ATE258158T1 - Verfahren zum reinigen von milchsäureestern - Google Patents
Verfahren zum reinigen von milchsäureesternInfo
- Publication number
- ATE258158T1 ATE258158T1 AT00989027T AT00989027T ATE258158T1 AT E258158 T1 ATE258158 T1 AT E258158T1 AT 00989027 T AT00989027 T AT 00989027T AT 00989027 T AT00989027 T AT 00989027T AT E258158 T1 ATE258158 T1 AT E258158T1
- Authority
- AT
- Austria
- Prior art keywords
- lactic acid
- acid esters
- sub
- ester
- purifying lactic
- Prior art date
Links
- 150000003903 lactic acid esters Chemical class 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 abstract 4
- 150000002148 esters Chemical class 0.000 abstract 2
- 235000014655 lactic acid Nutrition 0.000 abstract 2
- 239000004310 lactic acid Substances 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000000155 melt Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL1013870A NL1013870C2 (nl) | 1999-12-16 | 1999-12-16 | Werkwijze voor het zuiveren van melkzure esters. |
| PCT/NL2000/000860 WO2001044157A1 (en) | 1999-12-16 | 2000-11-24 | Method of purifying lactic acid esters |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE258158T1 true ATE258158T1 (de) | 2004-02-15 |
Family
ID=19770449
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT00989027T ATE258158T1 (de) | 1999-12-16 | 2000-11-24 | Verfahren zum reinigen von milchsäureestern |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US6967257B1 (de) |
| EP (1) | EP1237841B1 (de) |
| JP (1) | JP5065563B2 (de) |
| CN (1) | CN1184188C (de) |
| AT (1) | ATE258158T1 (de) |
| AU (1) | AU2557101A (de) |
| BR (1) | BR0016429B1 (de) |
| DE (1) | DE60007895T2 (de) |
| DK (1) | DK1237841T3 (de) |
| ES (1) | ES2211661T3 (de) |
| NL (1) | NL1013870C2 (de) |
| PT (1) | PT1237841E (de) |
| WO (1) | WO2001044157A1 (de) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5000814B2 (ja) * | 2001-06-05 | 2012-08-15 | 東邦化学工業株式会社 | 乳酸エチル中の不純物の除去方法 |
| BE1019021A3 (fr) * | 2009-07-01 | 2012-01-10 | Galactic Sa | Procede de preparation de lactate d'alkyle c1-c4 de grande purete par putrification des lactates d'alkyle c1-c4 bruts. |
| BE1019857A3 (fr) * | 2011-03-03 | 2013-01-08 | Galactic Sa | Procede de separation des deux isomeres de l'acide lactique et utilisation des isomeres ainsi recuperes. |
| NL2028900B1 (en) | 2021-08-02 | 2023-02-17 | Arapaha B V | A method of closed loop recycling of polylactic acid |
| CN115436511A (zh) * | 2022-08-31 | 2022-12-06 | 汉瑞药业(荆门)有限公司 | 一种乳酸乙酯及其对映异构体手性纯度的hplc检测方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3433400A1 (de) * | 1984-09-12 | 1986-03-20 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von milchsaeureestern |
| JPS6226249A (ja) * | 1985-07-26 | 1987-02-04 | Daicel Chem Ind Ltd | 光学活性乳酸エステルの精製方法 |
| US5264592A (en) * | 1992-09-08 | 1993-11-23 | Camelot Technologies Inc. | Lactide melt recrystallization |
| CA2115472C (en) * | 1993-02-17 | 2002-08-13 | William George O'brien | Melt crystallization purification of lactides |
| JPH0940663A (ja) * | 1995-08-01 | 1997-02-10 | Toyobo Co Ltd | α−オキシ酸の分子間環状ジエステルの精製方法 |
| JP4105797B2 (ja) * | 1998-05-11 | 2008-06-25 | 三菱レイヨン株式会社 | 光学活性α−トリフルオロメチル乳酸の精製方法 |
-
1999
- 1999-12-16 NL NL1013870A patent/NL1013870C2/nl not_active IP Right Cessation
-
2000
- 2000-11-24 WO PCT/NL2000/000860 patent/WO2001044157A1/en not_active Ceased
- 2000-11-24 US US10/149,652 patent/US6967257B1/en not_active Expired - Lifetime
- 2000-11-24 DK DK00989027T patent/DK1237841T3/da active
- 2000-11-24 EP EP00989027A patent/EP1237841B1/de not_active Expired - Lifetime
- 2000-11-24 BR BRPI0016429-1A patent/BR0016429B1/pt not_active IP Right Cessation
- 2000-11-24 ES ES00989027T patent/ES2211661T3/es not_active Expired - Lifetime
- 2000-11-24 DE DE60007895T patent/DE60007895T2/de not_active Expired - Lifetime
- 2000-11-24 JP JP2001545246A patent/JP5065563B2/ja not_active Expired - Fee Related
- 2000-11-24 PT PT00989027T patent/PT1237841E/pt unknown
- 2000-11-24 AU AU25571/01A patent/AU2557101A/en not_active Abandoned
- 2000-11-24 AT AT00989027T patent/ATE258158T1/de not_active IP Right Cessation
- 2000-11-24 CN CNB008172900A patent/CN1184188C/zh not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| CN1411433A (zh) | 2003-04-16 |
| EP1237841B1 (de) | 2004-01-21 |
| JP2003517031A (ja) | 2003-05-20 |
| NL1013870C2 (nl) | 2001-06-21 |
| DE60007895D1 (de) | 2004-02-26 |
| AU2557101A (en) | 2001-06-25 |
| PT1237841E (pt) | 2004-04-30 |
| DK1237841T3 (da) | 2004-02-23 |
| JP5065563B2 (ja) | 2012-11-07 |
| EP1237841A1 (de) | 2002-09-11 |
| DE60007895T2 (de) | 2004-06-09 |
| US6967257B1 (en) | 2005-11-22 |
| ES2211661T3 (es) | 2004-07-16 |
| BR0016429A (pt) | 2002-08-20 |
| WO2001044157A1 (en) | 2001-06-21 |
| CN1184188C (zh) | 2005-01-12 |
| BR0016429B1 (pt) | 2010-08-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |