert gas Substances 0.000 description 4
239000000203 mixture Substances 0.000 description 4
229910052757 nitrogen Inorganic materials 0.000 description 4
150000002989 phenols Chemical class 0.000 description 4
238000003756 stirring Methods 0.000 description 4
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
238000005481 NMR spectroscopy Methods 0.000 description 3
238000004458 analytical method Methods 0.000 description 3
239000007864 aqueous solution Substances 0.000 description 3
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
230000008859 change Effects 0.000 description 3
239000003086 colorant Substances 0.000 description 3
230000000694 effects Effects 0.000 description 3
238000000635 electron micrograph Methods 0.000 description 3
239000011521 glass Substances 0.000 description 3
238000009413 insulation Methods 0.000 description 3
150000002500 ions Chemical class 0.000 description 3
238000002156 mixing Methods 0.000 description 3
239000001301 oxygen Substances 0.000 description 3
229910052760 oxygen Inorganic materials 0.000 description 3
238000006116 polymerization reaction Methods 0.000 description 3
230000009257 reactivity Effects 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 2
229930040373 Paraformaldehyde Natural products 0.000 description 2
239000004372 Polyvinyl alcohol Substances 0.000 description 2
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
150000001335 aliphatic alkanes Chemical class 0.000 description 2
125000000217 alkyl group Chemical group 0.000 description 2
150000001412 amines Chemical class 0.000 description 2
229910052786 argon Inorganic materials 0.000 description 2
125000005605 benzo group Chemical group 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
238000010000 carbonizing Methods 0.000 description 2
238000001962 electrophoresis Methods 0.000 description 2
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
238000011156 evaluation Methods 0.000 description 2
239000000945 filler Substances 0.000 description 2
239000008098 formaldehyde solution Substances 0.000 description 2
229910002804 graphite Inorganic materials 0.000 description 2
239000010439 graphite Substances 0.000 description 2
238000010191 image analysis Methods 0.000 description 2
239000000976 ink Substances 0.000 description 2
239000011159 matrix material Substances 0.000 description 2
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 2
239000003973 paint Substances 0.000 description 2
ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
229920000642 polymer Polymers 0.000 description 2
229920006324 polyoxymethylene Polymers 0.000 description 2
229920002451 polyvinyl alcohol Polymers 0.000 description 2
238000001556 precipitation Methods 0.000 description 2
WGYKZJWCGVVSQN-UHFFFAOYSA-N propylamine Chemical compound CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 description 2
238000005245 sintering Methods 0.000 description 2
238000003860 storage Methods 0.000 description 2
LNETULKMXZVUST-UHFFFAOYSA-N 1-naphthoic acid Chemical compound C1=CC=C2C(C(=O)O)=CC=CC2=C1 LNETULKMXZVUST-UHFFFAOYSA-N 0.000 description 1
238000005160 1H NMR spectroscopy Methods 0.000 description 1
QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 1
YZCKVEUIGOORGS-OUBTZVSYSA-N Deuterium Chemical compound [2H] YZCKVEUIGOORGS-OUBTZVSYSA-N 0.000 description 1
XCIBSLBQRBITCY-UHFFFAOYSA-N OC1=CC2=CC=C(C=C2C=C1)O.C1=CC=CC2=CC=CC=C12 Chemical compound OC1=CC2=CC=C(C=C2C=C1)O.C1=CC=CC2=CC=CC=C12 XCIBSLBQRBITCY-UHFFFAOYSA-N 0.000 description 1
238000001237 Raman spectrum Methods 0.000 description 1
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
239000006230 acetylene black Substances 0.000 description 1
238000005054 agglomeration Methods 0.000 description 1
230000002776 aggregation Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
230000008901 benefit Effects 0.000 description 1
HUFIRBOBXZUFPV-UHFFFAOYSA-N benzene-1,3-diol Chemical compound OC1=CC=CC(O)=C1.OC1=CC=CC(O)=C1 HUFIRBOBXZUFPV-UHFFFAOYSA-N 0.000 description 1
230000005540 biological transmission Effects 0.000 description 1
239000003575 carbonaceous material Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000004020 conductor Substances 0.000 description 1
238000011109 contamination Methods 0.000 description 1
229930003836 cresol Natural products 0.000 description 1
239000013078 crystal Substances 0.000 description 1
238000002447 crystallographic data Methods 0.000 description 1
125000001995 cyclobutyl group Chemical group [H]C1([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 description 1
125000004850 cyclobutylmethyl group Chemical group C1(CCC1)C* 0.000 description 1
125000001511 cyclopentyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 description 1
125000001559 cyclopropyl group Chemical group [H]C1([H])C([H])([H])C1([H])* 0.000 description 1
125000004186 cyclopropylmethyl group Chemical group [H]C([H])(*)C1([H])C([H])([H])C1([H])[H] 0.000 description 1
229910052805 deuterium Inorganic materials 0.000 description 1
229910003460 diamond Inorganic materials 0.000 description 1
239000010432 diamond Substances 0.000 description 1
239000002270 dispersing agent Substances 0.000 description 1
239000003822 epoxy resin Substances 0.000 description 1
238000000445 field-emission scanning electron microscopy Methods 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
229940030980 inova Drugs 0.000 description 1
230000010354 integration Effects 0.000 description 1
125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
239000004973 liquid crystal related substance Substances 0.000 description 1
238000004949 mass spectrometry Methods 0.000 description 1
SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 description 1
125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
XOOMNEFVDUTJPP-UHFFFAOYSA-N naphthalene-1,3-diol Chemical compound C1=CC=CC2=CC(O)=CC(O)=C21 XOOMNEFVDUTJPP-UHFFFAOYSA-N 0.000 description 1
FZZQNEVOYIYFPF-UHFFFAOYSA-N naphthalene-1,6-diol Chemical compound OC1=CC=CC2=CC(O)=CC=C21 FZZQNEVOYIYFPF-UHFFFAOYSA-N 0.000 description 1
ZUVBIBLYOCVYJU-UHFFFAOYSA-N naphthalene-1,7-diol Chemical compound C1=CC=C(O)C2=CC(O)=CC=C21 ZUVBIBLYOCVYJU-UHFFFAOYSA-N 0.000 description 1
JRNGUTKWMSBIBF-UHFFFAOYSA-N naphthalene-2,3-diol Chemical compound C1=CC=C2C=C(O)C(O)=CC2=C1 JRNGUTKWMSBIBF-UHFFFAOYSA-N 0.000 description 1
MNZMMCVIXORAQL-UHFFFAOYSA-N naphthalene-2,6-diol Chemical compound C1=C(O)C=CC2=CC(O)=CC=C21 MNZMMCVIXORAQL-UHFFFAOYSA-N 0.000 description 1
DFQICHCWIIJABH-UHFFFAOYSA-N naphthalene-2,7-diol Chemical compound C1=CC(O)=CC2=CC(O)=CC=C21 DFQICHCWIIJABH-UHFFFAOYSA-N 0.000 description 1
238000006386 neutralization reaction Methods 0.000 description 1
238000001579 optical reflectometry Methods 0.000 description 1
230000000737 periodic effect Effects 0.000 description 1
239000005011 phenolic resin Substances 0.000 description 1
229920000647 polyepoxide Polymers 0.000 description 1
229920000417 polynaphthalene Polymers 0.000 description 1
239000000843 powder Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
230000002265 prevention Effects 0.000 description 1
230000008569 process Effects 0.000 description 1
239000000047 product Substances 0.000 description 1
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
238000000985 reflectance spectrum Methods 0.000 description 1
238000007086 side reaction Methods 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
229910000029 sodium carbonate Inorganic materials 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
239000012798 spherical particle Substances 0.000 description 1
239000003381 stabilizer Substances 0.000 description 1
125000001424 substituent group Chemical group 0.000 description 1
239000006228 supernatant Substances 0.000 description 1
239000003115 supporting electrolyte Substances 0.000 description 1
230000001629 suppression Effects 0.000 description 1
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
229920001187 thermosetting polymer Polymers 0.000 description 1
238000001291 vacuum drying Methods 0.000 description 1
235000012431 wafers Nutrition 0.000 description 1

Images

Classifications

- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/44—Carbon
- C09C1/48—Carbon black
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/02—Amorphous compounds
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/84—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/89—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by mass-spectroscopy
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Compositions Of Macromolecular Compounds (AREA)
Pigments, Carbon Blacks, Or Wood Stains (AREA)
Carbon And Carbon Compounds (AREA)

TW106105444A 2016-02-18 2017-02-18 黑色粒子及黑色粒子之製造方法 TWI739802B (zh)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
JP2016029267		2016-02-18
JPJP2016-029267		2016-02-18

Publications (2)

Publication Number	Publication Date
TW201733788A TW201733788A (zh)	2017-10-01
TWI739802B true TWI739802B (zh)	2021-09-21

Family

ID=59625259

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
TW106105444A TWI739802B (zh)	2016-02-18	2017-02-18	黑色粒子及黑色粒子之製造方法

Country Status (7)

Country	Link
US (1)	US20180354798A1 (de)
EP (1)	EP3418334A4 (de)
JP (1)	JP6941837B2 (de)
KR (1)	KR102658084B1 (de)
CN (1)	CN107949606B (de)
TW (1)	TWI739802B (de)
WO (1)	WO2017142087A1 (de)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP7112192B2 (ja) *	2017-11-07	2022-08-03	株式会社日本触媒	炭素材料の製造方法
JP7480035B2 (ja) *	2019-02-20	2024-05-09	積水化学工業株式会社	樹脂組成物、硬化物、ブラックマトリックス、カラーフィルタ、液晶表示装置、有機エレクトロルミネッセンス表示装置及び樹脂組成物の製造方法
WO2020202819A1 (ja) *	2019-04-04	2020-10-08	ナミックス株式会社	多孔質炭素及び樹脂組成物
JP7289477B2 (ja) *	2019-05-14	2023-06-12	積水化学工業株式会社	カーボン被覆粒子及び黒色顔料
KR102380787B1 (ko)	2019-09-24	2022-03-31	서울과학기술대학교 산학협력단	흑색 이산화티탄을 이용한 전기영동 디스플레이용 안료 및 잉크
JP7642376B2 (ja) *	2019-11-18	2025-03-10	積水化学工業株式会社	黒色粒子、黒色塗料、塗膜及びカラーフィルター用ブラックマトリクス
JP7784308B2 (ja) *	2020-08-31	2025-12-11	積水化学工業株式会社	近赤外線透過性黒色材料

Citations (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2011068829A (ja) *	2009-09-28	2011-04-07	Sekisui Chem Co Ltd	耐熱膜の製造方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS543501B1 (de)	1971-03-19	1979-02-23
US5152939A (en) *	1991-03-12	1992-10-06	Edison Polymer Innovation Corp.	Composite densification with benzoxazines
JPH1197011A (ja) *	1997-09-17	1999-04-09	Unitika Ltd	非水リチウム二次電池
JP3576433B2 (ja) *	1999-10-18	2004-10-13	群栄化学工業株式会社	球状フェノール樹脂の製造方法
JP4473515B2 (ja) *	2003-03-20	2010-06-02	リグナイト株式会社	カーボン・オキサジン系化合物複合成形材料及び燃料電池用セパレータ
JP4338479B2 (ja)	2003-09-04	2009-10-07	富士フイルム株式会社	カラーフィルター及びその製造方法
TW200801077A (en) *	2006-05-01	2008-01-01	Sekisui Chemical Co Ltd	Sintered resin product and electronic device comprising the same
CN101157451B (zh) *	2007-09-16	2011-04-06	中国科学院山西煤炭化学研究所	一种树脂基球炭的制备方法
CN101830457B (zh) *	2010-05-20	2012-01-25	湖南大学	一种炭微球的制备方法及杂多酸在炭微球制备和石墨化中的应用
CN102225996B (zh) *	2011-05-06	2013-07-31	大连理工大学	一种苯并噁嗪树脂纳米聚合物球及炭球的制备方法
JP5883875B2 (ja)	2011-08-19	2016-03-15	積水化学工業株式会社	炭素繊維複合材の製造方法
BR112015012142A2 (pt) *	2012-11-26	2017-07-11	Energ2 Tech Inc	preparação de resinas poliméricas e materiais de carbono
JP5934127B2 (ja) *	2013-02-26	2016-06-15	積水化学工業株式会社	繊維束の製造方法
JP2015093883A (ja) *	2013-11-08	2015-05-18	積水化学工業株式会社	炭素繊維複合材及び炭素繊維
EP3199494B1 (de) *	2014-09-22	2019-03-13	Sekisui Chemical Co., Ltd.	Kohlenstoffbeschichtete vanadiumdioxidpartikel
JP2016097654A (ja) *	2014-11-26	2016-05-30	積水化学工業株式会社	繊維基材、樹脂シート、繊維基材の製造方法及び樹脂シートの製造方法

2017
- 2017-02-17 KR KR1020187006979A patent/KR102658084B1/ko active Active
- 2017-02-17 US US16/066,771 patent/US20180354798A1/en not_active Abandoned
- 2017-02-17 EP EP17753341.1A patent/EP3418334A4/de active Pending
- 2017-02-17 JP JP2017518168A patent/JP6941837B2/ja active Active
- 2017-02-17 CN CN201780002945.9A patent/CN107949606B/zh active Active
- 2017-02-17 WO PCT/JP2017/005999 patent/WO2017142087A1/ja not_active Ceased
- 2017-02-18 TW TW106105444A patent/TWI739802B/zh not_active IP Right Cessation

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2011068829A (ja) *	2009-09-28	2011-04-07	Sekisui Chem Co Ltd	耐熱膜の製造方法

Also Published As

Publication number	Publication date
EP3418334A4 (de)	2019-10-09
WO2017142087A1 (ja)	2017-08-24
CN107949606A (zh)	2018-04-20
TW201733788A (zh)	2017-10-01
JPWO2017142087A1 (ja)	2018-12-13
KR20180115664A (ko)	2018-10-23
US20180354798A1 (en)	2018-12-13
EP3418334A1 (de)	2018-12-26
KR102658084B1 (ko)	2024-04-16
JP6941837B2 (ja)	2021-09-29
CN107949606B (zh)	2021-10-12

Legal Events

Date	Code	Title	Description
2023-06-21	MM4A	Annulment or lapse of patent due to non-payment of fees

Publication	Publication Date	Title
TWI739802B (zh)	2021-09-21	黑色粒子及黑色粒子之製造方法
Su et al.	2012	Synthesis and characterization of polypyrrole doped with anionic spherical polyelectrolyte brushes.
Ramesan	2014	Synthesis, characterization, and properties of new conducting polyaniline/copper sulfide nanocomposites
JP5578175B2 (ja)	2014-08-27	伝導性ナノ複合体およびその製造方法
US10121717B2 (en)	2018-11-06	Carbon-coated thermal conductive material
JPWO2015129466A1 (ja)	2017-03-30	銅ナノ粒子及びその製造方法、銅ナノ粒子分散液、銅ナノインク、銅ナノ粒子の保存方法及び銅ナノ粒子の焼結方法
DE102013002855A1 (de)	2014-08-21	Formulierungen aus gewaschenen Silberdrähten und PEDOT
Khanna et al.	2006	Synthesis of HCl doped polyaniline–CdS nanocomposite by use of organometallic cadmium precursor
KR20140080710A (ko)	2014-07-01	공중합물 캡핑제를 이용한 은 나노와이어 제조방법
CN104010752A (zh)	2014-08-27	银微粒及其制造方法、以及含有该银微粒的导电性糊、导电性膜和电子器件
Bhadra et al.	2010	Synthesis of water soluble sulfonated polyaniline and determination of crystal structure
KR102233293B1 (ko)	2021-03-29	구리포메이트-아민 컴플렉스를 포함하는 잉크 조성물의 제조방법
Vulpe et al.	2006	PAN–PAni nanocomposites obtained in thermocentrifugal fields
JP7784308B2 (ja)	2025-12-11	近赤外線透過性黒色材料
CN111050958A (zh)	2020-04-21	银微粒分散液
KR20160120716A (ko)	2016-10-18	금속 나노 미립자의 제조 방법
Rakić et al.	2014	Formation of nanostructured polyaniline by dopant-free oxidation of aniline in a water/isopropanol mixture
Park et al.	2013	Enhanced dielectric properties of electrospun titanium dioxide/polyvinylidene fluoride nanofibrous composites
Ramalingam et al.	2016	SYNTHESIS, SURFACE AND TEXTURAL CHARACTERIZATION OF Ag DOPED POLYANILINE-SiO 2 (Pan-Ag/RHA) NANOCOMPOSITESDERIVEDFROM BIOMASS MATERIALS.
KR102846922B1 (ko)	2025-08-20	다공질 탄소 및 수지 조성물
Wang et al.	2017	Synthesis, characterization, thermal, electrical and magnetic properties of polyaniline composites with rare earth gadolinium coordination complex
WO2020073101A1 (en)	2020-04-16	Graphitic compositions, coatings and materials
Rathore et al.	2019	Synthesis and Characterization of Copolymer Nanocomposite NMethyl Pyrrole (NMPy) and Aniline-2-Sulphonic Acid (ASA)
KR20210121726A (ko)	2021-10-08	고분산 나노 카본 코팅 조성물
Rathore et al.	2019	Study of Chemically Synthesized Nanocomposite Copolymer of N-methyl Pyrrole and 2, 5-Dimethoxy Aniline