ATE546412T1 - Verfahren zur herstellung von kohlenstofffasern - Google Patents

Verfahren zur herstellung von kohlenstofffasern

Info

Publication number
ATE546412T1
ATE546412T1 AT01944546T AT01944546T ATE546412T1 AT E546412 T1 ATE546412 T1 AT E546412T1 AT 01944546 T AT01944546 T AT 01944546T AT 01944546 T AT01944546 T AT 01944546T AT E546412 T1 ATE546412 T1 AT E546412T1
Authority
AT
Austria
Prior art keywords
catalyst
carbon
chamber
carbon fibers
deposition
Prior art date
Application number
AT01944546T
Other languages
English (en)
Inventor
Avetik R Harutyunyan
Leonid Grigorian
Original Assignee
Penn State Res Found
Honda Motor Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Penn State Res Found, Honda Motor Co Ltd filed Critical Penn State Res Found
Application granted granted Critical
Publication of ATE546412T1 publication Critical patent/ATE546412T1/de

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/158Carbon nanotubes
    • C01B32/16Preparation
    • C01B32/162Preparation characterised by catalysts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74Iron group metals
    • B01J23/745Iron
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00Manufacture or treatment of nanostructures
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/127Carbon filaments; Apparatus specially adapted for the manufacture thereof by thermal decomposition of hydrocarbon gases or vapours or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00132Controlling the temperature using electric heating or cooling elements
    • B01J2219/00135Electric resistance heaters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0803Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • B01J2219/085Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy creating magnetic fields
    • B01J2219/0852Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy creating magnetic fields employing permanent magnets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0871Heating or cooling of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0873Materials to be treated
    • B01J2219/0875Gas
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/0873Materials to be treated
    • B01J2219/0892Materials to be treated involving catalytically active material

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Textile Engineering (AREA)
  • Composite Materials (AREA)
  • General Chemical & Material Sciences (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Manufacturing & Machinery (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Inorganic Fibers (AREA)
  • Catalysts (AREA)
AT01944546T 2000-06-16 2001-06-15 Verfahren zur herstellung von kohlenstofffasern ATE546412T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US21219200P 2000-06-16 2000-06-16
PCT/US2001/019227 WO2001098208A1 (en) 2000-06-16 2001-06-15 Method and apparatus for producing carbonaceous articles

Publications (1)

Publication Number Publication Date
ATE546412T1 true ATE546412T1 (de) 2012-03-15

Family

ID=22789943

Family Applications (1)

Application Number Title Priority Date Filing Date
AT01944546T ATE546412T1 (de) 2000-06-16 2001-06-15 Verfahren zur herstellung von kohlenstofffasern

Country Status (5)

Country Link
US (1) US6730284B2 (de)
EP (1) EP1296890B1 (de)
JP (1) JP4896345B2 (de)
AT (1) ATE546412T1 (de)
WO (1) WO2001098208A1 (de)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6591658B1 (en) * 2000-10-25 2003-07-15 Advanced Micro Devices, Inc. Carbon nanotubes as linewidth standards for SEM & AFM
US6761871B2 (en) * 2001-05-22 2004-07-13 Reginald Bernard Little Magnetic production of carbon nanotubes and filaments
US6897603B2 (en) * 2001-08-24 2005-05-24 Si Diamond Technology, Inc. Catalyst for carbon nanotube growth
AU2002332622A1 (en) * 2001-08-24 2003-03-10 Nano-Proprietary, Inc. Catalyst for carbon nanotube growth
JP4404961B2 (ja) * 2002-01-08 2010-01-27 双葉電子工業株式会社 カーボンナノ繊維の製造方法。
CA2385802C (en) * 2002-05-09 2008-09-02 Institut National De La Recherche Scientifique Method and apparatus for producing single-wall carbon nanotubes
JP3876313B2 (ja) * 2002-11-12 2007-01-31 国立大学法人 北海道大学 繊維状固体炭素集合体の製造方法
JP4608863B2 (ja) * 2003-09-22 2011-01-12 富士ゼロックス株式会社 カーボンナノチューブの製造装置および製造方法、並びにそれに用いるガス分解器
US20060078489A1 (en) * 2004-09-09 2006-04-13 Avetik Harutyunyan Synthesis of small and narrow diameter distributed carbon single walled nanotubes
US7862795B2 (en) * 2004-11-16 2011-01-04 Hyperion Catalysis International, Inc. Method for preparing single walled carbon nanotubes
US7635518B1 (en) 2005-02-04 2009-12-22 University Of Louisiana At Lafayette Dendritic magnetic nanostructures and method for making same
US7862793B2 (en) * 2005-04-08 2011-01-04 The Regents Of The University Of California Growth of and defect reduction in nanoscale materials
TWI306834B (en) * 2005-05-27 2009-03-01 Ind Tech Res Inst A method for manufacturing carbonaceous nanofiber
WO2007009112A2 (en) * 2005-07-14 2007-01-18 Colorado School Of Mines Membrane separation of feed and growth environments in carbon nanostructure growth
CN1935637B (zh) * 2005-09-23 2010-05-05 清华大学 碳纳米管制备方法
JP2007091482A (ja) * 2005-09-26 2007-04-12 Sonac Kk カーボンファイバの集合体、集合体を構成するカーボンファイバ、およびカーボンファイバの回収方法
US8163263B2 (en) * 2006-01-30 2012-04-24 Honda Motor Co., Ltd. Catalyst for the growth of carbon single-walled nanotubes
US20080279753A1 (en) * 2006-01-30 2008-11-13 Harutyunyan Avetik R Method and Apparatus for Growth of High Quality Carbon Single-Walled Nanotubes
US8268281B2 (en) * 2006-05-12 2012-09-18 Honda Motor Co., Ltd. Dry powder injector for industrial production of carbon single walled nanotubes (SWNTs)
US20120132534A1 (en) * 2006-08-01 2012-05-31 The Board Of Regents Of The Nev. Sys. Of Higher Ed On Behalf Of The Unlv Growth of nanotubes from patterned and ordered nanoparticles
US8684284B2 (en) 2006-11-24 2014-04-01 Honda Motor Co., Ltd. Injector for large amount of aerosol powder for synthesis of carbon nanotubes
US8591858B2 (en) * 2008-05-01 2013-11-26 Honda Motor Co., Ltd. Effect of hydrocarbon and transport gas feedstock on efficiency and quality of grown single-walled nanotubes
US9174847B2 (en) * 2008-05-01 2015-11-03 Honda Motor Co., Ltd. Synthesis of high quality carbon single-walled nanotubes
US8119074B2 (en) * 2008-12-17 2012-02-21 Centro de Investigacion en Materiales Avanzados, S.C Method and apparatus for the continuous production of carbon nanotubes
KR20160057393A (ko) * 2013-09-30 2016-05-23 니폰 제온 가부시키가이샤 탄소 나노구조체의 제조 방법 및 카본 나노튜브
WO2015101917A1 (en) 2013-12-30 2015-07-09 Indian Oil Corporation Limited Process for simultaneous production of carbon nanotube and a product gas from crude oil and its products

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JPS57115488A (en) * 1980-12-30 1982-07-17 Nippon Oil Co Ltd Fluidized catalytic cracking method of heavy petroleum
CA1175616A (en) 1981-01-05 1984-10-09 Exxon Research And Engineering Company Production of iron monoxide and carbon filaments therefrom
JPS60195092A (ja) * 1984-03-15 1985-10-03 Tdk Corp カ−ボン系薄膜の製造方法および装置
US4663230A (en) 1984-12-06 1987-05-05 Hyperion Catalysis International, Inc. Carbon fibrils, method for producing same and compositions containing same
US5165909A (en) 1984-12-06 1992-11-24 Hyperion Catalysis Int'l., Inc. Carbon fibrils and method for producing same
US5149584A (en) 1990-10-23 1992-09-22 Baker R Terry K Carbon fiber structures having improved interlaminar properties
US5458784A (en) 1990-10-23 1995-10-17 Catalytic Materials Limited Removal of contaminants from aqueous and gaseous streams using graphic filaments
JPH06170244A (ja) * 1992-12-02 1994-06-21 Tdk Corp 磁性触媒粒子の回収装置
DE4339139A1 (de) * 1993-11-16 1995-05-24 Basf Ag Magnetisch abtrennbare Katalysatoren
US5547748A (en) * 1994-01-14 1996-08-20 Sri International Carbon nanoencapsulates
JPH0848510A (ja) * 1994-08-04 1996-02-20 Satoru Mieno アーク放電によるフラーレン自動合成装置
US5866434A (en) 1994-12-08 1999-02-02 Meso Scale Technology Graphitic nanotubes in luminescence assays
US5593740A (en) 1995-01-17 1997-01-14 Synmatix Corporation Method and apparatus for making carbon-encapsulated ultrafine metal particles
US5780101A (en) 1995-02-17 1998-07-14 Arizona Board Of Regents On Behalf Of The University Of Arizona Method for producing encapsulated nanoparticles and carbon nanotubes using catalytic disproportionation of carbon monoxide
US5872422A (en) 1995-12-20 1999-02-16 Advanced Technology Materials, Inc. Carbon fiber-based field emission devices
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US5997832A (en) 1997-03-07 1999-12-07 President And Fellows Of Harvard College Preparation of carbide nanorods
JPH11124740A (ja) * 1997-10-17 1999-05-11 Noritake Co Ltd カーボンマイクロコイル及びその製造方法
JP3497740B2 (ja) * 1998-09-09 2004-02-16 株式会社東芝 カーボンナノチューブの製造方法及び電界放出型冷陰極装置の製造方法
CA2344180C (en) * 1998-09-18 2008-04-29 William Marsh Rice University Catalytic growth of single-wall carbon nanotubes from metal particles
US6333016B1 (en) * 1999-06-02 2001-12-25 The Board Of Regents Of The University Of Oklahoma Method of producing carbon nanotubes
JP3355157B2 (ja) * 1999-09-24 2002-12-09 株式会社荏原製作所 カーボンナノファイバーの製造方法
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Also Published As

Publication number Publication date
EP1296890A1 (de) 2003-04-02
EP1296890B1 (de) 2012-02-22
EP1296890A4 (de) 2006-03-15
JP4896345B2 (ja) 2012-03-14
JP2003535802A (ja) 2003-12-02
US6730284B2 (en) 2004-05-04
US20010053344A1 (en) 2001-12-20
WO2001098208A1 (en) 2001-12-27

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