ATE396965T1 - Verfahren zur reaktiven extraktion von levulinsäure - Google Patents
Verfahren zur reaktiven extraktion von levulinsäureInfo
- Publication number
- ATE396965T1 ATE396965T1 AT05707842T AT05707842T ATE396965T1 AT E396965 T1 ATE396965 T1 AT E396965T1 AT 05707842 T AT05707842 T AT 05707842T AT 05707842 T AT05707842 T AT 05707842T AT E396965 T1 ATE396965 T1 AT E396965T1
- Authority
- AT
- Austria
- Prior art keywords
- alcohol
- levulinic acid
- reactive extraction
- aqueous mixture
- levulic acid
- Prior art date
Links
- JOOXCMJARBKPKM-UHFFFAOYSA-N 4-oxopentanoic acid Chemical compound CC(=O)CCC(O)=O JOOXCMJARBKPKM-UHFFFAOYSA-N 0.000 title abstract 7
- 238000000605 extraction Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 5
- 229940058352 levulinate Drugs 0.000 abstract 3
- -1 levulinate ester Chemical class 0.000 abstract 3
- 229940040102 levulinic acid Drugs 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000008346 aqueous phase Substances 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 230000032050 esterification Effects 0.000 abstract 1
- 238000005886 esterification reaction Methods 0.000 abstract 1
- 239000000284 extract Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP04100272 | 2004-01-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE396965T1 true ATE396965T1 (de) | 2008-06-15 |
Family
ID=34802686
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT05707842T ATE396965T1 (de) | 2004-01-26 | 2005-01-26 | Verfahren zur reaktiven extraktion von levulinsäure |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US7378549B2 (de) |
| EP (1) | EP1723099B1 (de) |
| JP (1) | JP2007518778A (de) |
| CN (1) | CN100548966C (de) |
| AT (1) | ATE396965T1 (de) |
| AU (1) | AU2005206337B2 (de) |
| BR (1) | BRPI0507060A (de) |
| CA (1) | CA2554186A1 (de) |
| DE (1) | DE602005007190D1 (de) |
| PL (1) | PL1723099T3 (de) |
| RU (1) | RU2391333C2 (de) |
| WO (1) | WO2005070867A1 (de) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7501062B2 (en) * | 2005-02-22 | 2009-03-10 | Shell Oil Company | Process for permeation enhanced reactive extraction of levulinic acid |
| EP1954140B1 (de) | 2005-11-22 | 2013-05-29 | Segetis, Inc. | Glycerinlevulinatketale und ihre verwendung |
| FI121541B (fi) | 2008-04-21 | 2010-12-31 | Kemira Oyj | Menetelmä muurahaishapon talteenottamiseksi |
| ITMI20081164A1 (it) * | 2008-06-26 | 2009-12-27 | Eni Spa | Processo per la produzione di esteri dell'acido levulinico da biomasse |
| WO2010036884A1 (en) | 2008-09-25 | 2010-04-01 | Segetis, Inc. | Ketal ester derivatives |
| JP5366128B2 (ja) * | 2008-12-19 | 2013-12-11 | 独立行政法人産業技術総合研究所 | レブリン酸エステルの製造方法 |
| US8138371B2 (en) | 2009-03-11 | 2012-03-20 | Biofine Technologies Llc | Production of formic acid |
| WO2010106536A1 (en) * | 2009-03-16 | 2010-09-23 | Ben-Gurion University Of The Negev Research And Development Authority | Diesel fuel from vegetable and animal oils blended with alkyl levulinates |
| US20100312006A1 (en) * | 2009-06-09 | 2010-12-09 | Meadwestvaco Corporation | Production of levulinic acid and levulinate esters from biomass |
| BR112012032172A2 (pt) | 2010-06-18 | 2015-11-24 | Butamax Tm Advanced Biofuels | método para produzir um álcool e composição |
| US9040263B2 (en) | 2010-07-28 | 2015-05-26 | Butamax Advanced Biofuels Llc | Production of alcohol esters and in situ product removal during alcohol fermentation |
| FI20106311L (fi) | 2010-12-10 | 2012-06-11 | Kemira Oyj | Menetelmä orgaanisen hapon talteenottamiseksi laimeasta vesiliuoksesta |
| CA2825625C (en) * | 2011-02-01 | 2020-01-07 | University Of Maine System Board Of Trustees | Process for improving the energy density of feedstocks using formate salts |
| BR112014011672A2 (pt) * | 2011-11-23 | 2017-05-30 | Segetis Inc | processo para preparar ácido levulínico |
| WO2013138222A1 (en) | 2012-03-12 | 2013-09-19 | Georgie-Pacific Llc | Method for producing levulinic acid from lignocellulosis biomass |
| FR2992643B1 (fr) | 2012-07-02 | 2014-08-08 | Centre Nat Rech Scient | Procede de preparation d'esters de l'acide levulinique |
| US9073841B2 (en) | 2012-11-05 | 2015-07-07 | Segetis, Inc. | Process to prepare levulinic acid |
| EP3227260B1 (de) | 2014-12-03 | 2021-02-24 | Praj Industries Limited | Verfahren zur herstellung von levulinsäure |
| FI126451B (fi) * | 2014-12-23 | 2016-12-15 | Chempolis Oy | Prosessijärjestelmä kemikaalien erottelemiseksi, tislauskolonnijärjestely ja kemikaalien erottelumenetelmä |
| WO2018011741A1 (en) | 2016-07-15 | 2018-01-18 | Sabic Global Technologies B.V. | Synthesis of ketals and levulinates |
| CN114315554B (zh) * | 2021-12-23 | 2024-05-28 | 山东理工大学 | 水合物熔盐中甲酸和乙酰丙酸的分离方法 |
| IT202200007589A1 (it) | 2022-04-15 | 2023-10-15 | Pabif Srl | Processo ed apparato per la produzione di acido levulinico da cellulosa ricavata da biomasse |
| AU2024201711B2 (en) * | 2023-04-12 | 2025-05-15 | Department Of Biotechnology | An integrated process for the purification of levulinic acid from technical lignin |
| MX2025013409A (es) | 2023-05-12 | 2026-02-03 | Biofine Tech Llc | Métodos de producción y recuperación de ácido levulínico |
| WO2025151936A1 (pt) * | 2024-01-18 | 2025-07-24 | Oxiteno S.A. Indústria E Comércio | Composto éster, processo de preparação de um composto éster, e, uso do composto |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2029412A (en) | 1934-12-19 | 1936-02-04 | Niacet Chemicals Corp | Manufacture of esters of levulinic acid |
| IE33399B1 (en) | 1968-10-10 | 1974-06-12 | El Paso Products Co | Esterification and extraction process |
| JPS5139205B2 (de) * | 1972-05-12 | 1976-10-26 | ||
| CA1100148A (en) * | 1978-01-04 | 1981-04-28 | Rudolph L. Pohl | Photopolymer compositions for printing plates |
| JPS5587741A (en) * | 1978-12-27 | 1980-07-02 | Noguchi Kenkyusho | Preparation of levulinic acid |
| US4442303A (en) * | 1980-12-09 | 1984-04-10 | El Paso Products Company | Recovery of water miscible organic acids from aqueous solution as alkyl esters |
| US4476025A (en) | 1983-05-09 | 1984-10-09 | The United States Of America As Represented By The United States Department Of Energy | Separation of certain carboxylic acids utilizing cation exchange membranes |
| US4897497A (en) | 1988-04-26 | 1990-01-30 | Biofine Incorporated | Lignocellulose degradation to furfural and levulinic acid |
| US5562777A (en) | 1993-03-26 | 1996-10-08 | Arkenol, Inc. | Method of producing sugars using strong acid hydrolysis of cellulosic and hemicellulosic materials |
| US5608105A (en) | 1995-06-07 | 1997-03-04 | Biofine Incorporated | Production of levulinic acid from carbohydrate-containing materials |
| WO1997047579A1 (en) | 1996-06-10 | 1997-12-18 | Renewable Energy Development Corporation | Methods for synthesis of high purity carboxylic and fatty acids |
| US5892107A (en) | 1996-11-08 | 1999-04-06 | Arkenol, Inc. | Method for the production of levulinic acid |
| US6518454B1 (en) * | 2001-10-12 | 2003-02-11 | Eastman Chemical Company | Preparation of esters of carboxylic acids |
| RU2203266C1 (ru) * | 2001-11-08 | 2003-04-27 | Институт химии и химической технологии СО РАН | Способ получения левулиновой кислоты низкотемпературным кислотным гидролизом сахарозы |
| EP1490457B1 (de) | 2002-04-01 | 2007-06-13 | E.I. du Pont de Nemours and Company | Herstellung von lävulinsäureestern und ameisensäureestern aus biomasse und olefinen |
| US7501062B2 (en) | 2005-02-22 | 2009-03-10 | Shell Oil Company | Process for permeation enhanced reactive extraction of levulinic acid |
-
2005
- 2005-01-24 US US11/041,324 patent/US7378549B2/en not_active Expired - Fee Related
- 2005-01-26 DE DE602005007190T patent/DE602005007190D1/de not_active Expired - Lifetime
- 2005-01-26 AU AU2005206337A patent/AU2005206337B2/en not_active Ceased
- 2005-01-26 BR BRPI0507060-0A patent/BRPI0507060A/pt not_active IP Right Cessation
- 2005-01-26 PL PL05707842T patent/PL1723099T3/pl unknown
- 2005-01-26 CA CA002554186A patent/CA2554186A1/en not_active Abandoned
- 2005-01-26 EP EP05707842A patent/EP1723099B1/de not_active Expired - Lifetime
- 2005-01-26 RU RU2006130735/04A patent/RU2391333C2/ru not_active IP Right Cessation
- 2005-01-26 WO PCT/EP2005/050316 patent/WO2005070867A1/en not_active Ceased
- 2005-01-26 JP JP2006550181A patent/JP2007518778A/ja active Pending
- 2005-01-26 AT AT05707842T patent/ATE396965T1/de not_active IP Right Cessation
- 2005-01-26 CN CNB2005800032745A patent/CN100548966C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| AU2005206337B2 (en) | 2008-06-05 |
| US7378549B2 (en) | 2008-05-27 |
| RU2391333C2 (ru) | 2010-06-10 |
| CN1914148A (zh) | 2007-02-14 |
| EP1723099A1 (de) | 2006-11-22 |
| US20060047139A1 (en) | 2006-03-02 |
| EP1723099B1 (de) | 2008-05-28 |
| PL1723099T3 (pl) | 2008-12-31 |
| RU2006130735A (ru) | 2008-03-10 |
| AU2005206337A1 (en) | 2005-08-04 |
| BRPI0507060A (pt) | 2007-06-19 |
| JP2007518778A (ja) | 2007-07-12 |
| CN100548966C (zh) | 2009-10-14 |
| WO2005070867A1 (en) | 2005-08-04 |
| DE602005007190D1 (de) | 2008-07-10 |
| CA2554186A1 (en) | 2005-08-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |