BE678545A - - Google Patents

Info

Publication number: BE678545A
Authority: BE; Belgium
Prior art keywords: alkylphenol; sulfide; alcohol; barium; product
Prior art date: 1966-03-28

Application number

BE678545A

Other languages

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1966-03-28

Filing date

1966-03-28

Publication date

1966-09-28

1966-03-28 Application filed filed Critical

1966-03-28 Priority to BE678545A priority Critical patent/BE678545A/fr

1966-09-28 Publication of BE678545A publication Critical patent/BE678545A/fr

Links

238000000034 method Methods 0.000 claims description 28
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 21
229910052751 metal Inorganic materials 0.000 claims description 20
239000002184 metal Substances 0.000 claims description 20
150000003839 salts Chemical class 0.000 claims description 18
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 15
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
150000003568 thioethers Chemical class 0.000 claims description 12
229910052788 barium Inorganic materials 0.000 claims description 11
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 11
GOHYJHLGLUVFQB-UHFFFAOYSA-N 1-nonyl-7-thiabicyclo[4.1.0]hepta-2,4-dien-6-ol Chemical compound C1=CC=CC2(CCCCCCCCC)C1(O)S2 GOHYJHLGLUVFQB-UHFFFAOYSA-N 0.000 claims description 7
238000004519 manufacturing process Methods 0.000 claims description 6
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 4
239000011575 calcium Substances 0.000 claims description 4
229910052791 calcium Inorganic materials 0.000 claims description 4
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 3
ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 2
IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 claims description 2
238000001465 metallisation Methods 0.000 claims description 2
SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 claims description 2
DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims 3
239000003795 chemical substances by application Substances 0.000 claims 3
XENCZPMACKCGLJ-UHFFFAOYSA-N 5,6-dipentyl-7-thiabicyclo[4.1.0]hepta-2,4-dien-1-ol Chemical group C(CCCC)C=1C2(C(C=CC1)(O)S2)CCCCC XENCZPMACKCGLJ-UHFFFAOYSA-N 0.000 claims 1
159000000009 barium salts Chemical group 0.000 claims 1
BQDSDRAVKYTTTH-UHFFFAOYSA-N barium(2+);methanolate Chemical compound [Ba+2].[O-]C.[O-]C BQDSDRAVKYTTTH-UHFFFAOYSA-N 0.000 claims 1
159000000007 calcium salts Chemical group 0.000 claims 1
AMJQWGIYCROUQF-UHFFFAOYSA-N calcium;methanolate Chemical compound [Ca+2].[O-]C.[O-]C AMJQWGIYCROUQF-UHFFFAOYSA-N 0.000 claims 1
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 20
239000000047 product Substances 0.000 description 11
229910002092 carbon dioxide Inorganic materials 0.000 description 10
239000001569 carbon dioxide Substances 0.000 description 8
239000000203 mixture Substances 0.000 description 7
239000003921 oil Substances 0.000 description 7
238000007792 addition Methods 0.000 description 6
239000011541 reaction mixture Substances 0.000 description 6
239000002904 solvent Substances 0.000 description 6
229910044991 metal oxide Inorganic materials 0.000 description 5
150000004706 metal oxides Chemical class 0.000 description 5
239000000376 reactant Substances 0.000 description 5
239000002480 mineral oil Substances 0.000 description 4
235000010446 mineral oil Nutrition 0.000 description 4
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
150000001298 alcohols Chemical class 0.000 description 3
150000004703 alkoxides Chemical class 0.000 description 3
238000001914 filtration Methods 0.000 description 3
-1 hexylphenol sulfide Chemical compound 0.000 description 3
239000011593 sulfur Substances 0.000 description 3
229910052717 sulfur Inorganic materials 0.000 description 3
LJKQIQSBHFNMDV-UHFFFAOYSA-N 7-thiabicyclo[4.1.0]hepta-2,4-dien-6-ol Chemical class C1=CC=CC2(O)C1S2 LJKQIQSBHFNMDV-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 2
239000012467 final product Substances 0.000 description 2
150000002739 metals Chemical class 0.000 description 2
238000010992 reflux Methods 0.000 description 2
RRBIXDPHTCZGGW-UHFFFAOYSA-N 1-decyl-7-thiabicyclo[4.1.0]hepta-2,4-dien-6-ol Chemical compound C1=CC=CC2(CCCCCCCCCC)C1(O)S2 RRBIXDPHTCZGGW-UHFFFAOYSA-N 0.000 description 1
AJPMQQSNPDNRBL-UHFFFAOYSA-N 1-dodecyl-7-thiabicyclo[4.1.0]hepta-2,4-dien-6-ol Chemical compound C1=CC=CC2(CCCCCCCCCCCC)C1(O)S2 AJPMQQSNPDNRBL-UHFFFAOYSA-N 0.000 description 1
KFZMGEQAYNKOFK-UHFFFAOYSA-N 2-propanol Substances CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 1
KSTKJODKCKNREW-UHFFFAOYSA-N 5,6-di(nonyl)-7-thiabicyclo[4.1.0]hepta-2,4-dien-1-ol Chemical compound CCCCCCCCCC1=CC=CC2(O)SC12CCCCCCCCC KSTKJODKCKNREW-UHFFFAOYSA-N 0.000 description 1
JSGINBPBKJWIHS-UHFFFAOYSA-N 6-octadecyl-7-thiabicyclo[4.1.0]hepta-2,4-dien-1-ol Chemical compound C(CCCCCCCCCCCCCCCCC)C12C(C=CC=C1)(O)S2 JSGINBPBKJWIHS-UHFFFAOYSA-N 0.000 description 1
239000004215 Carbon black (E152) Substances 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
238000009835 boiling Methods 0.000 description 1
125000004432 carbon atom Chemical group C* 0.000 description 1
150000005323 carbonate salts Chemical class 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000001816 cooling Methods 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
239000003599 detergent Substances 0.000 description 1
239000002270 dispersing agent Substances 0.000 description 1
238000004821 distillation Methods 0.000 description 1
PXJJSXABGXMUSU-UHFFFAOYSA-N disulfur dichloride Chemical compound ClSSCl PXJJSXABGXMUSU-UHFFFAOYSA-N 0.000 description 1
230000000694 effects Effects 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
239000010687 lubricating oil Substances 0.000 description 1
239000011777 magnesium Substances 0.000 description 1
229910052749 magnesium Inorganic materials 0.000 description 1
239000000463 material Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
239000010688 mineral lubricating oil Substances 0.000 description 1
239000003208 petroleum Substances 0.000 description 1
150000002989 phenols Chemical class 0.000 description 1
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
239000011734 sodium Substances 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
238000003756 stirring Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/003—Compounds containing elements of Groups 2 or 12 of the Periodic Table without C-Metal linkages

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)

BE678545A 1966-03-28 1966-03-28 BE678545A (de)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
BE678545A BE678545A (de)	1966-03-28	1966-03-28

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
BE678545A BE678545A (de)	1966-03-28	1966-03-28

Publications (1)

Publication Number	Publication Date
BE678545A true BE678545A (de)	1966-09-28

Family

ID=3848394

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
BE678545A BE678545A (de)	1966-03-28	1966-03-28

Country Status (1)

Country	Link
BE (1)	BE678545A (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2382440A1 (fr) *	1977-01-28	1978-09-29	Exxon Research Engineering Co	Procede d'obtention de phenates metalliques, notamment de phenates de calcium

1966
- 1966-03-28 BE BE678545A patent/BE678545A/fr unknown

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2382440A1 (fr) *	1977-01-28	1978-09-29	Exxon Research Engineering Co	Procede d'obtention de phenates metalliques, notamment de phenates de calcium

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