WO2009089705A1 - Eau de bain comprenant une solution concentrée activée de minéraux naturels et d'eau de mer concentrée activée - Google Patents

Eau de bain comprenant une solution concentrée activée de minéraux naturels et d'eau de mer concentrée activée Download PDF

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Publication number
WO2009089705A1
WO2009089705A1 PCT/CN2008/073219 CN2008073219W WO2009089705A1 WO 2009089705 A1 WO2009089705 A1 WO 2009089705A1 CN 2008073219 W CN2008073219 W CN 2008073219W WO 2009089705 A1 WO2009089705 A1 WO 2009089705A1
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Prior art keywords
natural mineral
powder
solution
acid
trace element
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PCT/CN2008/073219
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English (en)
Chinese (zh)
Inventor
Jishan Yin
Ronghao Han
Shizhu Jin
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/68Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/27Zinc; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/02Non-contaminated water, e.g. for industrial water supply
    • C02F2103/026Treating water for medical or cosmetic purposes

Definitions

  • the invention relates to a bathing liquid and a preparation method thereof, in particular to a complex state bathing liquid containing natural minerals and trace elements and capable of floating the human body.
  • Israel's “Dead Sea” is a famous tourist destination in the Middle East. Because Israel's “Dead Sea” has the dual functions of "floating” and “healing and fitness”, hundreds of tourists from all over the world come to Israel to "dead sea” every year. Tens of thousands of people have brought huge income to the tourism industry in Israel. With the recognition of Israel's “Dead Sea”, various “artificial Dead Seas” have appeared in various places. However, the existing "Artificial Dead Sea” bathing liquid has many fatal shortcomings as follows:
  • the object of the present invention is to provide a natural mineral and trace element complex state bathing liquid and a preparation method thereof, and to solve the problem that the existing bath liquid has a single formula and the floating effect is unstable.
  • the present invention adopts the following technical solutions:
  • a natural mineral and trace element complexed bathing liquid characterized in that: the bath liquid comprises a natural mineral activating concentrate, a seawater activating concentrate, a shell powder, a complexing agent, an acid-base regulator and pure water;
  • the weight ratio of the natural mineral activating concentrate to the seawater activating concentrate is 1: 1 to 50, and the pure water is added in an amount of 0 to 50% of the total weight of the mixture of the natural mineral activating concentrate and the seawater activating concentrate, and the shell powder 5 ⁇
  • the specific gravity is 1. 1 ⁇ 1. 8;
  • the specific gravity is 1. 1 ⁇ 1. 8;
  • the above natural mineral activating concentrate is prepared by using ore powder and a dissolving solution, and the total weight of the ore powder is 100, the content of the zinc ore powder is 20 to 50%, the content of the mica powder is 10 to 20%, and the content of the vermiculite powder is 10 ⁇ 20%, the content of magnesium ore powder is 20 ⁇ 50%; the content of dissolved solution is 1 ⁇ 3 times of the total volume of ore powder.
  • the solution is an inorganic solution, an organic solution or a mixture of the two; the inorganic solution is one or a mixture of sulfuric acid, hydrochloric acid, phosphoric acid, and carbonic acid, and the organic solution is formic acid or acetic acid.
  • the inorganic solution is one or a mixture of sulfuric acid, hydrochloric acid, phosphoric acid, and carbonic acid
  • the organic solution is formic acid or acetic acid.
  • One or a mixture of one or more of oxalic acid and oxalic acid is one or a mixture of one or more of oxalic acid and oxalic acid.
  • the complexing agent is an inorganic complexing agent or an organic complexing agent, wherein the inorganic complexing agent is one or a mixture of ammonia water, sodium carbonate, chloride, iodide or sodium hydrogencarbonate, organic complexing agent It is one or more mixtures of amines or carboxylic acids.
  • the acid-base regulator is one or more alkaline solutions of sodium hydroxide, sodium carbonate, sodium hydrogencarbonate or saponin, or one or more of hydrochloric acid, phosphoric acid, formic acid and acetic acid. Acidic solution.
  • the invention relates to a method for preparing a natural mineral and trace element complex state bathing liquid, which is characterized in that the preparation steps are as follows: Step 1. The ratio of the prepared natural mineral activating concentrated liquid and the seawater activated concentrated liquid is 1:1 to 50. ⁇ 0. Adding a shell powder to adjust the mixture. ⁇ 2. 0 ;
  • Step 2 adding a complexing agent, using a frequency of 5 ⁇ l (MHz, an intensity of 10 ⁇ 15W / cm 2 of ultrasonic treatment 0. 5 ⁇ 1 hours, the metal ions form a stable complex state;
  • Step B the soaking, the raw material is added after the dewatering pressure in the tank lid, was heated to 150 ⁇ 300 ° C, pressurized to l ⁇ 5kg / cm 2 on standing 0.5 5 ⁇ 1 hours, down to room temperature after the fast, Atmospheric pressure
  • Step c moving the treated material into a dissolving tank, adding 1 ⁇ 3 times the volume of the ore powder to the acid solution, soaking at normal temperature and pressure for 2 to 7 hours, and using a frequency of 5 to 1 (MHz, intensity 10) Ultrasonic treatment of ⁇ 15W/cm 2 , soaking for 2 hours, start to send oxygen to the solution in the dissolution tank, and then filter through a microporous filter of 1 ⁇ 5 ⁇ m;
  • the filtrate after the above step c is retained, and the residue is further added with an acid solution of 1 to 3 times the volume of the ore powder, soaked at 40 to 80 ° C for 1 to 5 hours, and treated with ultrasonication. Filter through a 1 to 5 ⁇ m micropore filter.
  • Step I selecting the outer shell of the non-polluting marine shellfish
  • Step II crushing the shell into a fine powder of 90 mesh or more
  • Step III ashing the shell powder at a high temperature
  • Step IV The powder after high temperature ashing is the shell powder.
  • the preparation steps of the above seawater activating concentrate are:
  • Step A extracting seawater into the storage tank
  • Step B filtering
  • Step E activation treatment, to obtain a seawater activated concentrate.
  • the sterilization and disinfection steps described above employ one or a combination of one or more of ozone, ultraviolet light, chlorine dioxide, and sodium hypochlorite disinfection methods.
  • the present invention has the following characteristics and beneficial effects:
  • the invention overcomes the defects of the traditional "artificial Dead Sea” bathing liquid, and provides a variety of minerals and trace elements which are beneficial to human health, can float and bathe the human body, and has leisure entertainment, beauty and fitness.
  • the function of the bath liquid and the preparation method is not limited to:
  • the invention adopts several kinds of natural ores, utilizes advanced production technology, repeatedly extracts minerals and trace elements which are beneficial to human health, and mixes and activates together to form a natural mineral activated concentrate, and then with natural ones.
  • Underground The deep seawater activating concentrate is mixed in proportion to make the water rich in K, Na, Ca, Mg, Sr, Zn, Se, Li, Cu, Fe, Al, Mn, Mo, Ni, Ti, Si, Ge, F, Cl Dozens of natural minerals and trace elements such as Br, I, P, B, and V.
  • the liquid is enough to float the human body, adding a complexing agent, and then adjusting the PH value of the bathing liquid with an acid-base adjusting agent, which is close to neutral, and finally is activated again.
  • Zinc ore the main component is zinc sulfide, containing a large amount of minerals and trace elements such as zinc, iron, gallium, indium and antimony.
  • the purpose is to increase the zinc content of the mineral activation solution.
  • Mica the main component is aluminosilicate, which contains a large amount of macro and trace elements such as potassium, sodium, magnesium, iron, aluminum, titanium, lithium and silicon.
  • the purpose is to enrich the content of potassium, sodium, calcium, magnesium, iron, aluminum, lithium, silicon and other elements in the mineral activation solution.
  • Vermiculite a ferro-magnesium aluminosilicate containing a large amount of natural minerals such as iron, magnesium, aluminum and silicon.
  • the purpose is to increase the content of iron, aluminum, magnesium, silicon and other elements in the mineral activation solution.
  • Magnesium ore is a magnesite ore, whose main component is magnesia. There are other components such as calcium, silicon, manganese and iron. The purpose is to increase the content of magnesium in the activation solution.
  • the present invention Compared with the traditional bath liquid, the present invention has the following main advantages:
  • the main components of the present invention are derived from natural ore and underground seawater. They are not simply prepared by ordinary chemical materials. The various substances contained in the solution are natural, and are truly pure natural floating and bathing liquids.
  • the bathing liquid of the invention contains rich and balanced minerals and trace elements, and the natural mineral activating concentrated solution is activated and treated, and after adding water, the activity of the water can be significantly improved, and the minerals and trace elements in the water are more favorable.
  • the body absorbs, thus giving floating bathing health care, beauty and fitness and many other functions. It can promote blood circulation, promote human metabolism, quickly restore fatigue, and can be used for various skin diseases, cardiovascular and cerebrovascular diseases, diabetes, cervical spondylosis, frozen shoulder, arthritis, shoulder pain, muscle aches, neurasthenia and physical and psychological stress. Syndrome caused by excessive disease has a mitigating effect.
  • the bathing liquid of the invention adopts the conversion technology of natural salt, and the result is that the overall solubility of the salt in the bathing liquid is improved, and sufficient salt is dissolved in the water, and the proportion of the bathing liquid is remarkably and stably increased. (Up to 1. 8), the bath liquid will not crystallize at a lower temperature (minimum of minus 20 degrees), which lays the foundation for the establishment of a large floating bath in the outdoor. It meets the novelty and practicality of the technology of producing goods and has unique social and economic benefits. At the same time, reducing costs by improving product quality, reducing energy consumption in the use of technology and product consumption, reducing the cost of operators, and providing good conditions for the marketization of technology.
  • the complexed bath solution of the present invention does not use magnesium sulfate or sodium salt as a chemical raw material, purely from natural ore and underground sea.
  • the salt obtained by concentration in water is purely natural. Therefore, it is more secure in terms of safety. Even if the bathing liquid is mistaken into the abdomen, it will not cause diarrhea and poisoning.
  • the bath liquid of the present invention is finally activated by an activator, and the substance in the ore solution is paramagnetized during the severe vibration process, and the anions and cations in the ore solution are changed from a random arrangement to a linear arrangement to form a linear condensation. state.
  • This structure has a relatively high energy state, and the addition of water can significantly improve the activity of water.
  • the bathing liquid 11 of the present invention has a value of 5. 5 ⁇ 7. 5, so that it does not cause discomfort to human skin, wounds, facial features, etc.; because the bathing liquid of the present invention can ensure a stable specific gravity of the human body, When people are floating or bathing, they do not need to use complicated protective equipment such as pillows, which reduces unnecessary troubles and easily experiences the pleasure of floating and bathing.
  • Figure 1 is a flow chart of the formulation method of the present invention.
  • a natural mineral and trace element complexed bathing liquid characterized in that: the bath liquid contains a natural mineral activating concentrate, a seawater activating concentrate, a shell powder, a complexing agent, an acid-base regulator and a pure Water; wherein the weight ratio of the natural mineral activating concentrate to the seawater activating concentrate is 1:10, 1:20, 1:30, 1:40 or 1:50, and the pure water is added to the natural mineral activating concentrate ⁇ 1.
  • the specific gravity of the mixture is 1. 1 ⁇ 5%, the specific gravity is 1. 1 ⁇ 5%, the specific gravity is 1. 1 ⁇ 5% 1. 8.
  • the above natural mineral activating concentrate is prepared by using ore powder and a dissolving solution, and the total weight of the ore powder is 100, the zinc ore powder content is 30 to 40%, the mica powder content is 10 to 20%, and the vermiculite powder content is 10 ⁇ 20%, the content of magnesium ore powder is 30 ⁇ 40%; the content of dissolved solution is 1 ⁇ 3 times of the total volume of ore powder.
  • the solution is an inorganic solution, an organic solution or a mixture of the two; the inorganic solution is one or a mixture of sulfuric acid, hydrochloric acid, phosphoric acid, and carbonic acid, and the organic solution is formic acid or acetic acid.
  • the inorganic solution is one or a mixture of sulfuric acid, hydrochloric acid, phosphoric acid, and carbonic acid
  • the organic solution is formic acid or acetic acid.
  • One or a mixture of one or more of oxalic acid and oxalic acid is one or a mixture of one or more of oxalic acid and oxalic acid.
  • the complexing agent is an inorganic complexing agent or an organic complexing agent, wherein the inorganic complexing agent is one or a mixture of ammonia water, sodium carbonate, chloride, iodide or sodium hydrogencarbonate, organic complexing agent It is one or more mixtures of amines or carboxylic acids.
  • the purpose is to cause the dissolved metal ions in the ore to react with the complexing agent to form a stable complex to reduce the precipitation or precipitation of metal ions.
  • the acid-base regulator is one or more alkaline solutions of sodium hydroxide, sodium carbonate, sodium hydrogencarbonate or sodium ketone, or one or more of hydrochloric acid, phosphoric acid, formic acid and acetic acid. Acidic solution.
  • a method for preparing a natural mineral and trace element complexed bath solution is characterized in that the preparation steps are as follows:
  • Step 1 Mix the prepared natural mineral activating concentrate and seawater activating concentrate in a ratio of 1: 1 to 50, add 0 ⁇ 50% pure water of the total weight of the mixture, add shell powder, and add shell powder. ⁇ 1. 8 ⁇ The amount of the mixture is 0.
  • the viscous specific gravity is 1. 1 ⁇ 1. 8.
  • the specific gravity is 1. 1 ⁇ 1.
  • Step 4. Sterilization and disinfection.
  • the above sterilization and disinfection steps adopt one or more combinations of ozone, ultraviolet light, chlorine dioxide and sodium hypochlorite disinfection methods. Then it was filtered with a microporous filter of 0.2 to 5 ⁇ m.
  • Step 5 Activate the treatment with an activator for 1 to 3 hours to obtain a natural mineral and trace element complexed bath solution.
  • the above activator is a device capable of paramagnetizing a substance in a ore solution during a severe vibration process, that is, an anion and a cation in a ore solution is changed from a random arrangement to a linear arrangement to form a linear condensed state existing device. .
  • the preparation steps for the natural mineral activating concentrate are:
  • the step a the zinc ore powder, the mica powder, the vermiculite powder, the magnesium ore powder having a particle size of 50 to 200 mesh are weighed in proportion, soaked in pure water for 0.5 to 1 hour, and dehydrated to a semi-dry.
  • Step B the soaking, the raw material is added after the dewatering pressure in the tank lid, was heated to 150 ⁇ 300 ° C, pressurized to l ⁇ 5kg / cm 2 on standing 0.5 5 ⁇ 1 hours, down to room temperature after the fast, Atmospheric pressure.
  • Step c moving the treated material into a dissolving tank, adding 1 to 3 times the ore powder volume of No. 1 acid solution, soaking at normal temperature and pressure for 2 to 7 hours, and using a frequency of 5 to 1 (MHz, intensity)
  • a frequency of 5 to 1 MHz, intensity
  • immersion for 2 hours began to supply oxygen to the solution in the dissolution tank, and then filtered through a microporous filter of 1 to 5 ⁇ m.
  • No. 1 acid solution 30% to 80% sulfuric acid liquid was prepared with 98% sulfuric acid.
  • No. 1 acid solution is an inorganic or organic acid or In the mixed solution, the inorganic acid comprises one or more of sulfuric acid (concentration 98%), hydrochloric acid (concentration 36%), and phosphoric acid (concentration 90%).
  • step d the filtrate in step 3 is retained, and the residue is further added with 1 to 3 times the ore powder volume of the No. 2 acid solution, soaked at 40 to 80 ° C for 1 to 5 hours, while continuing to use the above ultrasonic treatment, by 1 Filter through a ⁇ 5 ⁇ microporous filter.
  • No. 2 acid solution 36% hydrochloric acid and 36% oxalic acid 1: 1 mixed.
  • the No. 2 acid solution is a mixture of one or more of organic acids including formic acid (concentration 30%), acetic acid (concentration 36%), and oxalic acid (20% concentration), the purpose of which is to maximize the metal ions in the ore. Limit to dissolve in the solution.
  • Step e the filtrate obtained in the steps 3 and 4 is mixed, mixed with a complexing agent, and activated by an activator for 1 to 8 hours to obtain a natural mineral activating concentrate.
  • the preparation steps of the above seawater activating concentrate are:
  • Step A Extract natural underground seawater into the storage tank for use.
  • Step B filtering through a 0.2 to 1 ⁇ m filter.
  • Step D transfer to a concentrator for concentration for 1 to 10 hours.
  • Step E activation treatment with an activator for 1 to 5 hours, to obtain a submerged seawater activated concentrate.
  • Step I select the outer shell of the natural, non-polluting shellfish.
  • Step II crush the shell into a fine powder of 100 mesh.
  • Step III The shell powder is added to the ashing furnace and ashed at a temperature of 500 to 1000 °C.
  • Step IV After collecting high temperature ashing, the remaining powder is shell powder.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Veterinary Medicine (AREA)
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  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
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  • Inorganic Chemistry (AREA)
  • Hydrology & Water Resources (AREA)
  • Organic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
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  • Engineering & Computer Science (AREA)
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Abstract

L'invention porte sur une eau de bain comprenant une solution concentrée activée de minéraux naturels, de l'eau de mer concentrée activée, de la poudre de coquille, un agent chélatant, un agent d'ajustement du pH et de l'eau pure. Ladite solution concentrée activée de minéraux naturels et ladite eau de mer concentrée activée sont mélangées dans le rapport de 1:1-50. Sur la base de la quantité totale dudit mélange ci-dessus, la quantité de poudre de coquille est de 0-30 %. Ladite eau de bain a un pH de 5,5-7,5 et la densité de 1,1-1,8. Ladite solution concentrée activée de minéraux naturels est préparée par dissolution de la poudre de minerais dans la solution de dissolution. Ladite poudre de minerais comprend des minerais parmi le minerai de zinc, le mica, la vermiculite et le minerai de magnésium.
PCT/CN2008/073219 2008-01-14 2008-11-27 Eau de bain comprenant une solution concentrée activée de minéraux naturels et d'eau de mer concentrée activée Ceased WO2009089705A1 (fr)

Applications Claiming Priority (2)

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CN200810300091.5 2008-01-14
CNA2008103000915A CN101268997A (zh) 2008-01-14 2008-01-14 天然矿物质和微量元素络合态洗浴液及其配制方法

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WO2009089705A1 true WO2009089705A1 (fr) 2009-07-23

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Publication number Priority date Publication date Assignee Title
CN101268997A (zh) * 2008-01-14 2008-09-24 尹吉山 天然矿物质和微量元素络合态洗浴液及其配制方法
CN101822403B (zh) * 2010-04-20 2012-12-26 王衍洲 海洋元素电解浓缩产品及其制造方法
CN104313617A (zh) * 2014-11-07 2015-01-28 合肥大安印刷有限责任公司 一种除锈金属表面清洗剂及其制备方法
CN105330421A (zh) * 2014-11-15 2016-02-17 深圳市芭田生态工程股份有限公司 一种络合态矿物质元素有机液体肥的制备方法
CN106316552A (zh) * 2015-06-18 2017-01-11 刘海涛 一种黄腐酸矿物质肥及其制备方法
CN111803518A (zh) * 2020-07-22 2020-10-23 烟台冠玉生物科技有限公司 一种液体微量元素、制备方法及用途

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Publication number Priority date Publication date Assignee Title
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JP2003246739A (ja) * 2002-02-25 2003-09-02 Hoso Shizai Center:Kk 健康水およびその製造方法
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