ATE171394T1 - Katalytischer reaktor und verfahren zur durchführung von stark exothermen reaktionen - Google Patents
Katalytischer reaktor und verfahren zur durchführung von stark exothermen reaktionenInfo
- Publication number
- ATE171394T1 ATE171394T1 AT94309380T AT94309380T ATE171394T1 AT E171394 T1 ATE171394 T1 AT E171394T1 AT 94309380 T AT94309380 T AT 94309380T AT 94309380 T AT94309380 T AT 94309380T AT E171394 T1 ATE171394 T1 AT E171394T1
- Authority
- AT
- Austria
- Prior art keywords
- reaction
- carrying
- zone
- catalytic reactor
- exothermic reactions
- Prior art date
Links
- 238000006243 chemical reaction Methods 0.000 title abstract 7
- 230000003197 catalytic effect Effects 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 2
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 abstract 2
- 239000012295 chemical reaction liquid Substances 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 abstract 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 abstract 1
- 238000010926 purge Methods 0.000 abstract 1
- 239000011949 solid catalyst Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
- B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
- B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00265—Part of all of the reactants being heated or cooled outside the reactor while recycling
- B01J2208/00283—Part of all of the reactants being heated or cooled outside the reactor while recycling involving reactant liquids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Epoxy Compounds (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US17114493A | 1993-12-20 | 1993-12-20 | |
| US08/310,546 US5466836A (en) | 1993-12-20 | 1994-09-22 | Catalytic converter and method for highly exothermic reactions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE171394T1 true ATE171394T1 (de) | 1998-10-15 |
Family
ID=22622713
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT94309380T ATE171394T1 (de) | 1993-12-20 | 1994-12-15 | Katalytischer reaktor und verfahren zur durchführung von stark exothermen reaktionen |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5573736A (de) |
| EP (1) | EP0659473B1 (de) |
| JP (1) | JP3597895B2 (de) |
| CN (1) | CN1133630C (de) |
| AT (1) | ATE171394T1 (de) |
| CA (1) | CA2137310C (de) |
| DE (1) | DE69413507T2 (de) |
| ES (1) | ES2121162T3 (de) |
| RU (1) | RU2126799C1 (de) |
Families Citing this family (56)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5468885A (en) * | 1993-12-20 | 1995-11-21 | Arco Chemical Technology, L.P. | Epoxidizer oxygen recovery |
| US5840933A (en) * | 1996-10-29 | 1998-11-24 | Arco Chemical Technology, L.P. | Catalytic converter system and progress |
| US5760253A (en) * | 1997-01-29 | 1998-06-02 | Arco Chemical Technology, L.P. | Catalytic converter and method for highly exothermic reactions |
| WO1999025461A1 (fr) * | 1997-11-18 | 1999-05-27 | Asahi Kasei Kogyo Kabushiki Kaisha | Procede et dispositif de prevention contre le rechauffement general de la planete |
| US5849937A (en) * | 1997-12-19 | 1998-12-15 | Arco Chemical Technology, L.P. | Epoxidation process using serially connected cascade of fixed bed reactors |
| DE19835907A1 (de) * | 1998-08-07 | 2000-02-17 | Basf Ag | Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid |
| US7033553B2 (en) * | 2000-01-25 | 2006-04-25 | Meggitt (Uk) Limited | Chemical reactor |
| EP1122248A1 (de) | 2000-02-07 | 2001-08-08 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
| EP1122246A1 (de) * | 2000-02-07 | 2001-08-08 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
| EP1122247A1 (de) | 2000-02-07 | 2001-08-08 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
| FR2810983B1 (fr) * | 2000-06-28 | 2004-05-21 | Solvay | Procede de fabrication d'oxiranne au moyen d'un compose peroxyde |
| FR2810980B1 (fr) * | 2000-06-28 | 2004-05-21 | Solvay | Procede de fabrication d'oxiranne en presence d'un catalyseur sous forme de particules |
| EP1221442B1 (de) | 2001-01-08 | 2010-07-28 | Evonik Degussa GmbH | Verfahren zur Epoxidierung von Olefinen |
| EP1247805A1 (de) † | 2001-03-05 | 2002-10-09 | Degussa AG | Verfahren zur epoxidierung von olefinen |
| EP1247806A1 (de) * | 2001-03-05 | 2002-10-09 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
| EP1258483A1 (de) * | 2001-03-05 | 2002-11-20 | Degussa AG | Verfahren zur epoxidierung von olefinen |
| US6608219B2 (en) | 2001-06-13 | 2003-08-19 | Degussa Ag | Process for the epoxidation of olefins |
| US6596881B2 (en) | 2001-06-13 | 2003-07-22 | Degussa Ag | Process for the epoxidation of olefins |
| US6600055B2 (en) | 2001-06-13 | 2003-07-29 | Degussa Ag | Process for the epoxidation of olefins |
| US6749668B2 (en) | 2001-06-18 | 2004-06-15 | Degussa Ag | Process for the recovery of combustible components of a gas stream |
| US6532741B2 (en) | 2001-06-29 | 2003-03-18 | United Technologies Corporation | Gas generator for producing adjustable flow |
| US6652248B2 (en) | 2001-06-29 | 2003-11-25 | United Technologies Corporation | Catalyst bed |
| EP1285915A1 (de) * | 2001-08-16 | 2003-02-26 | Degussa AG | Kontinuierliches Verfahren zur Herstellung von Epoxiden aus Olefinen und Wasserstoffperoxid |
| US6610865B2 (en) | 2001-08-15 | 2003-08-26 | Degussa Ag | Process for the epoxidation of olefins |
| US6596883B2 (en) | 2001-08-23 | 2003-07-22 | Degussa Ag | Process for the epoxidation of olefins |
| AU2002366573A1 (en) * | 2001-12-05 | 2003-06-23 | Dow Global Technologies Inc. | Process of preparing an olefin oxide from olefin and organic hydroperoxide |
| US6720436B2 (en) | 2002-03-18 | 2004-04-13 | Degussa Ag | Process for the epoxidation of olefins |
| EP1359148A1 (de) * | 2002-05-02 | 2003-11-05 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
| US7141683B2 (en) | 2002-05-02 | 2006-11-28 | Degussa Ag | Process for the epoxidation of olefins |
| US6838572B2 (en) | 2002-09-30 | 2005-01-04 | Degussa Ag | Process for the epoxidation of olefins |
| US7722847B2 (en) | 2002-09-30 | 2010-05-25 | Evonik Degussa Gmbh | Aqueous hydrogen peroxide solutions and method of making same |
| EP1403259A1 (de) * | 2002-09-30 | 2004-03-31 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
| US7169945B2 (en) | 2002-11-26 | 2007-01-30 | Degussa Ag | Process for the epoxidation of olefins |
| DE10317520A1 (de) * | 2003-04-16 | 2004-11-04 | Basf Ag | Verfahren zur Herstellung eines Alkenoxids |
| DE102004059191B4 (de) * | 2004-12-09 | 2010-07-01 | Evonik Degussa Gmbh | Vorrichtung und Verfahren zur Herstellung von Chlorsilanen |
| US20070004926A1 (en) * | 2005-06-29 | 2007-01-04 | Basf Aktiengesellschaft | Process for producing propylene oxide |
| KR101485955B1 (ko) * | 2007-05-11 | 2015-01-22 | 베리 제이. 빌릭 | 산화올레핀 제조 공장에서의 고선택성 촉매의 개시 방법 |
| JP2009035544A (ja) * | 2007-07-11 | 2009-02-19 | Sumitomo Chemical Co Ltd | エポキシ化合物の製造装置および製造方法 |
| BRPI0814211A2 (pt) * | 2007-07-11 | 2015-01-27 | Sumitomo Chemical Co | Método e aparelho para produção de gás misturado, e aparelho e método para produção de composto époxi. |
| ES2436625T3 (es) * | 2009-05-12 | 2014-01-03 | Basf Se | Proceso para producir óxido de propileno |
| CN101885711B (zh) * | 2009-05-13 | 2012-09-05 | 中国石油化工股份有限公司 | 环氧丙烷的生产方法 |
| CN101941955B (zh) * | 2009-07-06 | 2012-09-05 | 中国石油化工股份有限公司 | 由过氧化氢和丙烯生产环氧丙烷的方法 |
| CN101941954B (zh) * | 2009-07-06 | 2012-09-05 | 中国石油化工股份有限公司 | 由过氧化氢和丙烯制备环氧丙烷的方法 |
| GB201102551D0 (en) | 2011-02-14 | 2011-03-30 | Davy Process Techn Ltd | Reactor |
| RU2472786C1 (ru) * | 2011-05-13 | 2013-01-20 | Закрытое акционерное общество "Химтэк Инжиниринг" | Способ получения оксида пропилена |
| HUE046136T2 (hu) | 2015-11-25 | 2020-02-28 | Evonik Operations Gmbh | Eljárás 1,2-propándiol elõállítására propénból és hidrogén-peroxidból |
| TWI707847B (zh) | 2015-11-26 | 2020-10-21 | 德商贏創運營有限公司 | 丙烯之環氧化方法 |
| ES2873407T3 (es) * | 2015-11-26 | 2021-11-03 | Evonik Operations Gmbh | Procedimiento y reactor para la epoxidación de propeno |
| PL3380459T3 (pl) | 2015-11-26 | 2020-06-01 | Evonik Operations Gmbh | Sposób epoksydowania olefiny |
| CN108473453B (zh) | 2016-01-19 | 2020-08-04 | 赢创运营有限公司 | 烯烃的环氧化方法 |
| HUE052019T2 (hu) | 2016-03-21 | 2021-04-28 | Evonik Operations Gmbh | Eljárás propén epoxidálására |
| EP3246323A1 (de) | 2016-05-17 | 2017-11-22 | Evonik Degussa GmbH | Integrierter prozess zur herststellung von propenoxid aus propan |
| EP3406603A1 (de) | 2017-05-22 | 2018-11-28 | Evonik Degussa GmbH | Verfahren zur epoxidierung von propen |
| CN108043331A (zh) * | 2017-12-21 | 2018-05-18 | 红宝丽集团股份有限公司 | 一种用于1,2-环氧丁烷制备的多段反应装置及1,2-环氧丁烷的制备方法 |
| EP4332233A1 (de) | 2022-09-05 | 2024-03-06 | Syensqo Sa | Lösungsmittelfreie enzymatische epoxidierung von olefinen |
| CN119841791A (zh) * | 2025-03-18 | 2025-04-18 | 中国天辰工程有限公司 | 一种过氧化氢直接氧化法生产环氧丙烷的方法 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2271646A (en) * | 1939-05-17 | 1942-02-03 | Universal Oil Prod Co | Control of contact catalytic reactions |
| US2322366A (en) * | 1939-11-29 | 1943-06-22 | Universal Oil Prod Co | Hydrocarbon conversion process |
| US2938040A (en) * | 1957-09-09 | 1960-05-24 | Shell Oil Co | Epoxidation of unsaturated aldehydes |
| FR1506459A (fr) * | 1966-11-02 | 1967-12-22 | Naphtachimie Sa | Procédé de préparation d'époxydes et produits préparés selon ce procédé |
| US3728249A (en) * | 1971-02-05 | 1973-04-17 | Exxon Research Engineering Co | Selective hydrotreating of different hydrocarbonaceous feedstocks in temperature regulated hydrotreating zones |
| US3976713A (en) * | 1971-06-11 | 1976-08-24 | Sun Oil Company Of Pennsylvania | Isoparaffin-olefin alkylation utilizing recycle streams and multiple packed catalyst beds |
| DE2519297B2 (de) * | 1975-04-30 | 1981-05-14 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen Herstellung von Propylenoxid |
| AU526654B2 (en) * | 1977-08-29 | 1983-01-27 | Uop Inc. | Multi-st. ge catalytic hydroforming with gravity flowing catalysts |
| IT1152299B (it) * | 1982-07-28 | 1986-12-31 | Anic Spa | Procedimento per l'espossidazione di composti olefinici |
| US4550012A (en) * | 1984-05-01 | 1985-10-29 | Mobil Oil Corp. | Multi-phase countercurrent reactor system |
| US4937051A (en) * | 1985-11-07 | 1990-06-26 | Mobil Oil Corporation | Catalytic reactor with liquid recycle |
| ES2033693T3 (es) * | 1986-01-28 | 1993-04-01 | Eniricerche S.P.A. | Un procedimiento para la exposidacion de compuestos olefinicos. |
| DE3880877T2 (de) * | 1987-02-26 | 1993-09-23 | Ammonia Casale Sa | System zur verbesserung der reaktorausbeute fuer exotherme synthese, insbesondere fuer die ammoniakreaktion. |
| EP0297474B1 (de) * | 1987-07-03 | 1992-04-01 | Ammonia Casale S.A. | Heterogen-Syntheseverfahren und verwandte Reaktoren |
| JPH01132573A (ja) * | 1987-11-18 | 1989-05-25 | Mitsui Toatsu Chem Inc | プロピレンオキサイドの製造方法 |
| EP0355303B2 (de) * | 1988-06-27 | 1995-12-20 | Ammonia Casale S.A. | Reaktor für die exotherme heterogene Synthese mit Hilfe verschiedener katalytischer Betten und mit externer Rückgewinnung der Reaktionswärme |
| US5214168A (en) * | 1992-04-30 | 1993-05-25 | Arco Chemical Technology, L.P. | Integrated process for epoxide production |
| JPH1132573A (ja) * | 1997-07-17 | 1999-02-09 | Nippon Chem Ind Co Ltd | 植物栽培基盤用充填材及びその充填方法 |
-
1994
- 1994-12-05 CA CA002137310A patent/CA2137310C/en not_active Expired - Fee Related
- 1994-12-09 JP JP33099994A patent/JP3597895B2/ja not_active Expired - Fee Related
- 1994-12-14 RU RU94043783/25A patent/RU2126799C1/ru not_active IP Right Cessation
- 1994-12-15 CN CNB941190927A patent/CN1133630C/zh not_active Expired - Fee Related
- 1994-12-15 ES ES94309380T patent/ES2121162T3/es not_active Expired - Lifetime
- 1994-12-15 EP EP94309380A patent/EP0659473B1/de not_active Expired - Lifetime
- 1994-12-15 DE DE69413507T patent/DE69413507T2/de not_active Expired - Fee Related
- 1994-12-15 AT AT94309380T patent/ATE171394T1/de not_active IP Right Cessation
-
1995
- 1995-06-29 US US08/496,702 patent/US5573736A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JP3597895B2 (ja) | 2004-12-08 |
| JPH07196639A (ja) | 1995-08-01 |
| CN1109382A (zh) | 1995-10-04 |
| RU2126799C1 (ru) | 1999-02-27 |
| DE69413507T2 (de) | 1999-02-11 |
| DE69413507D1 (de) | 1998-10-29 |
| ES2121162T3 (es) | 1998-11-16 |
| EP0659473B1 (de) | 1998-09-23 |
| EP0659473A1 (de) | 1995-06-28 |
| US5573736A (en) | 1996-11-12 |
| RU94043783A (ru) | 1996-12-20 |
| CN1133630C (zh) | 2004-01-07 |
| CA2137310A1 (en) | 1995-06-21 |
| CA2137310C (en) | 2004-02-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| REN | Ceased due to non-payment of the annual fee |