ATE282006T1 - Verfahren zur herstellung von hydrophober kolloidaler kieselsäure - Google Patents
Verfahren zur herstellung von hydrophober kolloidaler kieselsäureInfo
- Publication number
- ATE282006T1 ATE282006T1 AT01908439T AT01908439T ATE282006T1 AT E282006 T1 ATE282006 T1 AT E282006T1 AT 01908439 T AT01908439 T AT 01908439T AT 01908439 T AT01908439 T AT 01908439T AT E282006 T1 ATE282006 T1 AT E282006T1
- Authority
- AT
- Austria
- Prior art keywords
- organic solvent
- colloidal silica
- hydrophobic
- new method
- organic
- Prior art date
Links
- 230000002209 hydrophobic effect Effects 0.000 title abstract 6
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 title 1
- 235000012239 silicon dioxide Nutrition 0.000 title 1
- 239000003960 organic solvent Substances 0.000 abstract 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 5
- 239000008119 colloidal silica Substances 0.000 abstract 5
- 239000002270 dispersing agent Substances 0.000 abstract 2
- 239000011347 resin Substances 0.000 abstract 2
- 229920005989 resin Polymers 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 229910021645 metal ion Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000003973 paint Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/141—Preparation of hydrosols or aqueous dispersions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
- C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/145—Preparation of hydroorganosols, organosols or dispersions in an organic medium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/146—After-treatment of sols
- C01B33/149—Coating
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3081—Treatment with organo-silicon compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
- C01P2006/82—Compositional purity water content
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/90—Other properties not specified above
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Silicon Compounds (AREA)
- Colloid Chemistry (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2000024767A JP4631119B2 (ja) | 2000-01-28 | 2000-01-28 | 疎水化コロイダルシリカの製造方法 |
| PCT/NL2001/000063 WO2001055030A2 (en) | 2000-01-28 | 2001-01-29 | Method for manufacturing hydrophobic colloidal silica |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE282006T1 true ATE282006T1 (de) | 2004-11-15 |
Family
ID=18550707
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT01908439T ATE282006T1 (de) | 2000-01-28 | 2001-01-29 | Verfahren zur herstellung von hydrophober kolloidaler kieselsäure |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US20030035888A1 (de) |
| EP (1) | EP1252095B1 (de) |
| JP (1) | JP4631119B2 (de) |
| KR (1) | KR100716853B1 (de) |
| CN (1) | CN1220627C (de) |
| AT (1) | ATE282006T1 (de) |
| AU (1) | AU2001236182A1 (de) |
| DE (1) | DE60107049T2 (de) |
| TW (1) | TW524772B (de) |
| WO (1) | WO2001055030A2 (de) |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4458396B2 (ja) * | 2002-08-29 | 2010-04-28 | 扶桑化学工業株式会社 | 高純度親水性有機溶媒分散シリカゾルの製造方法及びその方法で得られる高純度親水性有機溶媒分散シリカゾル並びに高純度有機溶媒分散シリカゾルの製造方法及びその方法で得られる高純度有機溶媒分散シリカゾル |
| JP4803630B2 (ja) * | 2003-05-21 | 2011-10-26 | 扶桑化学工業株式会社 | 高純度疎水性有機溶媒分散シリカゾルの製造方法 |
| JP5128044B2 (ja) * | 2003-12-10 | 2013-01-23 | 東京応化工業株式会社 | シリコン基板又は金属配線パターンが設けられたシリコン基板被覆用シリカ系被膜形成用材料の製造方法 |
| JP4816861B2 (ja) * | 2003-12-19 | 2011-11-16 | 日産化学工業株式会社 | 有機溶媒分散無機酸化物ゾルの製造方法 |
| US7737187B2 (en) | 2003-12-19 | 2010-06-15 | Nissan Chemical Industries, Ltd. | Process for producing inorganic oxide organosol |
| KR100680680B1 (ko) * | 2003-12-23 | 2007-02-08 | 삼성코닝 주식회사 | 실리카 졸 및 그 제조 방법 |
| KR100572801B1 (ko) * | 2003-12-23 | 2006-04-19 | 삼성코닝 주식회사 | 기계적 특성이 우수한 절연막 코팅 조성물 |
| US20110094418A1 (en) * | 2004-06-15 | 2011-04-28 | David Monroe Chapman | Chemically assisted milling of silicas |
| US20060283095A1 (en) * | 2005-06-15 | 2006-12-21 | Planar Solutions, Llc | Fumed silica to colloidal silica conversion process |
| MX2008000101A (es) | 2005-06-21 | 2008-03-19 | Akzo Nobel Nv | Procedimiento para la modificacion de material particulado que contiene oxigeno inorganico producto obtenido a partir de este y su uso. |
| US7186440B2 (en) * | 2005-07-04 | 2007-03-06 | Nissan Chemical Industries, Ltd. | Process for producing hydrophobic silica powder |
| US8435474B2 (en) * | 2006-09-15 | 2013-05-07 | Cabot Corporation | Surface-treated metal oxide particles |
| US8202502B2 (en) * | 2006-09-15 | 2012-06-19 | Cabot Corporation | Method of preparing hydrophobic silica |
| US20080070146A1 (en) * | 2006-09-15 | 2008-03-20 | Cabot Corporation | Hydrophobic-treated metal oxide |
| US8455165B2 (en) * | 2006-09-15 | 2013-06-04 | Cabot Corporation | Cyclic-treated metal oxide |
| EP2064291B1 (de) | 2006-09-18 | 2017-02-22 | Dow Corning Corporation | Mit organopolysiloxanen behandelte füllstoffe, pigmente und mineralpulver |
| IL188647A0 (en) * | 2008-01-08 | 2008-11-03 | Orina Gribova | Adaptable structured drug and supplements administration system (for oral and/or transdermal applications) |
| CN100575256C (zh) * | 2008-03-07 | 2009-12-30 | 南京工业大学 | 一种超疏水二氧化硅的制备方法 |
| WO2009152301A2 (en) * | 2008-06-12 | 2009-12-17 | 3M Innovative Properties Company | Low ion content, nanoparticle-containing resin systems |
| WO2011004376A1 (en) | 2009-07-09 | 2011-01-13 | Oshadi Drug Administration Ltd. | Matrix carrier compositions, methods and uses |
| DE102010043721A1 (de) * | 2010-11-10 | 2012-05-10 | Evonik Degussa Gmbh | Hydrophobierte Siliciumdioxidpartikel enthaltende Dispersion und Lackzubereitung |
| JP5906635B2 (ja) * | 2011-09-26 | 2016-04-20 | 富士ゼロックス株式会社 | シリカ粒子分散液の製造方法 |
| CN103101916B (zh) * | 2013-03-06 | 2015-05-20 | 山东百特新材料有限公司 | 一种醇分散硅溶胶的制备方法 |
| CN106414328B (zh) * | 2014-06-03 | 2019-01-22 | Az电子材料(卢森堡)有限公司 | 表面改性二氧化硅纳米颗粒的制造方法以及表面改性二氧化硅纳米颗粒 |
| CN104891826B (zh) * | 2015-05-26 | 2018-02-16 | 奇瑞汽车股份有限公司 | 一种车辆用疏水玻璃及其制备方法 |
| WO2018186468A1 (ja) * | 2017-04-06 | 2018-10-11 | 株式会社日本触媒 | シリカ粒子 |
| WO2019050008A1 (ja) | 2017-09-07 | 2019-03-14 | 日産化学株式会社 | シリカ含有絶縁性組成物 |
| WO2019129605A1 (en) | 2017-12-27 | 2019-07-04 | Rhodia Operations | Silica suspensions |
| US11987501B2 (en) * | 2018-01-25 | 2024-05-21 | Cabot Corporation | Aqueous hydrophobic silica dispersions |
| CN108516557B (zh) * | 2018-05-23 | 2019-03-19 | 东莞理工学院 | 一种用渗透气化膜分离装置制备疏水二氧化硅气凝胶的方法 |
| WO2019241498A1 (en) | 2018-06-15 | 2019-12-19 | W. R. Grace & Co.-Conn | Defoamer active, manufacturing method thereof, and defoaming formuation |
| WO2020230823A1 (ja) * | 2019-05-14 | 2020-11-19 | 日産化学株式会社 | ケトン系溶媒分散シリカゾル及び樹脂組成物 |
| EP4067456A4 (de) * | 2019-11-28 | 2023-12-06 | INPEX Corporation | Kieselsäurenanopartikel zur gewinnung von rohölen unter verwendung von kohlendioxid und verfahren zur gewinnung von rohöl |
| CN115974087A (zh) * | 2022-12-13 | 2023-04-18 | 江苏辉迈粉体科技有限公司 | 一种高纯纳米球形二氧化硅的制备方法 |
| CN121226966A (zh) * | 2023-01-06 | 2025-12-30 | 日产化学株式会社 | 无溶剂系有机无机杂化树脂组合物和固化膜 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58110416A (ja) * | 1981-12-18 | 1983-07-01 | Asahi Denka Kogyo Kk | シリカゾルの製造方法 |
| JPS58145614A (ja) * | 1982-02-23 | 1983-08-30 | Shokubai Kasei Kogyo Kk | 有機溶剤に均質に分散可能な粉末状シリカとその製造法 |
| JPS598614A (ja) * | 1982-06-30 | 1984-01-17 | Shokubai Kasei Kogyo Kk | 有機溶剤を分散媒とするシリカゾルの製造方法 |
| JP2638170B2 (ja) * | 1988-12-21 | 1997-08-06 | イー・アイ・デュポン・ドゥ・ヌムール・アンド・カンパニー | コロイダルシリカメタノールゾルの製造方法 |
| US5013585A (en) * | 1989-06-13 | 1991-05-07 | Shin-Etsu Chemical Co., Ltd. | Method for the preparation of surface-modified silica particles |
| ATE113930T1 (de) * | 1990-07-02 | 1994-11-15 | Nalco Chemical Co | Herstellung von kieselsäuresolen. |
| JP2646150B2 (ja) * | 1990-08-27 | 1997-08-25 | 出光興産 株式会社 | 撥水性シリカゾルおよびその製造方法 |
| JPH05170423A (ja) * | 1991-12-24 | 1993-07-09 | Ngk Insulators Ltd | コロイダルシリカの濃縮方法 |
| JP3235864B2 (ja) * | 1992-03-28 | 2001-12-04 | 触媒化成工業株式会社 | 無機酸化物コロイド粒子 |
| JP3122688B2 (ja) * | 1992-04-11 | 2001-01-09 | 触媒化成工業株式会社 | 無機酸化物コロイド粒子 |
| JP4032503B2 (ja) * | 1997-05-26 | 2008-01-16 | 日産化学工業株式会社 | 疎水性オルガノシリカゾルの製造方法 |
| US5908660A (en) * | 1997-09-03 | 1999-06-01 | Dow Corning Corporation | Method of preparing hydrophobic precipitated silica |
| EP1010666B1 (de) * | 1998-06-12 | 2009-11-04 | Mitsubishi Paper Mills Limited | Siliciumdioxid-aluminiumoxid-verbund-sol, verfahren zu dessen herstellung, und aufnahme-medium |
| US6051672A (en) * | 1998-08-24 | 2000-04-18 | Dow Corning Corporation | Method for making hydrophobic non-aggregated colloidal silica |
-
2000
- 2000-01-28 JP JP2000024767A patent/JP4631119B2/ja not_active Expired - Lifetime
-
2001
- 2001-01-29 WO PCT/NL2001/000063 patent/WO2001055030A2/en not_active Ceased
- 2001-01-29 AU AU2001236182A patent/AU2001236182A1/en not_active Abandoned
- 2001-01-29 TW TW090101689A patent/TW524772B/zh not_active IP Right Cessation
- 2001-01-29 DE DE60107049T patent/DE60107049T2/de not_active Expired - Lifetime
- 2001-01-29 KR KR1020027009163A patent/KR100716853B1/ko not_active Expired - Lifetime
- 2001-01-29 CN CNB018042821A patent/CN1220627C/zh not_active Expired - Lifetime
- 2001-01-29 EP EP01908439A patent/EP1252095B1/de not_active Expired - Lifetime
- 2001-01-29 AT AT01908439T patent/ATE282006T1/de not_active IP Right Cessation
-
2002
- 2002-07-26 US US10/205,626 patent/US20030035888A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| EP1252095B1 (de) | 2004-11-10 |
| JP4631119B2 (ja) | 2011-02-16 |
| WO2001055030A2 (en) | 2001-08-02 |
| TW524772B (en) | 2003-03-21 |
| CN1429178A (zh) | 2003-07-09 |
| US20030035888A1 (en) | 2003-02-20 |
| JP2001213617A (ja) | 2001-08-07 |
| DE60107049T2 (de) | 2005-10-20 |
| KR100716853B1 (ko) | 2007-05-09 |
| CN1220627C (zh) | 2005-09-28 |
| KR20020074479A (ko) | 2002-09-30 |
| DE60107049D1 (de) | 2004-12-16 |
| EP1252095A2 (de) | 2002-10-30 |
| AU2001236182A1 (en) | 2001-08-07 |
| WO2001055030A3 (en) | 2002-02-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |