WO2010022830A3 - Katalysator für die katalytische gasphasenoxidation von aromatischen kohlenwasserstoffen zu aldehyden, carbonsäuren und/oder carbonsäureanhydriden, insbesondere zu phthalsäurenanhydrid, sowie verfahren zur herstellung eines solchen katalysators - Google Patents

Katalysator für die katalytische gasphasenoxidation von aromatischen kohlenwasserstoffen zu aldehyden, carbonsäuren und/oder carbonsäureanhydriden, insbesondere zu phthalsäurenanhydrid, sowie verfahren zur herstellung eines solchen katalysators Download PDF

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WO2010022830A3
WO2010022830A3 PCT/EP2009/005372 EP2009005372W WO2010022830A3 WO 2010022830 A3 WO2010022830 A3 WO 2010022830A3 EP 2009005372 W EP2009005372 W EP 2009005372W WO 2010022830 A3 WO2010022830 A3 WO 2010022830A3
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catalyst
vanadium
mixing element
producing
gas phase
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French (fr)
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WO2010022830A2 (de
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Josef Breimair
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Priority to CN200980142796.1A priority Critical patent/CN102196859B/zh
Priority to EP09777410A priority patent/EP2321045A2/de
Priority to KR1020117006837A priority patent/KR101706790B1/ko
Priority to BRPI0913160-4A priority patent/BRPI0913160B1/pt
Publication of WO2010022830A2 publication Critical patent/WO2010022830A2/de
Publication of WO2010022830A3 publication Critical patent/WO2010022830A3/de
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/66—Silver or gold
    • B01J23/68—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20—Vanadium, niobium or tantalum
    • B01J23/22—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/66—Silver or gold
    • B01J23/68—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/682—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium, tantalum or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/66—Silver or gold
    • B01J23/68—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/683—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with chromium, molybdenum or tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198—Vanadium
    • B01J27/199—Vanadium with chromium, molybdenum, tungsten or polonium
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    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/391—Physical properties of the active metal ingredient
    • B01J35/395—Thickness of the active catalytic layer
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    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
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    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0219—Coating the coating containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
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    • B01J37/0221—Coating of particles
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    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0228—Coating in several steps
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B41/00—Formation or introduction of functional groups containing oxygen
    • C07B41/08—Formation or introduction of functional groups containing oxygen of carboxyl groups or salts, halides or anhydrides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
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    • C07D307/87—Benzo [c] furans; Hydrogenated benzo [c] furans
    • C07D307/89—Benzo [c] furans; Hydrogenated benzo [c] furans with two oxygen atoms directly attached in positions 1 and 3
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    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)

Abstract

Die Erfindung betrifft einen Katalysator für die katalytische Gasphasenoxidation von aromatischen Kohlenwasserstoffen zu Aldehyden, Carbonsäuren und/oder Carbonsäureanhydriden, insbesondere zu Phthalsäureanhydrid, wobei die aktive Masse Vanadiumoxid, bevorzugt Vanadiumpentoxid, Titandioxid, bevorzugt in der Anatas-Modifikation, und mindestens ein Mischelementoxid des Silbers mit definierten Elementen, bevorzugt Vanadium und/oder Molybdän und/oder Wolfram und/oder Niob und/oder Antimon, und/oder ein Mischelementoxid des Vanadiums mit definierten Elementen, bevorzugt Wismut und/oder Molybdän und/oder Wolfram und/oder Antimon und/oder Niob, aufweist, und wobei bei der Herstellung des Katalysators, insbesondere bei der Herstellung einer Katalysatorsuspension oder eines für die Beschichtung eines Trägers benötigten Pulvergemisches, mindestens ein Mischelementoxid des Silbers und/oder des Vanadiums und/oder mindestens eine Vorläuferverbindung, insbesondere mindestens eine mehrkernige Vorläuferverbindung, mindestens eines Mischelementoxides des Silbers und/oder des Vanadiums als Rohstoffquelle eingesetzt ist.
PCT/EP2009/005372 2008-08-29 2009-07-24 Katalysator für die katalytische gasphasenoxidation von aromatischen kohlenwasserstoffen zu aldehyden, carbonsäuren und/oder carbonsäureanhydriden, insbesondere zu phthalsäurenanhydrid, sowie verfahren zur herstellung eines solchen katalysators Ceased WO2010022830A2 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN200980142796.1A CN102196859B (zh) 2008-08-29 2009-07-24 用于将芳族烃催化气相氧化以得到醛、羧酸和/或羧酸酐，特别是得到邻苯二甲酸酐的催化剂，以及用于制备这种催化剂的方法
EP09777410A EP2321045A2 (de) 2008-08-29 2009-07-24 Katalysator für die katalytische gasphasenoxidation von aromatischen kohlenwasserstoffen zu aldehyden, carbonsäuren und/oder carbonsäureanhydriden, insbesondere zu phthalsäurenanhydrid, sowie verfahren zur herstellung eines solchen katalysators
KR1020117006837A KR101706790B1 (ko) 2008-08-29 2009-07-24 촉매 기상 산화반응에 의해 방향족 탄화수소로부터 알데히드, 카르복실산 및 카르복실산 무수물, 특히 프탈산 무수물을 형성하기 위한 촉매 및 상기 유형의 촉매 제조 방법
BRPI0913160-4A BRPI0913160B1 (pt) 2008-08-29 2009-07-24 Catalisador para a oxidação catalítica de fase gasosa de hidrocarbonetos aromáticos formando aldeídos, ácidos carboxílicos e/ou anidridos de ácido carboxílico, especialmente anidrido de ácido ftálico, assim como método para a fabricação de um catalisador desse tipo

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102008044890.7A DE102008044890B4 (de) 2008-08-29 2008-08-29 Katalysator für die katalytische Gasphasenoxidation von aromatischen Kohlenwasserstoffen zu Aldehyden, Carbonsäuren und/oder Carbonsäureanhydriden, insbesondere zu Phthalsäureanhydrid, sowie Verfahren zur Herstellung eines solchen Katalysators
DE102008044890.7 2008-08-29

Publications (2)

Publication Number Publication Date
WO2010022830A2 WO2010022830A2 (de) 2010-03-04
WO2010022830A3 true WO2010022830A3 (de) 2010-05-20

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PCT/EP2009/005372 Ceased WO2010022830A2 (de) 2008-08-29 2009-07-24 Katalysator für die katalytische gasphasenoxidation von aromatischen kohlenwasserstoffen zu aldehyden, carbonsäuren und/oder carbonsäureanhydriden, insbesondere zu phthalsäurenanhydrid, sowie verfahren zur herstellung eines solchen katalysators

Country Status (7)

Country Link
EP (1) EP2321045A2 (de)
KR (1) KR101706790B1 (de)
CN (1) CN102196859B (de)
BR (1) BRPI0913160B1 (de)
DE (1) DE102008044890B4 (de)
TW (1) TWI518079B (de)
WO (1) WO2010022830A2 (de)

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CN104968435A (zh) * 2013-02-07 2015-10-07 巴斯夫欧洲公司 制备呈包含元素Mo和V的多元素氧化物与至少一种钼的氧化物的混合物的催化活性组合物的方法

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EP2501472A1 (de) * 2009-11-20 2012-09-26 Basf Se Mehrlagenkatalysator zur herstellung von carbonsäuren und/oder carbonsäureanhydriden mit vanadiumantimonat in wenigstens einer katalysatorlage und verfahren zur herstellung von phthalsäureanhydrid mit niedriger hotspottemperatur
EP3047904A1 (de) 2015-01-22 2016-07-27 Basf Se Katalysatorsystem zur Oxidierung von O-Xylen und/oder Naphthalen zu Phthalsäureanhydrid
CN107999107A (zh) * 2016-10-28 2018-05-08 中国石油化工股份有限公司 一种顺酐催化剂及其制备方法和应用
DE102017202351A1 (de) * 2017-02-14 2018-08-16 Clariant International Ltd Katalysatormaterial zur Oxidation von Kohlenwasserstoffen mit antimondotiertem Titandioxid
NL2018890B1 (en) * 2017-05-10 2018-11-15 Admatec Europe B V Additive manufacturing of metal objects
CN109110910A (zh) * 2018-08-31 2019-01-01 江苏新亿源环保科技有限公司 一种高催化性悬浮梯级生物滤料的制备方法
CN109158119A (zh) * 2018-09-14 2019-01-08 中海油天津化工研究设计院有限公司 一种用于均四甲苯氧化的催化剂及制备方法
CN109369544B (zh) * 2018-12-05 2022-06-03 兰州大学 一种催化氧化制备5-甲基吡嗪-2-羧酸的方法
CN113926452A (zh) * 2020-06-29 2022-01-14 中国石油化工股份有限公司 一种钒银铋金属氧化物催化剂、制备方法及其应用
CN114100651B (zh) * 2020-08-25 2023-12-08 中国石油化工股份有限公司 一种苯氧化制顺酐催化剂及其制备方法和应用
CN114539207B (zh) * 2020-11-24 2023-09-19 万华化学(四川)有限公司 一种制备丙交酯的方法及催化剂
CN114682278B (zh) * 2020-12-29 2023-09-01 中国石油化工股份有限公司 一种抗失磷钒磷氧催化剂
IT202100021746A1 (it) 2021-08-11 2023-02-11 Polynt S P A Letto catalitico multistrato per la produzione di anidride ftalica.
CN117123243B (zh) * 2022-05-18 2026-04-03 中国石油化工股份有限公司 具有氧化萘功能的催化剂及其制备方法和应用
CN116474802B (zh) * 2023-05-09 2025-08-15 常州新日催化剂股份有限公司 一种钒基催化剂及其制备方法和在制备均酐中的应用
CN118792540B (zh) * 2024-06-03 2025-04-08 中国北方车辆研究所 一种复合改性的耐高温摩擦材料及其制备方法
CN120515429B (zh) * 2025-07-23 2025-10-03 国科大杭州高等研究院 一种催化净化氯代芳烃的电驱动催化剂及其制备方法与使用方法
CN120771857B (zh) * 2025-09-10 2025-11-18 国网安徽省电力有限公司电力科学研究院 一种钒掺杂二氧化钛复合材料的制备方法及其应用

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EP0522871A1 (de) * 1991-07-10 1993-01-13 Nippon Shokubai Co., Ltd. Katalysator und Verfahren zur Herstellung von Phtalsäureanhydrid
DE102004014918A1 (de) * 2004-03-26 2005-10-13 Basf Ag Katalysator mit einer Silber-Vanadiumoxidphase und einer Promotorphase
WO2009095216A2 (de) * 2008-02-01 2009-08-06 Josef Breimair Katalysator für die katalytische gasphasenoxidation von aromatischen kohlenwasserstoffen zu aldehyden, carbonsäuren und/oder carbonsäureanhydriden, insbesondere zu phthalsäureanhydrid

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