ATE72566T1 - Tetrachlorraffinose und deren verwendung zur herstellung von sucralose. - Google Patents

Tetrachlorraffinose und deren verwendung zur herstellung von sucralose.

Info

Publication number: ATE72566T1
Authority: AT; Austria
Prior art keywords: tcr; chloro; sucralose; tetrachloraffinose; production
Prior art date: 1985-10-21

Application number

AT86308128T

Other languages

English (en)

Inventor

Elner Brean Rathbone

Khizar Sultan Mufti

Riaz Ahmed Khan

Peter Samuel James Cheetham

Andrew John Hacking

Jonathan Seth Dordick

Original Assignee

Tate & Lyle Plc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-10-21

Filing date

1986-10-20

Publication date

1992-02-15

1986-10-20 Application filed by Tate & Lyle Plc filed Critical Tate & Lyle Plc

1992-02-15 Application granted granted Critical

1992-02-15 Publication of ATE72566T1 publication Critical patent/ATE72566T1/de

Links

239000004376 Sucralose Substances 0.000 title abstract 2
BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 title abstract 2
235000019408 sucralose Nutrition 0.000 title abstract 2
102000004190 Enzymes Human genes 0.000 abstract 2
108090000790 Enzymes Proteins 0.000 abstract 2
FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 abstract 2
-1 6-chloro-6-deoxygalactosyl moiety Chemical group 0.000 abstract 1
241000228245 Aspergillus niger Species 0.000 abstract 1
241000467320 Circinella muscae Species 0.000 abstract 1
MUPFEKGTMRGPLJ-RMMQSMQOSA-N Raffinose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 MUPFEKGTMRGPLJ-RMMQSMQOSA-N 0.000 abstract 1
MUPFEKGTMRGPLJ-UHFFFAOYSA-N UNPD196149 Natural products OC1C(O)C(CO)OC1(CO)OC1C(O)C(O)C(O)C(COC2C(C(O)C(O)C(CO)O2)O)O1 MUPFEKGTMRGPLJ-UHFFFAOYSA-N 0.000 abstract 1
241000180122 Umbelopsis vinacea Species 0.000 abstract 1
MUPFEKGTMRGPLJ-ZQSKZDJDSA-N raffinose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O2)O)O1 MUPFEKGTMRGPLJ-ZQSKZDJDSA-N 0.000 abstract 1
FIQMHBFVRAXMOP-UHFFFAOYSA-N triphenylphosphane oxide Chemical compound C=1C=CC=CC=1P(C=1C=CC=CC=1)(=O)C1=CC=CC=C1 FIQMHBFVRAXMOP-UHFFFAOYSA-N 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
- C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/20—Preparation of compounds containing saccharide radicals produced by the action of an exo-1,4 alpha-glucosidase, e.g. dextrose

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Health & Medical Sciences (AREA)
Biochemistry (AREA)
Biotechnology (AREA)
General Health & Medical Sciences (AREA)
Genetics & Genomics (AREA)
Molecular Biology (AREA)
Zoology (AREA)
Wood Science & Technology (AREA)
Microbiology (AREA)
General Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Bioinformatics & Cheminformatics (AREA)
General Engineering & Computer Science (AREA)
Saccharide Compounds (AREA)
Preparation Of Compounds By Using Micro-Organisms (AREA)
Enzymes And Modification Thereof (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Agricultural Chemicals And Associated Chemicals (AREA)

AT86308128T 1985-10-21 1986-10-20 Tetrachlorraffinose und deren verwendung zur herstellung von sucralose. ATE72566T1 (de)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
GB858525871A GB8525871D0 (en)	1985-10-21	1985-10-21	Chemical compound
EP86308128A EP0221717B1 (de)	1985-10-21	1986-10-20	Tetrachlorraffinose und deren Verwendung zur Herstellung von Sucralose

Publications (1)

Publication Number	Publication Date
ATE72566T1 true ATE72566T1 (de)	1992-02-15

Family

ID=10586980

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT86308128T ATE72566T1 (de)	1985-10-21	1986-10-20	Tetrachlorraffinose und deren verwendung zur herstellung von sucralose.

Country Status (21)

Country	Link
US (1)	US4826962A (de)
EP (1)	EP0221717B1 (de)
JP (2)	JPH0644874B2 (de)
KR (1)	KR950005922B1 (de)
AT (1)	ATE72566T1 (de)
AU (1)	AU589224B2 (de)
CA (1)	CA1282728C (de)
DE (1)	DE3683888D1 (de)
DK (1)	DK164869C (de)
ES (1)	ES2033236T3 (de)
FI (1)	FI82836C (de)
GB (2)	GB8525871D0 (de)
GR (1)	GR3004316T3 (de)
IE (1)	IE59482B1 (de)
IL (1)	IL80365A (de)
NO (1)	NO168373C (de)
NZ (1)	NZ217998A (de)
PH (1)	PH24621A (de)
PT (1)	PT83587B (de)
SU (1)	SU1635905A3 (de)
ZA (1)	ZA867918B (de)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2602774B1 (fr) *	1986-07-29	1990-10-19	Atta	Nouvelles molecules amphiphiles polyhydroxylees et perfluoroalkylees ayant des proprietes tensioactives
US4986991A (en) *	1987-05-15	1991-01-22	Wm Wrigley, Jr., Company	Chewing gum having an extended sweetness
US5191071A (en) *	1987-08-21	1993-03-02	Novo Nordisk A/S	Monoesters of glycosides and a process for enzymatic preparation thereof
GB8818430D0 (en) *	1988-08-03	1988-09-07	Tate & Lyle Plc	Process
MD31C2 (ro) *	1988-09-16	1995-01-31	Tate & Lyle Public Limited Company	Procedeu de obţinere a zaharolozei
GB2222827B (en) *	1988-09-16	1992-08-19	Tate & Lyle Plc	Chlorination of sugars
US5136031A (en) *	1990-07-09	1992-08-04	Tate & Lyle Public Limited Company	Chlorination of sugars
JPH05509095A (ja) *	1990-07-17	1993-12-16	ヨーロピアン　カラー　ピーエルシー	カルミン酸および主要中間体の合成
NZ240818A (en) *	1990-12-14	1993-08-26	Mcneil Ppc Inc	Liquid sucralose concentrate compositions containing preservative, buffer and liquid
US7049435B2 (en)	2002-03-08	2006-05-23	Tate & Lyle Public Limited Company	Extractive methods for purifying sucralose
US6998480B2 (en)	2002-03-08	2006-02-14	Tate & Lyle Public Limited Company	Process for improving sucralose purity and yield
US6890581B2 (en) *	2002-04-05	2005-05-10	Tate & Lyle Public Limited Company	Methods for buffer stabilized aqueous deacylation
US20040086605A1 (en) *	2002-10-30	2004-05-06	Sox Thomas E.	Composition for delivering a high intensity sweetener
US6943248B2 (en) *	2003-04-30	2005-09-13	Tate & Lyle Public Limited Company	Crystalline form of sucralose, and method for producing it
US20050196503A1 (en) *	2004-03-05	2005-09-08	Sunil Srivastava	High-intensity sweetener-polyol compositions
US20050214425A1 (en) *	2004-03-23	2005-09-29	Roma Vazirani	Sugar substitute prepared with nutritive and high-intensity sweeteners
CN101098972A (zh) *	2004-12-10	2008-01-02	法马德医疗保险私人有限公司	硅烷化硅胶色谱纯化6-乙酰基-4,1',6'三氯半乳蔗糖和4,1',6'三氯半乳蔗糖的改良方法
WO2006061855A2 (en) *	2004-12-10	2006-06-15	Pharmed Medicare Private Limited	Salts assisted selective extraction of 6-acetyl-4.1', 6' trichlorogalactosucrose and 4, 1 ', 6' trichlorogalactosucrose from aqueous reaction mixture
US20060188629A1 (en) *	2005-01-21	2006-08-24	Greg Liesen	Method for the purification of sucralose
US20100184969A1 (en) *	2005-11-08	2010-07-22	Mangesh Rajadhyaksha	Process to Prepare Sucralose
WO2008004246A1 (en) *	2006-07-06	2008-01-10	Alembic Limited	An improved process for the preparation of sucralose of high purity
US8436156B2 (en) *	2008-01-04	2013-05-07	Tate & Lyle Technology Limited	Method for the production of sucralose
WO2009117317A1 (en) *	2008-03-20	2009-09-24	Tate & Lyle Technology Ltd	Removal of acids from tertiary amide solvents
US8436157B2 (en) *	2008-03-26	2013-05-07	Tate & Lyle Technology Limited	Method for the production of sucralose
US8212022B2 (en) *	2008-04-03	2012-07-03	Tate & Lyle Technology Limited	Effect of carbohydrate concentration on sucralose extraction efficiency
US8497367B2 (en) *	2008-04-03	2013-07-30	Tate & Lyle Technology Limited	Sucralose purification process
AR071134A1 (es) *	2008-04-03	2010-05-26	Tate & Lyle Technology Ltd	Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
WO2009124113A1 (en) *	2008-04-03	2009-10-08	Tate & Lyle Technology Ltd.	Extraction of less polar impurities from sucralose containing aqueous feed streams
US20090299055A1 (en) *	2008-04-03	2009-12-03	Tate & Lyle Technology Limited	Purification of Sucralose Containing Feed Streams for Sucralose Crystallization
GB2474310B (en)	2009-10-12	2012-02-29	Tate & Lyle Technology Ltd	Process for the production of sucrose-6-ester
GB2474311B (en) *	2009-10-12	2012-10-17	Tate & Lyle Technology Ltd	Low temperature, single solvent process for the production of sucrose-6-ester
CN101979396A (zh) *	2010-10-13	2011-02-23	南京甘倍加生物科技有限责任公司	蔗糖-6-酯及三氯蔗糖的合成方法
CN102241708B (zh) *	2011-05-10	2013-10-30	山东大学	一种半乳糖苷化合物及其制备方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS556360B1 (de) *	1968-10-07	1980-02-15
US3795585A (en) *	1972-08-31	1974-03-05	Agency Ind Science Techn	Method for manufacture of alpha-galactosidase
US3867256A (en) *	1974-01-28	1975-02-18	Hokkaido Sugar Co	Method for production of alpha-galactosidase by microorganism
JPS5144651A (en) *	1974-09-28	1976-04-16	Hokkaido Sugar Co	Tensaitoseizo no kairyoho
US3957578A (en) *	1975-01-03	1976-05-18	Hokkaido Sugar Co., Ltd.	Method for manufacture of α-galactosidase by microorganism
CA1138443A (en) *	1979-03-09	1982-12-28	Tate & Lyle Patent Holdings Limited	Process for the preparation of chloro-deoxysugars
DE3062467D1 (en) *	1979-12-20	1983-04-28	Tate & Lyle Plc	Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3165986D1 (en) *	1980-07-08	1984-10-18	Tate & Lyle Plc	Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs)
CA1183133A (en) *	1980-10-28	1985-02-26	Tate & Lyle Public Limited Company	Sweet chlorine-substituted disaccharides
CA1213887A (en) *	1982-09-13	1986-11-12	Riaz A. Khan	Sucrose derivative

1985
- 1985-10-21 GB GB858525871A patent/GB8525871D0/en active Pending
1986
- 1986-10-20 ES ES198686308128T patent/ES2033236T3/es not_active Expired - Lifetime
- 1986-10-20 AU AU64211/86A patent/AU589224B2/en not_active Expired
- 1986-10-20 PT PT83587A patent/PT83587B/pt not_active IP Right Cessation
- 1986-10-20 KR KR1019860008778A patent/KR950005922B1/ko not_active Expired - Lifetime
- 1986-10-20 IE IE276186A patent/IE59482B1/en not_active IP Right Cessation
- 1986-10-20 FI FI864244A patent/FI82836C/fi not_active IP Right Cessation
- 1986-10-20 PH PH34389A patent/PH24621A/en unknown
- 1986-10-20 CA CA000520919A patent/CA1282728C/en not_active Expired - Lifetime
- 1986-10-20 IL IL80365A patent/IL80365A/xx not_active IP Right Cessation
- 1986-10-20 GB GB8625056A patent/GB2181734B/en not_active Expired
- 1986-10-20 SU SU864028456A patent/SU1635905A3/ru active
- 1986-10-20 US US06/921,370 patent/US4826962A/en not_active Expired - Lifetime
- 1986-10-20 EP EP86308128A patent/EP0221717B1/de not_active Expired - Lifetime
- 1986-10-20 DE DE8686308128T patent/DE3683888D1/de not_active Expired - Lifetime
- 1986-10-20 ZA ZA867918A patent/ZA867918B/xx unknown
- 1986-10-20 AT AT86308128T patent/ATE72566T1/de not_active IP Right Cessation
- 1986-10-20 JP JP61249397A patent/JPH0644874B2/ja not_active Expired - Lifetime
- 1986-10-20 DK DK502986A patent/DK164869C/da not_active IP Right Cessation
- 1986-10-20 NZ NZ217998A patent/NZ217998A/xx unknown
- 1986-10-20 NO NO864171A patent/NO168373C/no not_active IP Right Cessation
1992
- 1992-04-08 GR GR920400678T patent/GR3004316T3/el unknown
1993
- 1993-12-01 JP JP5301909A patent/JPH0735391B2/ja not_active Expired - Lifetime

Also Published As

Publication number	Publication date
IL80365A (en)	1990-09-17
JPH0644874B2 (ja)	1994-06-15
ZA867918B (en)	1987-06-24
IE862761L (en)	1987-04-21
FI864244A0 (fi)	1986-10-20
EP0221717A3 (en)	1988-11-30
FI82836C (fi)	1991-04-25
JPH0735391B2 (ja)	1995-04-19
FI82836B (fi)	1991-01-15
CA1282728C (en)	1991-04-09
DK164869B (da)	1992-08-31
GB8625056D0 (en)	1986-11-26
DK502986D0 (da)	1986-10-20
JPH06293787A (ja)	1994-10-21
GR3004316T3 (de)	1993-03-31
FI864244L (fi)	1987-04-22
ES2033236T3 (es)	1993-03-16
NO168373C (no)	1992-02-12
IE59482B1 (en)	1994-03-09
DE3683888D1 (de)	1992-03-26
EP0221717B1 (de)	1992-02-12
NZ217998A (en)	1989-03-29
AU589224B2 (en)	1989-10-05
KR950005922B1 (ko)	1995-06-07
NO864171L (no)	1987-04-22
DK164869C (da)	1993-01-11
JPS62181288A (ja)	1987-08-08
PT83587A (en)	1986-11-01
IL80365A0 (en)	1987-01-30
GB2181734B (en)	1989-09-20
PT83587B (pt)	1988-10-14
EP0221717A2 (de)	1987-05-13
US4826962A (en)	1989-05-02
NO864171D0 (no)	1986-10-20
SU1635905A3 (ru)	1991-03-15
KR870004149A (ko)	1987-05-07
NO168373B (no)	1991-11-04
PH24621A (en)	1990-08-17
DK502986A (da)	1987-04-22
GB8525871D0 (en)	1985-11-27
GB2181734A (en)	1987-04-29
AU6421186A (en)	1987-04-30

Legal Events

Date	Code	Title	Description
1992-11-15	UEP	Publication of translation of european patent specification
2003-07-15	REN	Ceased due to non-payment of the annual fee

Publication	Publication Date	Title
ATE72566T1 (de)	1992-02-15	Tetrachlorraffinose und deren verwendung zur herstellung von sucralose.
DE3783741D1 (de)	1993-03-04	Karrageenan enthaltendes waessriges gel.
SE8404930D0 (sv)	1984-10-02	Aqueous compositions containing stabilized enzymes
FI853618A7 (fi)	1986-03-22	Glukosonin tuotannossa ja muissa entsymaattisissa menetelmissä käyttökelpoisten entsyymien stabilointi.
IT8720338A0 (it)	1987-04-30	Glucosio deidrogenasi e suaproduzione.
NO871707D0 (no)	1987-04-24	Aromastoff, fremstilling av et slikt, samt anvendelse av det.
BR8601461A (pt)	1986-12-09	Processo regulador,com a finalidade de queima na fornalha de soda calcinada,das condicoes de alimentacao ou combustao de solucoes concentradas usadas de composicao quimica e fisica variavel
ES8609157A1 (es)	1986-09-01	Procedimiento para producir tripolifosfato sodico.
ATE39699T1 (de)	1989-01-15	Oxa-fenchylester und -amide von alpha-lasparagins\|ure-d-phenylglycin.
JPS54140743A (en)	1979-11-01	Production of glucose solution with various concentration
DE3665168D1 (en)	1989-09-28	Oculoselective beta blockers
FI863194A0 (fi)	1986-08-05	Foerfarande foer delignifiering av cellulosamaterial.
PH22606A (en)	1988-10-17	New use of 1,4-dihydropyridine derivatives
DE3769407D1 (de)	1991-05-23	Herstellung von eigelblecithin mit niedrigem gehalt an phosphatidyl-aethanolamin und/oder enthaltend keine unreinheiten.
DE3239734A1 (de)	1983-04-07	Extraktion und aufbereitung von fossilen brennstoffen unter verwendung von geschmolzenem alkali und saeureloesungen
FI860307L (fi)	1987-06-12	Produktion av vaeteperoxid.
AU98500S (en)	1987-11-05	Elongate member
AU98480S (en)	1987-11-05	Elongate member
ATE63035T1 (de)	1991-05-15	Stabilisierte wasserstoffperoxydzusammensetzung, deren herstellungsverfahren und verwendung.