UA73638C2 - A method for producing hydroxylaminesulfate - Google Patents

A method for producing hydroxylaminesulfate Download PDF

Info

Publication number: UA73638C2
Authority: UA; Ukraine
Prior art keywords: concentrated; ammonia; gas; hydroxylamine sulfate; condensation
Prior art date: 2003-08-06

Application number

UA2003087438A

Other languages

English (en)

Ukrainian (uk)

Inventor

Abil Abasovych Mamedov

Ivan Ivanovych Barabash

Olha Viktorivna Konoplina

Original Assignee

Ukrainian State Res And Design

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2003-08-06

Filing date

2003-08-06

Publication date

2005-08-15

2003-08-06 Application filed by Ukrainian State Res And Design filed Critical Ukrainian State Res And Design

2003-08-06 Priority to UA2003087438A priority Critical patent/UA73638C2/uk

2004-05-18 Priority to RU2006101361/15A priority patent/RU2324645C2/ru

2004-05-18 Priority to SK43-2006A priority patent/SK288233B6/sk

2004-05-18 Priority to PL379371A priority patent/PL209559B1/pl

2004-05-18 Priority to PCT/UA2004/000031 priority patent/WO2005014473A1/ru

2005-08-15 Publication of UA73638C2 publication Critical patent/UA73638C2/uk

Links

ZNBNBTIDJSKEAM-UHFFFAOYSA-N 4-[7-hydroxy-2-[5-[5-[6-hydroxy-6-(hydroxymethyl)-3,5-dimethyloxan-2-yl]-3-methyloxolan-2-yl]-5-methyloxolan-2-yl]-2,8-dimethyl-1,10-dioxaspiro[4.5]decan-9-yl]-2-methyl-3-propanoyloxypentanoic acid Chemical compound C1C(O)C(C)C(C(C)C(OC(=O)CC)C(C)C(O)=O)OC11OC(C)(C2OC(C)(CC2)C2C(CC(O2)C2C(CC(C)C(O)(CO)O2)C)C)CC1 ZNBNBTIDJSKEAM-UHFFFAOYSA-N 0.000 title claims abstract description 17
229910000378 hydroxylammonium sulfate Inorganic materials 0.000 title claims abstract description 17
238000004519 manufacturing process Methods 0.000 title abstract description 11
239000007789 gas Substances 0.000 claims abstract description 39
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 34
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
229910017604 nitric acid Inorganic materials 0.000 claims abstract description 19
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 18
229910021529 ammonia Inorganic materials 0.000 claims abstract description 17
238000000034 method Methods 0.000 claims abstract description 17
238000009833 condensation Methods 0.000 claims abstract description 12
230000005494 condensation Effects 0.000 claims abstract description 12
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 11
230000015572 biosynthetic process Effects 0.000 claims abstract description 10
238000007254 oxidation reaction Methods 0.000 claims abstract description 9
230000003647 oxidation Effects 0.000 claims abstract description 8
239000001301 oxygen Substances 0.000 claims abstract description 8
229910052760 oxygen Inorganic materials 0.000 claims abstract description 8
238000003786 synthesis reaction Methods 0.000 claims abstract description 8
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 7
230000003197 catalytic effect Effects 0.000 claims abstract description 7
239000000203 mixture Substances 0.000 claims abstract description 7
239000011541 reaction mixture Substances 0.000 claims abstract description 6
239000001257 hydrogen Substances 0.000 claims abstract description 4
229910052739 hydrogen Inorganic materials 0.000 claims abstract description 4
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 3
GQPLMRYTRLFLPF-UHFFFAOYSA-N nitrous oxide Inorganic materials [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims description 20
239000002253 acid Substances 0.000 claims description 3
238000007865 diluting Methods 0.000 claims 1
238000012876 topography Methods 0.000 claims 1
239000000243 solution Substances 0.000 abstract description 11
238000010790 dilution Methods 0.000 abstract description 5
239000012895 dilution Substances 0.000 abstract description 5
JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 abstract description 4
238000002156 mixing Methods 0.000 abstract description 3
239000000126 substance Substances 0.000 abstract description 2
229910002651 NO3 Inorganic materials 0.000 abstract 4
NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 4
VQTGUFBGYOIUFS-UHFFFAOYSA-N nitrosylsulfuric acid Chemical compound OS(=O)(=O)ON=O VQTGUFBGYOIUFS-UHFFFAOYSA-N 0.000 abstract 3
239000002245 particle Substances 0.000 abstract 2
235000011149 sulphuric acid Nutrition 0.000 abstract 2
239000001117 sulphuric acid Substances 0.000 abstract 2
238000002955 isolation Methods 0.000 abstract 1
238000004886 process control Methods 0.000 abstract 1
MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 6
238000002360 preparation method Methods 0.000 description 5
230000006641 stabilisation Effects 0.000 description 5
238000011105 stabilization Methods 0.000 description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
239000003054 catalyst Substances 0.000 description 4
238000009903 catalytic hydrogenation reaction Methods 0.000 description 3
238000004821 distillation Methods 0.000 description 3
239000003337 fertilizer Substances 0.000 description 3
238000005984 hydrogenation reaction Methods 0.000 description 3
229910052500 inorganic mineral Inorganic materials 0.000 description 3
239000011707 mineral Substances 0.000 description 3
RQCJDSANJOCRMV-UHFFFAOYSA-N [Mn].[Ag] Chemical compound [Mn].[Ag] RQCJDSANJOCRMV-UHFFFAOYSA-N 0.000 description 2
230000006835 compression Effects 0.000 description 2
238000007906 compression Methods 0.000 description 2
238000001816 cooling Methods 0.000 description 2
229910052757 nitrogen Inorganic materials 0.000 description 2
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 description 1
ODUCDPQEXGNKDN-UHFFFAOYSA-N Nitrogen oxide(NO) Natural products O=N ODUCDPQEXGNKDN-UHFFFAOYSA-N 0.000 description 1
241001415849 Strigiformes Species 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
230000033228 biological regulation Effects 0.000 description 1
244000309464 bull Species 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000012141 concentrate Substances 0.000 description 1
239000000110 cooling liquid Substances 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
150000002431 hydrogen Chemical class 0.000 description 1
FGHSTPNOXKDLKU-UHFFFAOYSA-N nitric acid;hydrate Chemical compound O.O[N+]([O-])=O FGHSTPNOXKDLKU-UHFFFAOYSA-N 0.000 description 1
229910052697 platinum Inorganic materials 0.000 description 1
239000002994 raw material Substances 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
239000002912 waste gas Substances 0.000 description 1
239000002699 waste material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
- C01B21/38—Nitric acid

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Fertilizers (AREA)
Electric Connection Of Electric Components To Printed Circuits (AREA)

UA2003087438A 2003-08-06 2003-08-06 A method for producing hydroxylaminesulfate UA73638C2 (en)

Priority Applications (5)

Application Number	Priority Date	Filing Date	Title
UA2003087438A UA73638C2 (en)	2003-08-06	2003-08-06	A method for producing hydroxylaminesulfate
RU2006101361/15A RU2324645C2 (ru)	2003-08-06	2004-05-18	Способ получения гидроксиламинсульфата
SK43-2006A SK288233B6 (sk)	2003-08-06	2004-05-18	Spôsob výroby hydroxylamínu síranu
PL379371A PL209559B1 (pl)	2003-08-06	2004-05-18	Sposób wytwarzania siarczanu hydroksyloaminy
PCT/UA2004/000031 WO2005014473A1 (en)	2003-08-06	2004-05-18	Method for producing hydroxylamine sulphate

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
UA2003087438A UA73638C2 (en)	2003-08-06	2003-08-06	A method for producing hydroxylaminesulfate

Publications (1)

Publication Number	Publication Date
UA73638C2 true UA73638C2 (en)	2005-08-15

Family

ID=34134568

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
UA2003087438A UA73638C2 (en)	2003-08-06	2003-08-06	A method for producing hydroxylaminesulfate

Country Status (5)

Country	Link
PL (1)	PL209559B1 (pl)
RU (1)	RU2324645C2 (pl)
SK (1)	SK288233B6 (pl)
UA (1)	UA73638C2 (pl)
WO (1)	WO2005014473A1 (pl)

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
SU1673505A1 (ru) *	1989-01-24	1991-08-30	Гродненское производственное объединение "Азот" им.С.О.Притыцкого	Способ получени гидроксиламинсульфата
RU2045471C1 (ru) *	1991-08-07	1995-10-10	Украинский государственный институт азотной промышленности и продуктов органического синтеза	Способ получения гидроксиламинсульфата и установка для его осуществления
DE4132800A1 (de) *	1991-10-02	1993-04-08	Basf Ag	Verfahren zur herstellung von hydroxylammoniumsulfat
RU2257340C1 (ru) *	2003-01-20	2005-07-27	Украинский государственный научно-исследовательский и проектный институт азотной промышленности и продуктов органического синтеза (УкрГИАП)	Способ получения гидроксиламинсульфата

2003
- 2003-08-06 UA UA2003087438A patent/UA73638C2/uk unknown
2004
- 2004-05-18 RU RU2006101361/15A patent/RU2324645C2/ru not_active IP Right Cessation
- 2004-05-18 WO PCT/UA2004/000031 patent/WO2005014473A1/ru not_active Ceased
- 2004-05-18 SK SK43-2006A patent/SK288233B6/sk not_active IP Right Cessation
- 2004-05-18 PL PL379371A patent/PL209559B1/pl not_active IP Right Cessation

Also Published As

Publication number	Publication date
SK288233B6 (sk)	2014-12-04
WO2005014473A1 (en)	2005-02-17
PL209559B1 (pl)	2011-09-30
PL379371A1 (pl)	2006-08-21
SK432006A3 (sk)	2006-08-03
RU2006101361A (ru)	2006-07-10
RU2324645C2 (ru)	2008-05-20

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