BRPI0508420A - método para remover oxalato de sódio de um licor de bayer e aparelho para o mesmo - Google Patents
método para remover oxalato de sódio de um licor de bayer e aparelho para o mesmoInfo
- Publication number
- BRPI0508420A BRPI0508420A BRPI0508420-2A BRPI0508420A BRPI0508420A BR PI0508420 A BRPI0508420 A BR PI0508420A BR PI0508420 A BRPI0508420 A BR PI0508420A BR PI0508420 A BRPI0508420 A BR PI0508420A
- Authority
- BR
- Brazil
- Prior art keywords
- liquor
- sodium oxalate
- bayer
- recycled
- bayer liquor
- Prior art date
Links
- ZNCPFRVNHGOPAG-UHFFFAOYSA-L sodium oxalate Chemical compound [Na+].[Na+].[O-]C(=O)C([O-])=O ZNCPFRVNHGOPAG-UHFFFAOYSA-L 0.000 title abstract 4
- 229940039790 sodium oxalate Drugs 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 2
- 239000013078 crystal Substances 0.000 abstract 2
- 238000004131 Bayer process Methods 0.000 abstract 1
- 229910001570 bauxite Inorganic materials 0.000 abstract 1
- 239000003518 caustics Substances 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 150000002894 organic compounds Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/46—Purification of aluminium oxide, aluminium hydroxide or aluminates
- C01F7/47—Purification of aluminium oxide, aluminium hydroxide or aluminates of aluminates, e.g. removal of compounds of Si, Fe, Ga or of organic compounds from Bayer process liquors
- C01F7/473—Removal of organic compounds, e.g. sodium oxalate
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0018—Evaporation of components of the mixture to be separated
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Thermal Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Treatment Of Sludge (AREA)
- Physical Water Treatments (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
MéTODO PARA REMOVER OXALATO DE SóDIO DE UM LICOR DE BAYER E APARELHO PARA O MESMO. O processo Bayer usa solução de hidróxido de sódio quente para obter alumina pura a partir de minério bauxita. Alumina dissolve, sendo então precipitada, e o licor de Bayer cáustico restante pode ser reciclado para uso novamente. No entanto, oxalato de sódio tende a se acumular no licor reciclado e causar problemas. Ao remover uma corrente do licor, tratando o mesmo de modo a ficar supersaturado com oxalato de sódio, e então submeter o mesmo à irradiação ultra-sónica, são formados núcleos de cristal. Os cristais resultantes podem ser então separados do licor. De forma surpreendente, outros compostos orgânicos em solução não impedem que este processo de cristalização seja eficaz.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GBGB0405108.2A GB0405108D0 (en) | 2004-03-06 | 2004-03-06 | Removal of sodium oxalate from a bayer liquor |
| PCT/GB2005/000812 WO2005085136A1 (en) | 2004-03-06 | 2005-03-03 | Removal of sodium oxalate from a bayer liquor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BRPI0508420A true BRPI0508420A (pt) | 2007-07-24 |
Family
ID=32088862
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0508420-2A BRPI0508420A (pt) | 2004-03-06 | 2005-03-03 | método para remover oxalato de sódio de um licor de bayer e aparelho para o mesmo |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US20090087360A1 (pt) |
| EP (1) | EP1723077B1 (pt) |
| JP (1) | JP2007527355A (pt) |
| CN (1) | CN100548885C (pt) |
| AP (1) | AP2006003749A0 (pt) |
| AT (1) | ATE368633T1 (pt) |
| AU (1) | AU2005219639B2 (pt) |
| BR (1) | BRPI0508420A (pt) |
| CA (1) | CA2556665A1 (pt) |
| DE (1) | DE602005001855T2 (pt) |
| ES (1) | ES2287907T3 (pt) |
| GB (1) | GB0405108D0 (pt) |
| RU (1) | RU2006135229A (pt) |
| WO (1) | WO2005085136A1 (pt) |
| ZA (1) | ZA200606787B (pt) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB0524823D0 (en) * | 2005-12-06 | 2006-01-11 | Accentus Plc | Removal of contaminants from a bayer liquor |
| WO2008144838A1 (en) * | 2007-05-31 | 2008-12-04 | Commonwealth Scientific And Industrial Research Organisation | Method for treating residue from a bayer process |
| CN101462114B (zh) * | 2007-12-17 | 2010-10-13 | 贵阳铝镁设计研究院 | 一种氧化铝生产中换热器中草酸钠结晶的处理方法 |
| RU2375307C1 (ru) * | 2008-04-14 | 2009-12-10 | Открытое акционерное общество "РУСАЛ Всероссийский Алюминиево-магниевый Институт" | Способ получения глинозема из боксита |
| CN101575111B (zh) * | 2008-05-08 | 2011-04-06 | 沈阳铝镁设计研究院 | 一种铝酸钠溶液中草酸盐的去除系统及方法 |
| RU2375308C1 (ru) * | 2008-07-14 | 2009-12-10 | Открытое акционерное общество "РУСАЛ Всероссийский Алюминиево-магниевый Институт" | Способ получения глинозема из боксита |
| CN105480994B (zh) * | 2014-09-18 | 2017-05-10 | 沈阳铝镁设计研究院有限公司 | 一种高效的细种子洗涤富集草酸盐的方法 |
| FI20146163A7 (fi) * | 2014-12-30 | 2016-07-01 | Lappeenrannan Teknillinen Yliopisto | Menetelmä ja laite jatkuvatoimiseen kiteytykseen ja niiden käyttö |
| DE102016008296B4 (de) * | 2016-07-05 | 2020-02-20 | Technische Universität Bergakademie Freiberg | Verfahren und Vorrichtung zur Sonokristallisation |
| CN111905398A (zh) * | 2020-06-26 | 2020-11-10 | 中国轻工业长沙工程有限公司 | 一种连续结晶生产镍钴盐、铵盐的工艺 |
| CN112299461B (zh) * | 2020-11-08 | 2023-03-24 | 湖南诺兰蒂尔环保科技有限公司 | 一种铝酸钠溶液中草酸盐排除装置及工艺 |
| CN114655972B (zh) * | 2022-04-27 | 2023-10-27 | 云南省生态环境科学研究院 | 拜耳法氧化铝溶液有机物高效脱除的方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS53400B2 (pt) * | 1972-12-06 | 1978-01-07 | ||
| ZA728668B (en) * | 1972-12-07 | 1974-07-31 | African Explosives & Chem | Improvements in the manufacture of safety fuse |
| US4275042A (en) * | 1980-01-22 | 1981-06-23 | Alcan Research And Development Limited | Removal of oxalate from Bayer process liquor |
| GB2306202B (en) * | 1995-10-05 | 1999-04-14 | British Nuclear Fuels Plc | An ultrasonic apparatus |
| GB9827360D0 (en) * | 1998-12-12 | 1999-02-03 | Aea Technology Plc | Process and apparatus for irradiating fluids |
| AUPP933499A0 (en) * | 1999-03-19 | 1999-04-15 | Worsley Alumina Pty Ltd | Process for the removal of oxalate and/or sulphate from bayer liquors |
| BR0209433A (pt) * | 2001-05-05 | 2004-08-03 | Accentus Plc | Método para realizar cristalização, e, aparelho |
| US7357835B2 (en) * | 2002-05-31 | 2008-04-15 | Accentus Plc | Production of crystalline materials by using high intensity ultrasound |
-
2004
- 2004-03-06 GB GBGB0405108.2A patent/GB0405108D0/en not_active Ceased
-
2005
- 2005-03-03 EP EP05717890A patent/EP1723077B1/en not_active Expired - Lifetime
- 2005-03-03 CN CNB2005800070662A patent/CN100548885C/zh not_active Expired - Fee Related
- 2005-03-03 RU RU2006135229/15A patent/RU2006135229A/ru not_active Application Discontinuation
- 2005-03-03 US US10/591,795 patent/US20090087360A1/en not_active Abandoned
- 2005-03-03 BR BRPI0508420-2A patent/BRPI0508420A/pt not_active IP Right Cessation
- 2005-03-03 AP AP2006003749A patent/AP2006003749A0/xx unknown
- 2005-03-03 ES ES05717890T patent/ES2287907T3/es not_active Expired - Lifetime
- 2005-03-03 ZA ZA200606787A patent/ZA200606787B/xx unknown
- 2005-03-03 CA CA002556665A patent/CA2556665A1/en not_active Abandoned
- 2005-03-03 WO PCT/GB2005/000812 patent/WO2005085136A1/en not_active Ceased
- 2005-03-03 AT AT05717890T patent/ATE368633T1/de not_active IP Right Cessation
- 2005-03-03 JP JP2007501350A patent/JP2007527355A/ja active Pending
- 2005-03-03 DE DE602005001855T patent/DE602005001855T2/de not_active Expired - Lifetime
- 2005-03-03 AU AU2005219639A patent/AU2005219639B2/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| US20090087360A1 (en) | 2009-04-02 |
| DE602005001855T2 (de) | 2008-04-10 |
| DE602005001855D1 (de) | 2007-09-13 |
| EP1723077A1 (en) | 2006-11-22 |
| WO2005085136A1 (en) | 2005-09-15 |
| GB0405108D0 (en) | 2004-04-07 |
| AU2005219639A1 (en) | 2005-09-15 |
| EP1723077B1 (en) | 2007-08-01 |
| AU2005219639B2 (en) | 2011-01-20 |
| ES2287907T3 (es) | 2007-12-16 |
| CN100548885C (zh) | 2009-10-14 |
| ATE368633T1 (de) | 2007-08-15 |
| CA2556665A1 (en) | 2005-09-15 |
| JP2007527355A (ja) | 2007-09-27 |
| CN1930086A (zh) | 2007-03-14 |
| ZA200606787B (en) | 2007-12-27 |
| RU2006135229A (ru) | 2008-04-20 |
| AP2006003749A0 (en) | 2006-10-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B25G | Requested change of headquarter approved |
Owner name: ACCENTUS PLC (GB) Free format text: ANOTADAS AS ALTERACOES DE SEDE SOLICITADAS ATRAVES DA PETICAO NO 020070184946/RJ DE 28/12/2007. |
|
| B25A | Requested transfer of rights approved |
Owner name: PROSONIX LIMITED (GB) Free format text: TRANSFERIDO DE: ACCENTUS PLC |
|
| B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 9A ANUIDADE. |
|
| B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 2260 DE 29/04/2014. |