BE901329A - Procede de purification de l'acide phosphorique de voie humide par elimination du cadmium. - Google Patents

Procede de purification de l'acide phosphorique de voie humide par elimination du cadmium.

Info

Publication number
BE901329A
BE901329A BE0/214201A BE214201A BE901329A BE 901329 A BE901329 A BE 901329A BE 0/214201 A BE0/214201 A BE 0/214201A BE 214201 A BE214201 A BE 214201A BE 901329 A BE901329 A BE 901329A
Authority
BE
Belgium
Prior art keywords
cadmium
phosphoric acid
removal
purification
wet phosphoric
Prior art date
Application number
BE0/214201A
Other languages
English (en)
Original Assignee
Pechiney Uranium
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pechiney Uranium filed Critical Pechiney Uranium
Publication of BE901329A publication Critical patent/BE901329A/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/234—Purification; Stabilisation; Concentration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/234—Purification; Stabilisation; Concentration
    • C01B25/237—Selective elimination of impurities
    • C01B25/238—Cationic impurities, e.g. arsenic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00—Flotation
    • B03D1/001—Flotation agents
    • B03D1/004—Organic compounds
    • B03D1/014—Organic compounds containing phosphorus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00—Flotation
    • B03D1/02—Froth-flotation processes
    • B03D1/021—Froth-flotation processes for treatment of phosphate ores
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D2201/00—Specified effects produced by the flotation agents
    • B03D2201/02—Collectors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D2203/00—Specified materials treated by the flotation agents; Specified applications
    • B03D2203/02—Ores
    • B03D2203/04—Non-sulfide ores
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/09—Reaction techniques
    • Y10S423/14—Ion exchange; chelation or liquid/liquid ion extraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Processing Of Solid Wastes (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)

Abstract

Procédé d'élimination du cadmium contenu dans l'acide phosphorique de voie humide par flottation au moyen d'un agent tensioactif anionique collecteur du cadmium et d'un gaz injecté, en présence d'autres impuretés dont le fer et éventuellement de l'uranium qui se caractérise en ce que dans le but d'améliorer l'élimination du cadmium, on effectue la réduction du fer contenu dans l'acide phosphorique à l'état trivalent pour la conduire à l'état divalent avant d'introduire le collecteur du cadmium dans le milieu à purifier par flottation. L'agent collecteur est choisi dans le groupe des acides esters dithiophosphoriques ou de leurs sels alcalins.
BE0/214201A 1983-12-23 1984-12-20 Procede de purification de l'acide phosphorique de voie humide par elimination du cadmium. BE901329A (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR8321039A FR2557090B1 (fr) 1983-12-23 1983-12-23 Procede de purification de l'acide phosphorique de voie humide par elimination du cadmium

Publications (1)

Publication Number Publication Date
BE901329A true BE901329A (fr) 1985-06-20

Family

ID=9295717

Family Applications (1)

Application Number Title Priority Date Filing Date
BE0/214201A BE901329A (fr) 1983-12-23 1984-12-20 Procede de purification de l'acide phosphorique de voie humide par elimination du cadmium.

Country Status (9)

Country Link
US (1) US4634580A (fr)
JP (1) JPS60155514A (fr)
KR (1) KR900000080B1 (fr)
BE (1) BE901329A (fr)
FR (1) FR2557090B1 (fr)
JO (1) JO1350B1 (fr)
MA (1) MA20300A1 (fr)
NL (1) NL8403788A (fr)
OA (1) OA07898A (fr)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2574002B1 (fr) * 1984-11-30 1987-02-27 Inst Nat Rech Chimique Perfectionnement apporte a la separation et a la recuperation de solides a partir de liquides les contenant et faisant appel au procede de flottation ionique, et moyen pour la mise en oeuvre de ce perfectionnement
NO164768C (no) * 1988-03-04 1990-11-14 Norsk Hydro As Fremgangsmaate for fjerning av tungmetaller, spesielt kadmium, fra fosforsyreholdige loesninger.
US5378262A (en) * 1994-03-22 1995-01-03 Inco Limited Process for the extraction and separation of nickel and/or cobalt
BRPI0916382A2 (pt) 2008-07-31 2018-06-05 Urtek Llc extração de urânio do ácido fosfórico de processo hidrometalúrgico
US8883096B2 (en) 2008-07-31 2014-11-11 Urtek, Llc Extraction of uranium from wet-process phosphoric acid
CN103949352B (zh) * 2014-05-06 2017-01-11 云南磷化集团有限公司 一种含磷渣酸用于磷矿浮选调整剂的方法
CN105366654B (zh) * 2015-12-02 2017-07-28 云南磷化集团有限公司 一种非磷酸盐沉淀湿法磷酸净化方法
WO2021035058A1 (fr) * 2019-08-21 2021-02-25 Jesa Technologies Llc Procédé d'élimination de cadmium dans la préparation d'acide phosphorique
HRP20240928T1 (hr) * 2020-06-16 2024-10-11 Yara International Asa Postupak uklanjanja teških metala iz sastava koji sadrži fosfornu kiselinu korištenjem ionskog polimernog surfaktanta i upotreba navedenog surfaktanta u talošenju teških metala u sastavu koji sadrži fosfornu kiselinu
CN115427164A (zh) 2020-06-16 2022-12-02 雅苒国际集团 使用絮凝剂从含磷酸组合物中去除重金属的方法
US12545583B2 (en) 2020-06-16 2026-02-10 Yara International Asa Process for the removal of heavy metals from a phosphoric acid containing composition
EP3925710A1 (fr) 2020-06-16 2021-12-22 Yara International ASA Procédé de traitement de compositions dangereuses solides contenant des métaux lourds
KR102721153B1 (ko) * 2023-07-27 2024-10-22 에스케이에코플랜트(주) 사용후 리튬이온배터리로부터 니켈, 코발트, 망간 및 리튬 회수를 위한 분지형 방향족 치환체를 가진 다이싸이오포스페이트 추출제, 이의 제조방법 및 이를 이용한 추출방법
KR102920554B1 (ko) * 2023-10-10 2026-01-29 에스케이에코플랜트(주) 사용후 리튬이온배터리로부터 금속 회수를 위한 유기 추출제, 이의 제조방법 및 이를 이용한 추출방법
CN120864455A (zh) * 2025-08-08 2025-10-31 湖北富邦科技股份有限公司 一种除镉助剂及制备方法和应用

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR665179A (fr) * 1928-05-08 1929-09-16 American Cyanamid Co Perfectionnements apportés aux agents de flottation
US2266514A (en) * 1938-09-09 1941-12-16 American Cyanamid Co Esters of dithiophosphoric acids
US2288752A (en) * 1939-05-17 1942-07-07 Gen Chemical Corp Purification of phosphoric acid
US2789879A (en) * 1950-11-15 1957-04-23 Kaufman David Recovery of uranium from phosphoric acid
FR1472624A (fr) * 1965-03-25 1967-03-10 Monsanto Co Procédé de purification de l'acide phosphorique pour éliminer le fer et nouveau produit purifié ainsi obtenu
FI50715C (fi) * 1973-02-26 1976-06-10 Outokumpu Oy Tapa ja laite erottaa veteen liuenneita aineita toisistaan sementointi aineella.
US4374805A (en) * 1978-05-26 1983-02-22 Uranium Recovery Corporation Reductants for reducing metals in acid media
DE3022662A1 (de) * 1980-06-18 1982-01-21 Hoechst Ag, 6000 Frankfurt Verfahren zur reduktion dreiwertigen eisens in nassverfahrensphosphorsaeure
US4397820A (en) * 1980-07-24 1983-08-09 Wyoming Mineral Corporation Method to maintain a high Fe+2 /Fe+3 ratio in the stripping system for the recovery of uranium from wet process phosphoric acid
DE3045645A1 (de) * 1980-12-04 1982-07-22 Hoechst Ag, 6000 Frankfurt Verfahren zur reduktion von eisen in phospharsaurer loesung
DE3127900A1 (de) * 1981-07-15 1983-02-03 Hoechst Ag, 6000 Frankfurt Verfahren zur extraktion von schwermetallionen aus waessrigen loesungen
DE3135801A1 (de) * 1981-09-10 1983-03-24 Hoechst Ag, 6000 Frankfurt Verfahren zur nachbehandlung von extraktionsrueckstaenden der phosphorsaeurereinigung
DE3202658A1 (de) * 1982-01-28 1983-08-04 Hoechst Ag, 6230 Frankfurt Verfahren zur entfernung von schwermetallionen aus nassverfahrensphosphorsaeure
IL69100A (en) * 1982-07-21 1986-11-30 Hoechst Ag Process for removing heavy metal ions and arsenic from wet-processed phosphoric acid

Also Published As

Publication number Publication date
FR2557090A1 (fr) 1985-06-28
JPS6357363B2 (fr) 1988-11-11
FR2557090B1 (fr) 1986-04-11
KR850004441A (ko) 1985-07-15
KR900000080B1 (ko) 1990-01-19
MA20300A1 (fr) 1985-07-01
JPS60155514A (ja) 1985-08-15
US4634580A (en) 1987-01-06
OA07898A (fr) 1986-11-20
NL8403788A (nl) 1985-07-16
JO1350B1 (en) 1986-11-30

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Legal Events

Date Code Title Description
RE Patent lapsed

Owner name: S.A. URANIUM PECHINEY

Effective date: 19951231