BRPI0408007A - processo para a produção de dióxido de cloro - Google Patents

processo para a produção de dióxido de cloro

Info

Publication number
BRPI0408007A
BRPI0408007A BRPI0408007-6A BRPI0408007A BRPI0408007A BR PI0408007 A BRPI0408007 A BR PI0408007A BR PI0408007 A BRPI0408007 A BR PI0408007A BR PI0408007 A BRPI0408007 A BR PI0408007A
Authority
BR
Brazil
Prior art keywords
chlorine dioxide
feed nozzle
reactor
sulfuric acid
present
Prior art date
Application number
BRPI0408007-6A
Other languages
English (en)
Inventor
Thomas Woodruff
James Jefferson
Original Assignee
Akzo Nobel Nv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Akzo Nobel Nv filed Critical Akzo Nobel Nv
Publication of BRPI0408007A publication Critical patent/BRPI0408007A/pt
Publication of BRPI0408007B1 publication Critical patent/BRPI0408007B1/pt

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002—Nozzle-type elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B11/00—Oxides or oxyacids of halogens; Salts thereof
    • C01B11/02—Oxides of chlorine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20—Jet mixers, i.e. mixers using high-speed fluid streams
    • B01F25/23—Mixing by intersecting jets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30—Injector mixers
    • B01F25/31—Injector mixers in conduits or tubes through which the main component flows
    • B01F25/312—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof
    • B01F25/3121—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof with additional mixing means other than injector mixers, e.g. screens, baffles or rotating elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30—Injector mixers
    • B01F25/31—Injector mixers in conduits or tubes through which the main component flows
    • B01F25/312—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof
    • B01F25/3124—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof characterised by the place of introduction of the main flow
    • B01F25/31243—Eductor or eductor-type venturi, i.e. the main flow being injected through the venturi with high speed in the form of a jet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B11/00—Oxides or oxyacids of halogens; Salts thereof
    • C01B11/02—Oxides of chlorine
    • C01B11/022—Chlorine dioxide (ClO2)
    • C01B11/023—Preparation from chlorites or chlorates
    • C01B11/026—Preparation from chlorites or chlorates from chlorate ions in the presence of a peroxidic compound, e.g. hydrogen peroxide, ozone, peroxysulfates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)

Abstract

"PROCESSO PARA A PRODUçãO DE DIóXIDO DE CLORO". A presente invenção se refere a um processo para a produção continuamente de dióxido de cloro. Em concordância com a presente invenção, o referido processo está caracterizado pelo fato de que compreende as etapas de: diluir ácido sulfúrico de uma concentração inicial excedendo cerca de 90 % em peso com água para uma concentração a partir de cerca de 60 % em peso até de cerca de 90 % em peso; trazer o ácido sulfúrico diluído para uma temperatura abaixo de cerca de 100 <198>C; alimentar para um reator (5) o ácido sulfúrico diluído possuindo uma temperatura abaixo de cerca de 100 <198>C através de um primeiro bocal de alimentação (1); alimentar para o referido reator (5) uma solução aquosa compreendendo clorato de metal alcalino e peróxido de hidrogênio através de um segundo bocal de alimentação (2), em que o referido primeiro bocal de alimentação (1) e o referido segundo bocal de alimentação (2) estão opostos um para o outro e direcionados um contra o outro; reagir o clorato de metal alcalino com o ácido mineral e com o peróxido de hidrogênio para formar uma corrente de produto contendo dióxido de cloro; e extrair a corrente de produto a partir do reator (5). A presente invenção adicionalmente se refere a um aparelho utilizável para a produção continuamente de dióxido de cloro.
BRPI0408007-6A 2003-03-03 2004-03-02 Processo para a produção de dióxido de cloro BRPI0408007B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/376,261 2003-03-03
US10/376,261 US20040175322A1 (en) 2003-03-03 2003-03-03 Process for producing chlorine dioxide
PCT/SE2004/000282 WO2004078648A1 (en) 2003-03-03 2004-03-02 Process for producing chlorine dioxide

Publications (2)

Publication Number Publication Date
BRPI0408007A true BRPI0408007A (pt) 2006-02-14
BRPI0408007B1 BRPI0408007B1 (pt) 2014-09-09

Family

ID=32926287

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0408007-6A BRPI0408007B1 (pt) 2003-03-03 2004-03-02 Processo para a produção de dióxido de cloro

Country Status (19)

Country Link
US (1) US20040175322A1 (pt)
EP (1) EP1599416B1 (pt)
JP (1) JP4297910B2 (pt)
KR (1) KR100714529B1 (pt)
CN (1) CN100336716C (pt)
AU (1) AU2004218077B2 (pt)
BR (1) BRPI0408007B1 (pt)
CA (1) CA2517079C (pt)
EC (1) ECSP056021A (pt)
EG (1) EG24120A (pt)
IL (1) IL170075A (pt)
MX (1) MXPA05008509A (pt)
MY (1) MY136184A (pt)
NO (1) NO341210B1 (pt)
RU (1) RU2304558C2 (pt)
TW (1) TWI273089B (pt)
UA (1) UA79867C2 (pt)
WO (1) WO2004078648A1 (pt)
ZA (1) ZA200506201B (pt)

Families Citing this family (42)

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ZA200606282B (en) * 2004-02-23 2007-11-28 Akzo Nobel Nv Process for production of chlorine dioxide
CN100562488C (zh) * 2004-12-06 2009-11-25 阿克佐诺贝尔公司 含二氧化氯的水溶液的生产方法和设备
US20060120946A1 (en) * 2004-12-06 2006-06-08 Akzo Nobel N.V. Chemical process and apparatus
JP4637916B2 (ja) * 2004-12-06 2011-02-23 アクゾ ノーベル ナムローゼ フェンノートシャップ 化学的方法および製造装置
DE602005019778D1 (de) * 2004-12-06 2010-04-15 Akzo Nobel Nv Chemisches verfahren und produktionseinheit
CN101304944A (zh) * 2005-11-10 2008-11-12 阿克佐诺贝尔公司 二氧化氯的制备方法
RU2404118C2 (ru) * 2005-11-10 2010-11-20 Акцо Нобель Н.В. Способ получения диоксида хлора
US8425866B2 (en) * 2005-11-14 2013-04-23 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Control of emissions
KR100738987B1 (ko) * 2006-03-07 2007-07-13 한국해양연구원 선박 밸러스트수 처리를 위한 해수에서의 아염소산염과염소를 이용한 이산화염소 제조 장치 및 방법
CN101421182A (zh) * 2006-04-10 2009-04-29 阿克佐诺贝尔股份有限公司 制备二氧化氯的方法
RU2417946C2 (ru) * 2006-04-10 2011-05-10 Акцо Нобель Н.В. Способ получения диоксида хлора
CA2648673C (en) * 2006-04-10 2018-08-28 Thomas E. Woodruff Process for the production of chlorine dioxide
CN101511192B (zh) 2006-08-28 2013-07-31 本部三庆株式会社 作为杀菌剂使用的含亚氯酸的水溶液的制造方法
MX2009007470A (es) * 2007-01-12 2009-07-22 Akzo Nobel Nv Procedimiento para la produccion de dioxido de cloro.
US8409534B2 (en) * 2007-03-28 2013-04-02 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Control of emissions
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KR101162536B1 (ko) 2009-10-23 2012-07-05 주식회사 에코시아 ＴＨＭｓ등이 생성되지 않는 녹색 친환경 살균소독제인 이산화염소 수용액 제조장치 및 그 제조방법
EP2526047B1 (en) 2010-01-18 2017-08-23 Akzo Nobel Chemicals International B.V. Process for the production of chlorine dioxide
DE102010027840A1 (de) * 2010-04-16 2011-10-20 Infracor Gmbh Tauchreaktor
RU2562997C2 (ru) * 2010-07-08 2015-09-10 Акцо Нобель Кемикалз Интернэшнл Б.В. Способ получения диоксида хлора
JP6283551B2 (ja) * 2014-01-20 2018-02-21 高砂熱学工業株式会社 二酸化塩素ガスの発生装置および発生方法
TWI750330B (zh) 2017-02-27 2021-12-21 美商藝康美國公司 用於現場產生二氧化氯之方法
WO2018175732A1 (en) 2017-03-24 2018-09-27 Ecolab USA, Inc. Low risk chlorine dioxide onsite generation system
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CN109133008B (zh) * 2018-08-23 2020-05-19 四川齐力绿源水处理科技有限公司 一种高纯二氧化氯的制备设备
CN108975277B (zh) * 2018-08-23 2020-10-16 四川齐力绿源水处理科技有限公司 一种高纯二氧化氯的制备方法
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KR102002506B1 (ko) 2019-05-23 2019-07-22 김재우 연속 대량생산이 가능한 이산화염소의 제조방법 및 그 제조장치
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TW202404930A (zh) 2022-04-01 2024-02-01 美商藝康美國公司 在共軛二烯單體之萃取蒸餾期間減少非所要之乳化聚合
TW202348787A (zh) 2022-04-01 2023-12-16 美商藝康美國公司 用於乙烯系單體流之高苛刻度加工的防汙劑組成物
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Also Published As

Publication number Publication date
TWI273089B (en) 2007-02-11
NO341210B1 (no) 2017-09-11
JP4297910B2 (ja) 2009-07-15
KR20050116806A (ko) 2005-12-13
AU2004218077A1 (en) 2004-09-16
JP2006513972A (ja) 2006-04-27
WO2004078648A1 (en) 2004-09-16
EP1599416B1 (en) 2014-10-15
BRPI0408007B1 (pt) 2014-09-09
CA2517079C (en) 2011-03-01
CN1809506A (zh) 2006-07-26
MY136184A (en) 2008-08-29
ZA200506201B (en) 2006-10-25
UA79867C2 (en) 2007-07-25
NO20054543L (no) 2005-10-03
KR100714529B1 (ko) 2007-05-07
EG24120A (en) 2008-07-06
IL170075A (en) 2011-03-31
CA2517079A1 (en) 2004-09-16
RU2005130491A (ru) 2006-01-27
MXPA05008509A (es) 2005-10-20
AU2004218077B2 (en) 2007-06-07
US20040175322A1 (en) 2004-09-09
RU2304558C2 (ru) 2007-08-20
ECSP056021A (es) 2006-01-27
TW200424119A (en) 2004-11-16
CN100336716C (zh) 2007-09-12
EP1599416A1 (en) 2005-11-30

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B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
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B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

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B21A Patent or certificate of addition expired [chapter 21.1 patent gazette]

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