ATE475634T1 - Verfahren zur herstellung von isopulegol - Google Patents
Verfahren zur herstellung von isopulegolInfo
- Publication number
- ATE475634T1 ATE475634T1 AT02000464T AT02000464T ATE475634T1 AT E475634 T1 ATE475634 T1 AT E475634T1 AT 02000464 T AT02000464 T AT 02000464T AT 02000464 T AT02000464 T AT 02000464T AT E475634 T1 ATE475634 T1 AT E475634T1
- Authority
- AT
- Austria
- Prior art keywords
- group
- atom
- carbon atom
- isopulegol
- producing
- Prior art date
Links
- ZYTMANIQRDEHIO-KXUCPTDWSA-N isopulegol Chemical compound C[C@@H]1CC[C@@H](C(C)=C)[C@H](O)C1 ZYTMANIQRDEHIO-KXUCPTDWSA-N 0.000 title abstract 4
- 239000001871 (1R,2R,5S)-5-methyl-2-prop-1-en-2-ylcyclohexan-1-ol Substances 0.000 title abstract 3
- 229940095045 isopulegol Drugs 0.000 title abstract 3
- ZYTMANIQRDEHIO-UHFFFAOYSA-N neo-Isopulegol Natural products CC1CCC(C(C)=C)C(O)C1 ZYTMANIQRDEHIO-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- 229910052799 carbon Inorganic materials 0.000 abstract 3
- 125000004432 carbon atom Chemical group C* 0.000 abstract 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 2
- 125000003118 aryl group Chemical group 0.000 abstract 2
- NEHNMFOYXAPHSD-UHFFFAOYSA-N citronellal Chemical compound O=CCC(C)CCC=C(C)C NEHNMFOYXAPHSD-UHFFFAOYSA-N 0.000 abstract 2
- 239000007983 Tris buffer Substances 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 229930003633 citronellal Natural products 0.000 abstract 1
- 235000000983 citronellal Nutrition 0.000 abstract 1
- 125000004663 dialkyl amino group Chemical group 0.000 abstract 1
- 125000005843 halogen group Chemical group 0.000 abstract 1
- 125000001072 heteroaryl group Chemical group 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/56—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by isomerisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001010527A JP4676617B2 (ja) | 2001-01-18 | 2001-01-18 | イソプレゴールの製造方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE475634T1 true ATE475634T1 (de) | 2010-08-15 |
Family
ID=18877825
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT02000464T ATE475634T1 (de) | 2001-01-18 | 2002-01-08 | Verfahren zur herstellung von isopulegol |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US6774269B2 (de) |
| EP (1) | EP1225163B1 (de) |
| JP (1) | JP4676617B2 (de) |
| AT (1) | ATE475634T1 (de) |
| DE (1) | DE60237128D1 (de) |
| ES (1) | ES2347528T3 (de) |
Families Citing this family (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8877901B2 (en) | 2002-12-13 | 2014-11-04 | Immunomedics, Inc. | Camptothecin-binding moiety conjugates |
| DE102004011543A1 (de) | 2004-03-08 | 2005-10-06 | Basf Ag | Verfahren zur Herstellung optisch aktiver Carbonylverbindungen |
| DE102004049631A1 (de) | 2004-10-11 | 2006-04-20 | Basf Ag | Verfahren zur Herstellung optisch aktiver Carbonylverbindungen |
| DE102004057277A1 (de) | 2004-11-26 | 2006-06-01 | Basf Ag | Verfahren zur Herstellung von Menthol |
| DE102004063003A1 (de) * | 2004-12-22 | 2006-07-13 | Basf Ag | Verfahren zur Herstellung von Isopulegol |
| DE102005010329A1 (de) * | 2005-03-03 | 2006-09-07 | Basf Ag | Diarylphenoxy-Aluminium-Verbindungen |
| JP5279275B2 (ja) * | 2005-03-03 | 2013-09-04 | ビーエーエスエフ ソシエタス・ヨーロピア | ジアリールフェノキシアルミニウム化合物 |
| DE102005040655A1 (de) | 2005-08-26 | 2007-03-01 | Basf Ag | Verfahren zur Herstellung von angereichertem Isopulegol |
| EP1940758B1 (de) * | 2005-09-26 | 2012-11-28 | Symrise AG | Intramolekulare prins-reaktion |
| ES2573252T3 (es) * | 2006-09-01 | 2016-06-06 | Basf Se | Recuperación de ligandos de bis(diarilfenol) en la preparación de isopulegol |
| ES2615462T3 (es) * | 2006-09-01 | 2017-06-07 | Basf Se | Recuperación de ligandos de bisfenol durante la preparación de isopulegol |
| WO2008132057A1 (de) | 2007-04-25 | 2008-11-06 | Basf Se | Verfahren zur herstellung optisch aktiver carbonylverbindungen |
| WO2008152009A1 (de) | 2007-06-12 | 2008-12-18 | Basf Se | Mentholschuppen und verfahren zur herstellung derselben |
| EP2036875A1 (de) | 2007-09-11 | 2009-03-18 | Basf Se | Kontinuierliches Verfahren zur Herstellung von Menthol in reiner oder angereicherter Form |
| JP5599716B2 (ja) * | 2007-11-30 | 2014-10-01 | ビーエーエスエフ ソシエタス・ヨーロピア | 光学活性ラセミメントールを製造するための方法 |
| US8329930B2 (en) | 2008-05-26 | 2012-12-11 | Takasago International Corporation | Aluminum complex and use thereof |
| US20110319638A1 (en) * | 2008-12-17 | 2011-12-29 | Takasago International Corporation | Aluminium complexes and use thereof as a catalyst in intramolecular ring closure reactions |
| EP2376411B1 (de) | 2008-12-17 | 2014-11-12 | Takasago International Corporation | Aluminiumkomplexe und deren verwendung als katalysator bei intramolekularen ringschlussreaktionen |
| ES2738700T3 (es) | 2009-02-13 | 2020-01-24 | Immunomedics Inc | Inmunoconjugados con un enlace escindible intracelularmente |
| US8217204B2 (en) | 2009-06-03 | 2012-07-10 | Takasago International Corporation | Catalyst for asymmetric hydrogenation |
| JP5648240B2 (ja) | 2010-05-25 | 2015-01-07 | 高砂香料工業株式会社 | 有機アルミニウム化合物 |
| JP5780933B2 (ja) | 2010-12-01 | 2015-09-16 | 高砂香料工業株式会社 | 光学活性メントールの製造方法 |
| WO2014077321A1 (ja) | 2012-11-15 | 2014-05-22 | 高砂香料工業株式会社 | アルミニウム触媒 |
| US20150329452A1 (en) | 2012-11-15 | 2015-11-19 | Takasago International Corporation | Method for producing optically active isopulegol and optically active menthol |
| EP3919148B1 (de) | 2014-03-19 | 2024-05-08 | Basf Se | Vorrichtung zum abtrennen eines stoffes aus einer lösung |
| JP2016098207A (ja) * | 2014-11-25 | 2016-05-30 | 高砂香料工業株式会社 | 光学活性アルコールの製造方法 |
| WO2016097242A1 (de) | 2014-12-19 | 2016-06-23 | Basf Se | Verfahren zur herstellung optisch aktiver carbonylverbindungen |
| CN107188781B (zh) * | 2017-06-02 | 2020-07-24 | 万华化学集团股份有限公司 | 一种由香茅醛制备异胡薄荷醇的方法 |
| JP7456789B2 (ja) * | 2020-01-30 | 2024-03-27 | 高砂香料工業株式会社 | イソプレゴールの製造方法 |
| CN121443573A (zh) | 2023-07-07 | 2026-01-30 | 巴斯夫欧洲公司 | 香叶醛和橙花醛的光异构化 |
| WO2025191084A1 (en) | 2024-03-15 | 2025-09-18 | Basf Se | Rhodium-carbonyl compounds for use as selective hydrogenation catalysts |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5945661B2 (ja) * | 1977-03-18 | 1984-11-07 | 高砂香料工業株式会社 | ｄ−シトロネラ−ルからｌ−イソプレゴ−ルへの立体選択的閉環方法 |
| DE19857313A1 (de) * | 1997-12-12 | 1999-12-16 | Sec Dep Of Science And Technol | Stark saurer mikroporöser synergistischer Festkörper-Katalysator und Verwendungen desselben |
| EP0926117A1 (de) | 1997-12-22 | 1999-06-30 | Quest International B.V. | Verfahren zur Herstellung von Isopulegol |
| CA2265310C (en) * | 1998-03-23 | 2007-12-18 | Kuraray Co., Ltd. | Preparation process of acrylic acid ester polymer |
-
2001
- 2001-01-18 JP JP2001010527A patent/JP4676617B2/ja not_active Expired - Lifetime
-
2002
- 2002-01-08 EP EP02000464A patent/EP1225163B1/de not_active Expired - Lifetime
- 2002-01-08 ES ES02000464T patent/ES2347528T3/es not_active Expired - Lifetime
- 2002-01-08 DE DE60237128T patent/DE60237128D1/de not_active Expired - Lifetime
- 2002-01-08 AT AT02000464T patent/ATE475634T1/de not_active IP Right Cessation
- 2002-01-15 US US10/045,157 patent/US6774269B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| US20020133046A1 (en) | 2002-09-19 |
| EP1225163A3 (de) | 2004-01-14 |
| JP4676617B2 (ja) | 2011-04-27 |
| EP1225163B1 (de) | 2010-07-28 |
| EP1225163A2 (de) | 2002-07-24 |
| JP2002212121A (ja) | 2002-07-31 |
| DE60237128D1 (de) | 2010-09-09 |
| ES2347528T3 (es) | 2010-11-02 |
| US6774269B2 (en) | 2004-08-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |