BG101573A - Метод и устроиство за получаване на капролактам чрез хидролитично разграждане на стопен поликапролактам - Google Patents

Метод и устроиство за получаване на капролактам чрез хидролитично разграждане на стопен поликапролактам

Info

Publication number
BG101573A
BG101573A BG101573A BG10157397A BG101573A BG 101573 A BG101573 A BG 101573A BG 101573 A BG101573 A BG 101573A BG 10157397 A BG10157397 A BG 10157397A BG 101573 A BG101573 A BG 101573A
Authority
BG
Bulgaria
Prior art keywords
polymers
water
therepeating
caplolactam
consistingessentially
Prior art date
Application number
BG101573A
Other languages
English (en)
Other versions
BG62929B1 (bg
Inventor
Peter Bassler
Michael Kopietz
Original Assignee
Basf Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=23396923&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BG101573(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Aktiengesellschaft filed Critical Basf Aktiengesellschaft
Publication of BG101573A publication Critical patent/BG101573A/bg
Publication of BG62929B1 publication Critical patent/BG62929B1/bg

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/12—Preparation of lactams by depolymerising polyamides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/62—Plastics recycling; Rubber recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Polyamides (AREA)
  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)

Abstract

Методът включва разграждане на съдържащи капролактам полимери в присъствието на прегрята вода. Полимерите съдържат повтаряща се структурна единица -[-N(H)-(CH2)5-C(O)-]- или смеси, състоящи се по същество от следните компоненти в тегл.%: от 40 до 99,99 полимер с повтаряща се структурна единица -[-N(H)-(CH2)5-C(O)-]-, от 0,01 до 50 добавки, избраниот групата неорганични пълнители, органични и неорганични пигменти и багрила, от 0 до 10 органични и/или неорганични добавки, от 0 до 40 несъдържащи полиамид полимери, от 0 до 60 полиамиди, с изключение на поликапролактам и съполиамиди, произведени на база капролактам. Полимерите или сместа контактуват с прегрята вода при температура от 280 до 3200С и налягане от 7,5 до 15 МРа, тегловно съотношение на водата към посочения полимер с повтаряща се структурна единица от 5:1 до 13:1 и реакционно време под 3 h, при условие, че използваните полимери или сместа не съдържат газообразна фаза, при условията на хидролиза.
BG101573A 1994-12-12 1997-06-05 Метод и устройство за получаване на капролактам чрез хидролитично разграждане на стопен поликапролактам BG62929B1 (bg)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/355,286 US5495015A (en) 1994-12-12 1994-12-12 Process for producing caprolactam through hydrolytic cleavage of molten polycaprolactam
PCT/EP1995/004740 WO1996018613A1 (de) 1994-12-12 1995-12-01 Verfahren zur gewinnung von caprolactam durch hydrolytische spaltung von geschmolzenem polycaprolactam

Publications (2)

Publication Number Publication Date
BG101573A true BG101573A (bg) 1998-01-30
BG62929B1 BG62929B1 (bg) 2000-11-30

Family

ID=23396923

Family Applications (1)

Application Number Title Priority Date Filing Date
BG101573A BG62929B1 (bg) 1994-12-12 1997-06-05 Метод и устройство за получаване на капролактам чрез хидролитично разграждане на стопен поликапролактам

Country Status (19)

Country Link
US (1) US5495015A (bg)
EP (1) EP0797571B1 (bg)
JP (1) JPH10510280A (bg)
KR (1) KR100365454B1 (bg)
CN (1) CN1069313C (bg)
AU (1) AU4300996A (bg)
BG (1) BG62929B1 (bg)
BR (1) BR9510085A (bg)
CA (1) CA2208226C (bg)
CZ (1) CZ288486B6 (bg)
DE (1) DE59505461D1 (bg)
ES (1) ES2129885T3 (bg)
MY (1) MY111917A (bg)
PL (1) PL189334B1 (bg)
RU (1) RU2159233C2 (bg)
SK (1) SK281068B6 (bg)
TW (1) TW356465B (bg)
UA (1) UA51639C2 (bg)
WO (1) WO1996018613A1 (bg)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5681952A (en) * 1995-12-08 1997-10-28 Alliedsignal Inc. Process for depolymerizing nylon-containing waste to form caprolactam
US5948908A (en) * 1996-03-18 1999-09-07 Alliedsignal Inc. Process for depolymerizing polycaprolactam processing waste to form caprolactam
NL1005942C2 (nl) * 1997-05-01 1998-11-03 Dsm Nv Depolymeriseren van polyamiden.
US5990306A (en) 1997-09-03 1999-11-23 Alliedsignal Inc. Process for the purification of caprolactam obtained from the depolymerization of polyamide-containing carpet
US7934393B2 (en) * 2007-06-05 2011-05-03 Johns Nanville Process for recycling glass fiber
CN101423623B (zh) * 2007-11-02 2011-05-11 宁波大学 一种耐高温尼龙聚对苯二甲酰己二胺的解聚回收方法
ES2417854T3 (es) 2009-05-20 2013-08-09 Nestec S.A. Tapón dispensador
WO2013010934A1 (en) 2011-07-21 2013-01-24 Nestec S.A. Cup or mug cover
DE102018220616B3 (de) * 2018-11-20 2019-05-29 Thyssenkrupp Ag Verfahren zur Herstellung von Polyamid 6
JP7425539B2 (ja) * 2019-04-12 2024-01-31 マクセル株式会社 熱可塑性樹脂の水熱分解方法
IL303644A (en) 2020-12-17 2023-08-01 Basf Se Selective depolymerization of polyamide 6 to obtain caprolactam from mixtures of caprolactam-containing polymers and polyurethane-containing polymers, especially polyurethane block copolymers
JP7855316B2 (ja) * 2021-03-18 2026-05-08 本田技研工業株式会社 加水分解連続処理装置
WO2023074432A1 (ja) 2021-10-29 2023-05-04 東レ株式会社 ε－カプロラクタムの製造方法およびポリアミド６の製造方法
WO2023074437A1 (ja) 2021-10-29 2023-05-04 東レ株式会社 ε－カプロラクタムおよびポリアミド６オリゴマーの回収方法、ならびにポリアミド６の製造方法
EP4424758A4 (en) * 2021-10-29 2026-02-11 Toray Industries PROCESS FOR THERMOPLASTIC RESIN PRODUCTION
WO2023074433A1 (ja) 2021-10-29 2023-05-04 東レ株式会社 繊維状充填材およびε－カプロラクタムの回収方法、ならびにポリアミド６の製造方法
WO2023074441A1 (ja) 2021-10-29 2023-05-04 東レ株式会社 ε－カプロラクタムの製造方法およびポリアミド６の製造方法
JP7433353B2 (ja) * 2022-03-18 2024-02-19 本田技研工業株式会社 樹脂組成物のリサイクル装置
WO2024251758A1 (en) * 2023-06-06 2024-12-12 Basf Se Process for hydrolytically depolymerizing a polyamide

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL6704865A (bg) * 1967-04-05 1968-10-07
US3939153A (en) * 1974-08-09 1976-02-17 Hillyard Chemical Company Process for producing caprolactam
US4311642A (en) * 1980-09-17 1982-01-19 Allied Corporation Recovery of caprolactam from nylon 6 oligomers
US4605762A (en) * 1982-04-23 1986-08-12 Celanese Mexicana S.A. Depolymerization of condensation polymers
US5977193A (en) * 1991-06-21 1999-11-02 Basf Corporation Reclaiming epsilon-caprolactam from nylon 6 carpet
US5294707A (en) * 1993-02-25 1994-03-15 Basf Corporation Semi-continuous depolymerization of nylon 6 polymer
US5457197A (en) * 1994-04-08 1995-10-10 Alliedsignal Inc. Monomer recovery from multi-component materials

Also Published As

Publication number Publication date
CN1169719A (zh) 1998-01-07
DE59505461D1 (de) 1999-04-29
KR100365454B1 (ko) 2003-05-17
WO1996018613A1 (de) 1996-06-20
EP0797571A1 (de) 1997-10-01
JPH10510280A (ja) 1998-10-06
PL189334B1 (pl) 2005-07-29
BR9510085A (pt) 1998-07-14
US5495015A (en) 1996-02-27
PL320593A1 (en) 1997-10-13
ES2129885T3 (es) 1999-06-16
UA51639C2 (uk) 2002-12-16
SK66797A3 (en) 1998-07-08
MY111917A (en) 2001-02-28
EP0797571B1 (de) 1999-03-24
AU4300996A (en) 1996-07-03
RU2159233C2 (ru) 2000-11-20
MX9704285A (es) 1997-09-30
CN1069313C (zh) 2001-08-08
CZ176397A3 (cs) 1998-06-17
BG62929B1 (bg) 2000-11-30
CA2208226C (en) 2005-02-15
SK281068B6 (sk) 2000-11-07
CA2208226A1 (en) 1996-06-20
CZ288486B6 (en) 2001-06-13
TW356465B (en) 1999-04-21

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