ATE353348T1 - Kontinuierliches verfahren und system zur herstellung von polyetherpolyolen - Google Patents

Kontinuierliches verfahren und system zur herstellung von polyetherpolyolen

Info

Publication number
ATE353348T1
ATE353348T1 AT04717948T AT04717948T ATE353348T1 AT E353348 T1 ATE353348 T1 AT E353348T1 AT 04717948 T AT04717948 T AT 04717948T AT 04717948 T AT04717948 T AT 04717948T AT E353348 T1 ATE353348 T1 AT E353348T1
Authority
AT
Austria
Prior art keywords
loop reactor
rate
continuous process
reactor
polyether polyols
Prior art date
Application number
AT04717948T
Other languages
English (en)
Inventor
Jan W Verwijs
Walter J S Papadopulos
John W Weston
Richard J Elwell
Carlos M Villa
Original Assignee
Dow Global Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies Inc filed Critical Dow Global Technologies Inc
Application granted granted Critical
Publication of ATE353348T1 publication Critical patent/ATE353348T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1812—Tubular reactors
    • B01J19/1837—Loop-type reactors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • Polyethers (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
AT04717948T 2003-03-07 2004-03-05 Kontinuierliches verfahren und system zur herstellung von polyetherpolyolen ATE353348T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US45307303P 2003-03-07 2003-03-07

Publications (1)

Publication Number Publication Date
ATE353348T1 true ATE353348T1 (de) 2007-02-15

Family

ID=32990720

Family Applications (1)

Application Number Title Priority Date Filing Date
AT04717948T ATE353348T1 (de) 2003-03-07 2004-03-05 Kontinuierliches verfahren und system zur herstellung von polyetherpolyolen

Country Status (13)

Country Link
US (2) US7378559B2 (de)
EP (1) EP1603965B1 (de)
JP (1) JP2007524719A (de)
KR (1) KR20050107604A (de)
CN (1) CN1867609A (de)
AT (1) ATE353348T1 (de)
AU (1) AU2004220072A1 (de)
BR (1) BRPI0408669A (de)
CA (1) CA2518201A1 (de)
DE (1) DE602004004639T2 (de)
MX (1) MXPA05009512A (de)
WO (1) WO2004081082A1 (de)
ZA (1) ZA200506576B (de)

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DE102005034001A1 (de) * 2005-07-18 2007-01-25 Basf Ag Verfahren zur Herstellung von Polyetheralkoholen
US7495063B2 (en) 2006-02-03 2009-02-24 Dow Global Technologies Inc. Reduced oligomer concentration in high purity polyalkylene glycols
DE502007004339D1 (de) * 2006-06-23 2010-08-19 Basf Se Verfahren zur kontinuierlichen herstellung von polyetheralkoholen
CN101003622B (zh) * 2007-01-18 2010-05-26 浙江大学 一种负载型双金属氰化络合物催化剂及其制备方法和应用
AR073933A1 (es) * 2008-05-19 2010-12-15 Dow Global Technologies Inc Procedimiento de flujo de recirculacion continuo para la produccion de poliol de polieter
WO2010045104A2 (en) * 2008-10-13 2010-04-22 Dow Global Technologies, Inc. Process for the production of chlorinated and/or fluorinated propenes
CN102686544B (zh) 2009-10-09 2017-02-15 蓝立方知识产权公司 用于生产氯化和/或氟化丙烯和高级烯烃的方法
KR20120093857A (ko) * 2009-10-09 2012-08-23 다우 글로벌 테크놀로지스 엘엘씨 염화 및/또는 불화 프로펜의 제조 방법
KR20120091192A (ko) * 2009-10-09 2012-08-17 다우 글로벌 테크놀로지스 엘엘씨 등온 다중튜브 반응기 및 이를 도입한 방법
CN102753603B (zh) 2009-12-14 2015-01-14 陶氏环球技术有限责任公司 使用双金属氰化物催化剂连续制备低当量多元醇的方法
WO2011089120A1 (de) 2010-01-20 2011-07-28 Bayer Materialscience Ag Verfahren zur aktivierung von doppelmetallcyanidkatalysatoren zur herstellung von polyethercarbonatpolyolen
DE102010008410A1 (de) 2010-02-18 2011-08-18 Bayer MaterialScience AG, 51373 Verfahren zur Herstellung von Polyethercarbonatpolyolen
CA2794087A1 (en) 2010-03-24 2011-09-29 Christoph Guertler Method for producing polyether carbonate polyols
SG185607A1 (en) 2010-05-18 2012-12-28 Bayer Ip Gmbh Method for producing polyether carbonate polyols
DE102010040517A1 (de) 2010-09-09 2012-03-15 Bayer Materialscience Aktiengesellschaft Verfahren zur Herstellung von Polyetherpolyolen
DE102010043409A1 (de) 2010-11-04 2012-05-10 Bayer Materialscience Aktiengesellschaft Verfahren zur Herstellung von Polycarbonatpolyolen durch immortale Polymerisation von cyclischen Carbonaten
EP2465890A1 (de) 2010-12-17 2012-06-20 Bayer MaterialScience AG Verfahren zur Herstellung von Polyethercarbonatpolyolen mit primären Hydroxyl-Endgruppen und daraus hergestellte Polyurethanpolymere
WO2012113871A1 (en) * 2011-02-24 2012-08-30 Shell Internationale Research Maatschappij B.V. Process and reactor system for the preparation of polyether polyols
JP6212035B2 (ja) 2011-05-31 2017-10-11 ブルー キューブ アイピー エルエルシー 塩素化プロペンの製造方法
JP5918358B2 (ja) 2011-05-31 2016-05-18 ブルー キューブ アイピー エルエルシー 塩素化プロペンの製造方法
KR102007722B1 (ko) 2011-06-08 2019-08-07 다우 글로벌 테크놀로지스 엘엘씨 염화 및/또는 불화 프로펜의 제조 방법
CN103717557A (zh) 2011-08-07 2014-04-09 陶氏环球技术有限责任公司 生产氯化的丙烯的方法
CN103717559A (zh) 2011-08-07 2014-04-09 陶氏环球技术有限责任公司 生产氯化的丙烯的方法
CA2856271A1 (en) 2011-11-21 2013-05-30 Dow Global Technologies Llc Process for the production of chlorinated alkanes
EP2785671B1 (de) 2011-12-02 2017-03-01 Blue Cube IP LLC Verfahren zur herstellung von chlorierten propanen
JP6059246B2 (ja) 2011-12-02 2017-01-11 ブルー キューブ アイピー エルエルシー 塩素化アルカンの製造方法
JP6170068B2 (ja) 2011-12-13 2017-07-26 ブルー キューブ アイピー エルエルシー 塩素化プロパン及びプロペンの製造方法
CN104011000A (zh) 2011-12-22 2014-08-27 陶氏环球技术有限责任公司 生产四氯甲烷的方法
US9512049B2 (en) 2011-12-23 2016-12-06 Dow Global Technologies Llc Process for the production of alkenes and/or aromatic compounds
US9598334B2 (en) 2012-09-20 2017-03-21 Blue Cube Ip Llc Process for the production of chlorinated propenes
WO2014046970A1 (en) 2012-09-20 2014-03-27 Dow Global Technologies, Llc Process for the production of chlorinated propenes
WO2014052945A2 (en) 2012-09-30 2014-04-03 Dow Global Technologies, Llc Weir quench and processes incorporating the same
WO2014066083A1 (en) 2012-10-26 2014-05-01 Dow Global Technologies, Llc Mixer and reactor and process incorporating the same
CN104870411B (zh) 2012-12-18 2018-10-02 蓝立方知识产权有限责任公司 用于生产氯化丙烯的方法
CA2894168C (en) 2012-12-19 2018-04-24 Dow Global Technologies Llc Process for the production of chlorinated propenes
CA2901450A1 (en) 2013-02-27 2014-09-04 Blue Cube Ip Llc Process for the production of chlorinated propenes
WO2014164368A1 (en) 2013-03-09 2014-10-09 Dow Global Technologies Llc Process for the production of chlorinated alkanes
CN105408377B (zh) 2013-06-13 2018-06-22 科思创德国股份公司 聚醚碳酸酯-聚甲醛嵌段共聚物
CN114174381B (zh) 2019-08-01 2024-06-04 陶氏环球技术有限责任公司 纯化聚醚多元醇的方法

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Also Published As

Publication number Publication date
EP1603965A1 (de) 2005-12-14
ZA200506576B (en) 2006-12-27
CA2518201A1 (en) 2004-09-23
DE602004004639T2 (de) 2007-11-08
US20060155151A1 (en) 2006-07-13
CN1867609A (zh) 2006-11-22
DE602004004639D1 (de) 2007-03-22
WO2004081082A1 (en) 2004-09-23
JP2007524719A (ja) 2007-08-30
US20080221281A1 (en) 2008-09-11
KR20050107604A (ko) 2005-11-14
AU2004220072A1 (en) 2004-09-23
EP1603965B1 (de) 2007-02-07
US7378559B2 (en) 2008-05-27
MXPA05009512A (es) 2006-02-22
BRPI0408669A (pt) 2006-03-28

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