ATE228109T1 - Verfahren zur raffination von butylacrylat - Google Patents

Verfahren zur raffination von butylacrylat

Info

Publication number: ATE228109T1
Authority: AT; Austria
Prior art keywords: butyl acrylate; butyl; bottoms; butanol; heavies
Prior art date: 1997-05-20

Application number

AT97925718T

Other languages

English (en)

Inventor

Fungau Ho

Vivek Julka

Original Assignee

Union Carbide Chem Plastic

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1997-05-20

Filing date

1997-05-27

Publication date

2002-12-15

1997-05-20 Priority claimed from US08/859,143 external-priority patent/US6605738B1/en

1997-05-27 Application filed by Union Carbide Chem Plastic filed Critical Union Carbide Chem Plastic

2002-12-15 Application granted granted Critical

2002-12-15 Publication of ATE228109T1 publication Critical patent/ATE228109T1/de

Links

CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 title abstract 10
238000000034 method Methods 0.000 title abstract 3
238000007670 refining Methods 0.000 title abstract 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 abstract 6
238000004821 distillation Methods 0.000 abstract 3
DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 abstract 2
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 abstract 2
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 abstract 2
DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 abstract 2
FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 abstract 2
238000004519 manufacturing process Methods 0.000 abstract 2
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 abstract 1
238000000926 separation method Methods 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Crystallography & Structural Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Manufacture And Refinement Of Metals (AREA)

AT97925718T 1997-05-20 1997-05-27 Verfahren zur raffination von butylacrylat ATE228109T1 (de)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US08/859,143 US6605738B1 (en)	1996-05-29	1997-05-20	Processes for refining butyl acrylate
PCT/US1997/008814 WO1998052904A1 (en)	1997-05-20	1997-05-27	Processes for refining butylacrylate

Publications (1)

Publication Number	Publication Date
ATE228109T1 true ATE228109T1 (de)	2002-12-15

Family

ID=25330156

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT97925718T ATE228109T1 (de)	1997-05-20	1997-05-27	Verfahren zur raffination von butylacrylat

Country Status (8)

Country	Link
EP (1)	EP0984918B1 (de)
JP (1)	JP3934163B2 (de)
KR (1)	KR100462266B1 (de)
CN (1)	CN1099405C (de)
AT (1)	ATE228109T1 (de)
BR (1)	BR9714713A (de)
DE (1)	DE69717314T2 (de)
WO (1)	WO1998052904A1 (de)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP1028109A1 (de) *	1999-02-12	2000-08-16	Dsm N.V.	Verfahren zur Herstellung von Epsilon-Caprolactam
AU5605400A (en) *	1999-06-17	2001-01-09	Union Carbide Chemicals And Plastics Company Inc.	Processes for conducting equilibrium-limited reactions
US6482976B1 (en)	1999-06-17	2002-11-19	Union Carbide Chemicals & Plastics Technology Corporation	Processes for conducting equilibrium-limited reactions
US6180820B1 (en) *	1999-09-14	2001-01-30	Celanese International Corporation	Process for the production and purification of N-butyl acrylate
US6172258B1 (en) *	1999-09-14	2001-01-09	Celanese International Corporation	Process for the production and purification of n-butyl acrylate
JP2001181233A (ja) *	1999-10-12	2001-07-03	Nippon Shokubai Co Ltd	（メタ）アクリル酸エステルの製造方法
US6649787B1 (en)	1999-10-12	2003-11-18	Nippon Shokubai Co., Ltd.	Method for preparing (meth) acrylic acid ester
WO2001085666A2 (en) *	2000-05-09	2001-11-15	Union Carbide Chemicals & Plastics Technology Corporation	Improved refining processes
WO2004078679A2 (en)	2003-02-28	2004-09-16	Union Carbide Chemicals & Plastics Technology Corporation	Process for conducting equilibrium-limited reactions
JP2008266159A (ja) *	2007-04-17	2008-11-06	Mitsubishi Chemicals Corp	アクリル酸ブチルの精製方法
ATE519728T1 (de) *	2008-01-18	2011-08-15	Arkema Inc	Verfahren zur rückgewinnung eines sulfonsäurekatalysators und wertprodukten aus acrylatnachlauffraktionen
JP5169899B2 (ja) *	2009-02-19	2013-03-27	東亞合成株式会社	アクリル酸アルキルエステルの製造方法
KR101144306B1 (ko) *	2010-08-26	2012-05-11	주식회사 엘지화학	알킬(메트)아크릴레이트의 제조 방법
FR3008971B1 (fr) *	2013-07-29	2016-08-19	Arkema France	Procede de production en continu d'acrylates legers par esterification d'un acide acrylique de grade ester brut
FR3014870B1 (fr) *	2013-12-13	2015-12-11	Arkema France	Procede de production d'esters (meth)acryliques
JP6287269B2 (ja) *	2014-01-30	2018-03-07	三菱ケミカル株式会社	アクリル酸ブチルの製造方法
WO2016083506A1 (en)	2014-11-28	2016-06-02	Siemens Vai Metals Technologies Gmbh	Method for casting metal strip with crown control
CN107428860B (zh) *	2015-02-27	2020-09-01	株式会社可乐丽	(甲基)丙烯酸类树脂组合物的制造方法
CN104844456B (zh) *	2015-04-17	2017-06-13	江苏新东风化工科技有限公司	一种丙烯酸正丁酯废油回收工艺及装置
CN110937997A (zh) *	2019-12-09	2020-03-31	东营海德新材料有限公司	一种提高丙烯酸丁酯纯度的生产工艺
CN113121348A (zh) *	2021-03-15	2021-07-16	江苏新东风化工科技有限公司	一种丙烯酸正丁酯生产脱醚工艺
US20250074859A1 (en)	2021-07-29	2025-03-06	Basf Se	Process for the continuous distillation of acrylates
FR3126416B1 (fr) *	2021-08-25	2023-07-14	Arkema France	Procede perfectionne de fabrication d’acrylate de butyle de purete elevee
KR20240113809A (ko) *	2021-11-25	2024-07-23	바스프 에스이	C6-c12-알킬 (메트)아크릴산 에스터의 제조 방법

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2449811C2 (de) *	1974-10-19	1983-01-05	Hoechst Ag, 6000 Frankfurt	Verfahren zur kontinuierlichen Herstellung von dibutylätherfreiem n-Butylacrylat
DE2552987C2 (de) *	1975-11-26	1983-09-29	Hoechst Ag, 6230 Frankfurt	Verfahren zur kontinuierlichen Herstellung ätherfreier Acrylsäurealkylester
JPS5877845A (ja) *	1981-11-02	1983-05-11	Nippon Shokubai Kagaku Kogyo Co Ltd	アクリル酸エステルまたはメタクリル酸エステルの製造方法
US4814493A (en) *	1983-07-05	1989-03-21	Hoechst Celanese Corporation	Process for production of alkyl acrylates
JPH089567B2 (ja) *	1992-01-09	1996-01-31	株式会社日本触媒	アクリル酸製造においてアクリル酸を高純度に精製する方法
FR2723089B1 (fr) *	1994-07-28	1996-09-06	Atochem Elf Sa	Procede de fabrication de l'acrylate de butyle par esterification directe
DE19536178A1 (de) *	1995-09-28	1997-04-03	Basf Ag	Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure

1997
- 1997-05-27 JP JP55031698A patent/JP3934163B2/ja not_active Expired - Lifetime
- 1997-05-27 KR KR10-1999-7010423A patent/KR100462266B1/ko not_active Expired - Lifetime
- 1997-05-27 CN CN97182208A patent/CN1099405C/zh not_active Expired - Lifetime
- 1997-05-27 WO PCT/US1997/008814 patent/WO1998052904A1/en not_active Ceased
- 1997-05-27 EP EP97925718A patent/EP0984918B1/de not_active Expired - Lifetime
- 1997-05-27 BR BR9714713-3A patent/BR9714713A/pt not_active IP Right Cessation
- 1997-05-27 DE DE69717314T patent/DE69717314T2/de not_active Expired - Lifetime
- 1997-05-27 AT AT97925718T patent/ATE228109T1/de not_active IP Right Cessation

Also Published As

Publication number	Publication date
BR9714713A (pt)	2000-07-04
WO1998052904A1 (en)	1998-11-26
KR100462266B1 (ko)	2004-12-17
EP0984918A1 (de)	2000-03-15
CN1099405C (zh)	2003-01-22
DE69717314T2 (de)	2003-08-21
CN1254331A (zh)	2000-05-24
EP0984918B1 (de)	2002-11-20
DE69717314D1 (de)	2003-01-02
KR20010012468A (ko)	2001-02-15
JP2002507194A (ja)	2002-03-05
JP3934163B2 (ja)	2007-06-20

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Legal Events

Date	Code	Title	Description
2003-05-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties