WO2009014682A3 - Procédé de surveillance d'une réaction de polymérisation - Google Patents

Procédé de surveillance d'une réaction de polymérisation Download PDF

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Publication number
WO2009014682A3
WO2009014682A3 PCT/US2008/008871 US2008008871W WO2009014682A3 WO 2009014682 A3 WO2009014682 A3 WO 2009014682A3 US 2008008871 W US2008008871 W US 2008008871W WO 2009014682 A3 WO2009014682 A3 WO 2009014682A3
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WO
WIPO (PCT)
Prior art keywords
reaction
frequency
parameter data
domain data
monitoring
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2008/008871
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English (en)
Other versions
WO2009014682A2 (fr
Inventor
Michael E. Muhle
Richard B. Pannell
Eric J. Markel
Robert O. Hagerty
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Univation Technologies LLC
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Univation Technologies LLC
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Application filed by Univation Technologies LLC filed Critical Univation Technologies LLC
Publication of WO2009014682A2 publication Critical patent/WO2009014682A2/fr
Publication of WO2009014682A3 publication Critical patent/WO2009014682A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1809—Controlling processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0033—Optimalisation processes, i.e. processes with adaptive control systems
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/00044—Temperature measurement
    • B01J2208/00061—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00176—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles outside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00194—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/0061—Controlling the level
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00619—Controlling the weight
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00193—Sensing a parameter
    • B01J2219/00195—Sensing a parameter of the reaction system
    • B01J2219/00198—Sensing a parameter of the reaction system at the reactor inlet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00193—Sensing a parameter
    • B01J2219/00195—Sensing a parameter of the reaction system
    • B01J2219/002—Sensing a parameter of the reaction system inside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00193—Sensing a parameter
    • B01J2219/00195—Sensing a parameter of the reaction system
    • B01J2219/00202—Sensing a parameter of the reaction system at the reactor outlet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00209—Control algorithm transforming a sensed parameter
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00211—Control algorithm comparing a sensed parameter with a pre-set value
    • B01J2219/00216—Parameter value calculated by equations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00211—Control algorithm comparing a sensed parameter with a pre-set value
    • B01J2219/00218—Dynamically variable (in-line) parameter values
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00222—Control algorithm taking actions
    • B01J2219/00225—Control algorithm taking actions stopping the system or generating an alarm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00222—Control algorithm taking actions
    • B01J2219/00227—Control algorithm taking actions modifying the operating conditions
    • B01J2219/00229—Control algorithm taking actions modifying the operating conditions of the reaction system
    • B01J2219/00231—Control algorithm taking actions modifying the operating conditions of the reaction system at the reactor inlet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00222—Control algorithm taking actions
    • B01J2219/00227—Control algorithm taking actions modifying the operating conditions
    • B01J2219/00229—Control algorithm taking actions modifying the operating conditions of the reaction system
    • B01J2219/00234—Control algorithm taking actions modifying the operating conditions of the reaction system inside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00222—Control algorithm taking actions
    • B01J2219/00227—Control algorithm taking actions modifying the operating conditions
    • B01J2219/00238—Control algorithm taking actions modifying the operating conditions of the heat exchange system
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00243—Mathematical modelling
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2400/00—Characteristics for processes of polymerization
    • C08F2400/02—Control or adjustment of polymerization parameters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Automation & Control Theory (AREA)
  • Combustion & Propulsion (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polymerisation Methods In General (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)

Abstract

Dans certains modes de réalisation, l'invention porte sur un procédé consistant à surveiller une réaction de polymérisation pour la production d'une résine dans un système de réacteur à lit fluidisé pour générer des données de paramètre de réaction d'une manière en ligne, transformer par ondelettes les données de paramètre de réaction pour générer des données de domaine de fréquence ou déterminer un aplatissement de chacun d'au moins deux sous-ensembles des données de paramètre de réaction, et facultativement déterminer également à partir des données de domaine de fréquence ou des valeurs d'aplatissement une indication d'au moins l'un parmi le degré de caractère collant de la résine, une approche à ou l'imminence du caractère collant de la résine, et une approche à ou une imminence d'une condition de fonctionnement du réacteur dangereuse ou indésirée qui peut conduire à une formation de dépôts ou à un décollement. Facultativement également, la réaction contrôlée en réponse aux valeurs d'aplatissement ou aux données de domaine de fréquence, par exemple, dans un effort pour prévenir l'apparition d'une formation de dépôts ou autre événement de discontinuité ou pour maintenir le réacteur dans un état non collant, stable.
PCT/US2008/008871 2007-07-24 2008-07-22 Procédé de surveillance d'une réaction de polymérisation Ceased WO2009014682A2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US96177007P 2007-07-24 2007-07-24
US60/961,770 2007-07-24

Publications (2)

Publication Number Publication Date
WO2009014682A2 WO2009014682A2 (fr) 2009-01-29
WO2009014682A3 true WO2009014682A3 (fr) 2009-09-24

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PCT/US2008/008871 Ceased WO2009014682A2 (fr) 2007-07-24 2008-07-22 Procédé de surveillance d'une réaction de polymérisation

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106647597A (zh) * 2016-10-11 2017-05-10 南京工业大学 一种流化床催化燃烧电加热炉plc多段温控方法

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US7910668B2 (en) 2009-05-08 2011-03-22 Univation Technologies, Llc Method for on-line determination of degree or onset of resin stickiness using acoustic data
CN102421805A (zh) * 2009-05-08 2012-04-18 尤尼威蒂恩技术有限责任公司 用于监控聚合反应的系统和方法
CN102191069A (zh) * 2010-03-19 2011-09-21 北京林业大学 一种用于流化床式生物质快速热解设备的监控系统
US9452403B2 (en) 2012-10-19 2016-09-27 Sunedison, Inc. Using wavelet decomposition to determine the fluidization quality in a fluidized bed reactor
US9360453B2 (en) 2012-12-28 2016-06-07 Exxonmobil Research And Engineering Company Instruments for monitoring electrostatic phenomena in reactors
WO2014106078A2 (fr) 2012-12-28 2014-07-03 Exxonmobil Research And Engineering Company Instruments de surveillance de phénomènes électrostatiques dans des réacteurs
WO2014106039A2 (fr) 2012-12-28 2014-07-03 Exxonmobil Research And Engineering Company Procédés de traitement et d'interprétation de signaux provenant de sondes statiques et acoustiques dans des systèmes de réacteur à lit fluidisé
DE102013103689A1 (de) * 2013-02-26 2014-08-28 Franz Binzer Vorrichtung und Verfahren zur thermischen Reststoffverwertung
CN105548366B (zh) * 2015-12-05 2017-12-29 浙江大学 一种聚乙烯流化床气泡传热系数的测定方法
WO2021011768A1 (fr) * 2019-07-18 2021-01-21 Exxonmobil Research And Engineering Company Sondes multisensorielles et systèmes de surveillance de fluidisation
WO2021113040A1 (fr) * 2019-12-05 2021-06-10 Exxonmobil Research And Engineering Company Système de mesure de fluidisation
WO2025111109A1 (fr) 2023-11-21 2025-05-30 ExxonMobil Technology and Engineering Company Système de décharge de produit de réacteur à lit fluidisé en phase gazeuse

Citations (5)

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US6384157B1 (en) * 2000-05-16 2002-05-07 Union Carbide Chemicals & Plastics Technology Corporation Method of detecting and correcting local defluidization and channeling in fluidized-bed reactors for polymerization
WO2003051929A1 (fr) * 2001-12-17 2003-06-26 Univation Technologies Llc Procede d'application d'une dynamique non lineaire pour regler le fonctionnement d'un reacteur de polyethylene en phase gazeuse
US20040083028A1 (en) * 2002-10-28 2004-04-29 Ramaswamy Vaidyanathan Process control using on-line instrumentation and process models
US6826513B1 (en) * 2002-11-29 2004-11-30 Council Of Scientific & Industrial Research Method and apparatus for online identification of safe operation and advance detection of unsafe operation of a system or process
WO2006107437A1 (fr) * 2005-03-31 2006-10-12 Univation Technologies, Llc Procede et systeme pour evaluer une qualite de fluidisation et une efficacite operationnelle d'un reacteur a partir du spectre de frequences de donnees de temperature

Patent Citations (5)

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Publication number Priority date Publication date Assignee Title
US6384157B1 (en) * 2000-05-16 2002-05-07 Union Carbide Chemicals & Plastics Technology Corporation Method of detecting and correcting local defluidization and channeling in fluidized-bed reactors for polymerization
WO2003051929A1 (fr) * 2001-12-17 2003-06-26 Univation Technologies Llc Procede d'application d'une dynamique non lineaire pour regler le fonctionnement d'un reacteur de polyethylene en phase gazeuse
US20040083028A1 (en) * 2002-10-28 2004-04-29 Ramaswamy Vaidyanathan Process control using on-line instrumentation and process models
US6826513B1 (en) * 2002-11-29 2004-11-30 Council Of Scientific & Industrial Research Method and apparatus for online identification of safe operation and advance detection of unsafe operation of a system or process
WO2006107437A1 (fr) * 2005-03-31 2006-10-12 Univation Technologies, Llc Procede et systeme pour evaluer une qualite de fluidisation et une efficacite operationnelle d'un reacteur a partir du spectre de frequences de donnees de temperature

Non-Patent Citations (1)

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Title
Y. STAVROPOULOS, C. KIPARISSIDES: "Development of a prototype MSPC software package for on-line process monitoring and statistical quality control", COMPUT. APPL. ENG. EDUC., vol. 9, no. 3, 19 October 2001 (2001-10-19), pages 157 - 170, XP002538968 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106647597A (zh) * 2016-10-11 2017-05-10 南京工业大学 一种流化床催化燃烧电加热炉plc多段温控方法

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