WO2017196286A2 - Procédé de fabrication de verre antireflet - Google Patents

Procédé de fabrication de verre antireflet Download PDF

Info

Publication number
WO2017196286A2
WO2017196286A2 PCT/TR2017/050186 TR2017050186W WO2017196286A2 WO 2017196286 A2 WO2017196286 A2 WO 2017196286A2 TR 2017050186 W TR2017050186 W TR 2017050186W WO 2017196286 A2 WO2017196286 A2 WO 2017196286A2
Authority
WO
WIPO (PCT)
Prior art keywords
glass
hydrofluoric acid
matted
production method
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/TR2017/050186
Other languages
English (en)
Other versions
WO2017196286A3 (fr
Inventor
Yavuz MERT
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CAM MERKEZI SANAYI VE TICARET AS
Original Assignee
CAM MERKEZI SANAYI VE TICARET AS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CAM MERKEZI SANAYI VE TICARET AS filed Critical CAM MERKEZI SANAYI VE TICARET AS
Publication of WO2017196286A2 publication Critical patent/WO2017196286A2/fr
Publication of WO2017196286A3 publication Critical patent/WO2017196286A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00—Methods for coating glass
    • C03C2218/30—Aspects of methods for coating glass not covered above
    • C03C2218/34—Masking

Definitions

  • This invention relates to the production method of an antiglare glass on screens which are found at the front of electronical visual systems such as LCD, display, tablets, smart board and commercial type refrigerators.
  • the glass surface is loosed into a fluorosilicic super saturated acid (3 millimoles per litre) until the intended etch depth is obtained and thereby the skeletonizing treatment for the glass is performed.
  • the fluorosilicic acid solution of the solution used can be made by adding filtered, water diluted and precipitated silicic acid or hydrated silicic (and this provides a super saturated solution to be formed since the solubility of the silica increases and the density of the fluoride acid decreases).
  • the glass before starting the process, can be cleaned with hydrofluoric acid or with superheated, and condensed sodium hydroxide material.
  • the solution can be prepared by dissolving the glass containing silica, in fluorosilicic acid. Nonetheless, a certain amount of supersaturation can be applied only to a section of the glass and the saturation can be decreased by adding sodium and potassium fluoride or increased by adding H3Bo3i, NaOH, sodium silicate.
  • the thickness of the glass washed with a detergent and water mixture and then cleaned with ethanol can be etched in the range of 200 nm to 300 nm and antiglare peaks on the surface in the range of 10 to 160 nm can be formed (These treatments take 4 to 30 hours and the temperatures of the glass and the vapour are different).
  • using the glasses obtained by the applications mentioned in these documents do not give the intended results. For this reason, in order to eliminate the reflection on the screens of electronical video devices, the need for a novel glass production technique to be performed has risen. Purpose and Brief Description of the Invention
  • the purpose of this invention is to perform a production method of the glass to be used on the screens of electronic video devices, which will prevent reflection.
  • Another aim of this invention is to perform a production method of the glass, including the application of a solution to a surface of the glass comprising hydrofluoric acid, , barium sulphate and ammonium bifluoride, then removing the solution from the glass surface and immersing the glass again in a pool containing hydrofluoric acid.
  • the glass produced by acid etching technique can be cut into intended dimensions and then the glass will be taken through the entire treatment processes.
  • Detailed Description of the Invention The glass production method and line of production performed in order to accomplish the purposes of this invention are shown in the accompanying drawings. These drawings illustrate the following;
  • Figure-1 is the flowchart of the glass production method.
  • Figure-2 is the schematic view of the matting line at the production line where the glass production method takes place.
  • Figure-3 is the schematic view of the embossing line at the production line where the glass production method takes place.
  • the glass production method of the invention comprises the steps of
  • the first stage of the method takes place in the matting line (1).
  • the flat glass enters the matting line (1).
  • the glass is first washed by tap water in the washing unit (3) by means of lower and upper brushes.
  • the glass is washed again in the purified water washing unit (4) with purified water by being passed between the lower and upper brushes and the surface of the glass is cleaned and dried by being passed through drying fans (6).
  • the purpose here is to prevent the chemical from affecting the lower surface of the glass.
  • the solution comprising hydrofluoric acid, barium sulphate and ammonium bifluoride is drained onto the surface of the flat glass covered with foil by a curtain system (5) automatically.
  • the glass moving on the conveyors with the chemicals finishes its journey on time periods varying according to the haze degree of the desired product and the chemical is removed from the top of the glass by having the glass passed through the mains water washing unit (3) and the purified water washing unit (4) again.
  • the glass passing through the drying fans (6) is dried and then the protective foil on the back surface of the glass is removed.
  • the first step of the method is completed.
  • the products exiting the matting line (1) are controlled at the quality control unit (10) and are directed to the embossing line (2). These treatments are performed via the glass loading robot.
  • the second phase of the process takes place in the embossing line (2).
  • the non- matted surface of the semi-finished glass from the matting line (1) is covered with protective foil at the entrance of the embossing line (2).
  • the glass enters the decoration pool (7) filled with hydrofluoric solution and travels for approximately 36 m by being advanced on the rollers.
  • the speed at which this travel is desired again varies depending on the desired product qualities.
  • the glass is initially inserted into the prewashing machine (8).
  • the purpose here is to clean the glass from the acid remaining on its surface.
  • the glass is washed with mains water, by means of the lower and upper brushes and then dried via the drying fans (6).
  • the next stage is removing the protective foil from the glass and this treatment is performed by a semi-automatic machine.
  • the main washing machine (9) is used at the last stage.
  • the glass having been washed a few progressive times, is passed through the drying fans (6) and it reaches the quality control unit (10). As a result, the antiglare glass production is completed.
  • This glass can then be cut into intended dimensions according to the customer's demand and this process takes place in the cutting unit (11).
  • the glass can be subjected to all kinds of treatment processes.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Surface Treatment Of Glass (AREA)
  • Devices For Indicating Variable Information By Combining Individual Elements (AREA)

Abstract

L'invention concerne le procédé de production d'un verre antireflet sur des écrans qui sont prévus à l'avant de systèmes d'affichage électroniques tels que des afficheurs à cristaux liquides, des afficheurs, des tablettes, des cartes à puce et des réfrigérateurs de type commercial. Selon l'invention, le procédé de production du verre consiste à : protéger la surface du verre qui ne sera pas matée de préférence en recouvrant avec une feuille ; appliquer une solution comprenant de l'acide fluorhydrique, du sulfate de baryum et du bifluorure d'ammonium à la surface du verre qui sera matée ; retirer la solution comprenant de l'acide fluorhydrique de la surface du verre ; sécher le verre après lavage ; recouvrir la surface du verre qui ne sera pas matée de préférence avec une feuille ; déposer le verre par immersion dans un bain contenant de l'acide fluorhydrique ; débarrasser le verre de l'acide fluorhydrique restant sur sa surface ; découper le verre aux dimensions souhaitées et soumettre le verre au processus de traitement.
PCT/TR2017/050186 2016-05-12 2017-05-11 Procédé de fabrication de verre antireflet Ceased WO2017196286A2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
TR2016/06320A TR201606320A2 (tr) 2016-05-12 2016-05-12 Yansimayi engelleyi̇ci̇ cam üreti̇m yöntemi̇
TR2016/06320 2016-05-12

Publications (2)

Publication Number Publication Date
WO2017196286A2 true WO2017196286A2 (fr) 2017-11-16
WO2017196286A3 WO2017196286A3 (fr) 2017-12-28

Family

ID=60267923

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/TR2017/050186 Ceased WO2017196286A2 (fr) 2016-05-12 2017-05-11 Procédé de fabrication de verre antireflet

Country Status (2)

Country Link
TR (1) TR201606320A2 (fr)
WO (1) WO2017196286A2 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111499213A (zh) * 2019-01-31 2020-08-07 比亚迪股份有限公司 渐变玻璃及其制备方法和应用
WO2020263197A1 (fr) * 2019-06-25 2020-12-30 Yorglass Cam Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇ Système et procédé de production d'un effet mat ou d'un verre mat

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB546366A (en) * 1940-04-26 1942-07-09 British Thomson Houston Co Ltd Improvements relating to the reduction of surface reflection
CN101142148A (zh) * 2005-02-18 2008-03-12 格拉沃贝尔公司 玻璃制品表面的选择性蚀刻方法
CN102923965A (zh) * 2012-11-28 2013-02-13 山东兴氟新材料有限公司 平置法生产蒙砂玻璃的方法
CN105565674A (zh) * 2015-12-19 2016-05-11 重庆天和玻璃有限公司 玻璃刻蚀方法

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111499213A (zh) * 2019-01-31 2020-08-07 比亚迪股份有限公司 渐变玻璃及其制备方法和应用
CN111499213B (zh) * 2019-01-31 2021-09-21 比亚迪股份有限公司 渐变玻璃及其制备方法和应用
WO2020263197A1 (fr) * 2019-06-25 2020-12-30 Yorglass Cam Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇ Système et procédé de production d'un effet mat ou d'un verre mat
EP3990409A4 (fr) * 2019-06-25 2022-08-03 Yorglass Cam Sanayi Ve Ticaret Anonim Sirketi Système et procédé de production d'un effet mat ou d'un verre mat
US20230109486A1 (en) * 2019-06-25 2023-04-06 Yorglass Cam Sanayi Ve Ticaret Anonim Sirketi A system and method of production of matt effect or matt glass
AU2019454975B2 (en) * 2019-06-25 2024-02-29 Yorglass Cam Sanayi Ve Ticaret Anonim Şirketi A system and method of production of matt effect or matt glass

Also Published As

Publication number Publication date
WO2017196286A3 (fr) 2017-12-28
TR201606320A2 (tr) 2017-01-23

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