UA41356C2 - Спосіб одержання пікринової кислоти - Google Patents
Спосіб одержання пікринової кислотиInfo
- Publication number
- UA41356C2 UA41356C2 UA95094058A UA95094058A UA41356C2 UA 41356 C2 UA41356 C2 UA 41356C2 UA 95094058 A UA95094058 A UA 95094058A UA 95094058 A UA95094058 A UA 95094058A UA 41356 C2 UA41356 C2 UA 41356C2
- Authority
- UA
- Ukraine
- Prior art keywords
- picric acid
- producing
- nitration
- dinitrophenol
- nitrophenol
- Prior art date
Links
- OXNIZHLAWKMVMX-UHFFFAOYSA-N picric acid Chemical compound OC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O OXNIZHLAWKMVMX-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 238000006396 nitration reaction Methods 0.000 abstract 3
- UFBJCMHMOXMLKC-UHFFFAOYSA-N 2,4-dinitrophenol Chemical compound OC1=CC=C([N+]([O-])=O)C=C1[N+]([O-])=O UFBJCMHMOXMLKC-UHFFFAOYSA-N 0.000 abstract 2
- IQUPABOKLQSFBK-UHFFFAOYSA-N 2-nitrophenol Chemical compound OC1=CC=CC=C1[N+]([O-])=O IQUPABOKLQSFBK-UHFFFAOYSA-N 0.000 abstract 1
- BTJIUGUIPKRLHP-UHFFFAOYSA-N 4-nitrophenol Chemical compound OC1=CC=C([N+]([O-])=O)C=C1 BTJIUGUIPKRLHP-UHFFFAOYSA-N 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/16—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Спосіб отримання пікринової кислоти включає нітрацію нітропохідних фенолу. Здійснюють нітрацію о-нітрофенолу і/або п-нітрофенолу до дінітрофенолу так, щоб продукт, що утворюється, був розчинним у реакційному середовищі, і продовжують нітрацію дінітрофенолу до отримання пікринової кислоти, що випадає в осад.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9410781A FR2724378B1 (fr) | 1994-09-09 | 1994-09-09 | Procede de preparation de l'acide picrique |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA41356C2 true UA41356C2 (uk) | 2001-09-17 |
Family
ID=9466799
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UA95094058A UA41356C2 (uk) | 1994-09-09 | 1995-09-06 | Спосіб одержання пікринової кислоти |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6063967A (uk) |
| EP (1) | EP0700894B1 (uk) |
| JP (2) | JPH0881419A (uk) |
| CN (1) | CN1071307C (uk) |
| DE (1) | DE69508864T2 (uk) |
| FR (1) | FR2724378B1 (uk) |
| HU (1) | HU221379B1 (uk) |
| RU (1) | RU2128642C1 (uk) |
| UA (1) | UA41356C2 (uk) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ITMI991517A1 (it) * | 1999-07-09 | 2001-01-09 | Nicox Sa | Procedimento per ottenere nitrossimetil fenil esterni di derivati dell'acido salicilico |
| JP2005303062A (ja) * | 2004-04-13 | 2005-10-27 | Rubycon Corp | 電解コンデンサ駆動用電解液及び電解コンデンサ |
| JP5787402B2 (ja) * | 2011-08-30 | 2015-09-30 | 国立大学法人 鹿児島大学 | コークス炉ガスの脱硫に使用する吸収液中のピクリン酸還元生成物濃度の測定方法、及び、該測定方法を使用したコークス炉ガスの脱硫方法 |
| JP6039673B2 (ja) | 2011-09-23 | 2016-12-07 | ダブリュ.エル.ゴア アンド アソシエイツ,インコーポレイティドW.L. Gore & Associates, Incorporated | 表面変性フルオロポリマーメンブレン及びその製造方法 |
| RU2631509C1 (ru) * | 2016-07-25 | 2017-09-25 | Федеральное государственное автономное образовательное учреждение высшего образования "Северный (Арктический) федеральный университет имени М.В. Ломоносова" (САФУ) | Способ получения пикриновой кислоты |
| CN117603055A (zh) * | 2023-11-28 | 2024-02-27 | 四川蓝狮科技有限公司 | 一种火工药剂用苦味酸的精制方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB190511005A (en) * | 1905-05-26 | 1906-05-17 | Arthur Henry Johnson | Apparatus for Operating Railway Switch Points and Signals. |
| GB191511005A (en) * | 1915-07-29 | 1919-07-24 | Arthur Heinemann | Improvements in or relating to the Manufacture of Picric Acid. |
| US1393714A (en) * | 1919-10-25 | 1921-10-11 | Du Pont | Process of producing picric acid |
| US1349802A (en) * | 1919-12-30 | 1920-08-17 | Holliday Co Ltd L B | Process of manufacture of picric acid |
| FR2638741B1 (fr) * | 1988-11-07 | 1990-12-28 | Rhone Poulenc Chimie | Procede de preparation de nitrophenols |
| US5720783A (en) * | 1993-05-19 | 1998-02-24 | Elliott; Alan Frederick | Manufacture of ferrous picrate and additives containing same |
-
1994
- 1994-09-09 FR FR9410781A patent/FR2724378B1/fr not_active Expired - Fee Related
-
1995
- 1995-09-06 JP JP7229073A patent/JPH0881419A/ja not_active Withdrawn
- 1995-09-06 UA UA95094058A patent/UA41356C2/uk unknown
- 1995-09-08 JP JP7231417A patent/JPH08176072A/ja not_active Withdrawn
- 1995-09-08 EP EP95402032A patent/EP0700894B1/fr not_active Expired - Lifetime
- 1995-09-08 CN CN95116232A patent/CN1071307C/zh not_active Expired - Fee Related
- 1995-09-08 DE DE69508864T patent/DE69508864T2/de not_active Expired - Fee Related
- 1995-09-08 RU RU95115848A patent/RU2128642C1/ru not_active IP Right Cessation
- 1995-09-08 HU HU9502635A patent/HU221379B1/hu not_active IP Right Cessation
-
1998
- 1998-06-15 US US09/094,595 patent/US6063967A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0700894B1 (fr) | 1999-04-07 |
| DE69508864D1 (de) | 1999-05-12 |
| RU2128642C1 (ru) | 1999-04-10 |
| HUT73556A (en) | 1996-08-28 |
| EP0700894A1 (fr) | 1996-03-13 |
| US6063967A (en) | 2000-05-16 |
| CN1071307C (zh) | 2001-09-19 |
| JPH0881419A (ja) | 1996-03-26 |
| CN1136034A (zh) | 1996-11-20 |
| HU221379B1 (en) | 2002-09-28 |
| JPH08176072A (ja) | 1996-07-09 |
| HU9502635D0 (en) | 1995-11-28 |
| FR2724378B1 (fr) | 1996-12-20 |
| FR2724378A1 (fr) | 1996-03-15 |
| DE69508864T2 (de) | 1999-11-04 |
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