BRPI0512665A - processo aprimorado para a extração por solvente de polihidroxialcanoatos de biomassa - Google Patents

processo aprimorado para a extração por solvente de polihidroxialcanoatos de biomassa

Info

Publication number
BRPI0512665A
BRPI0512665A BRPI0512665-7A BRPI0512665A BRPI0512665A BR PI0512665 A BRPI0512665 A BR PI0512665A BR PI0512665 A BRPI0512665 A BR PI0512665A BR PI0512665 A BRPI0512665 A BR PI0512665A
Authority
BR
Brazil
Prior art keywords
liquor
biomass
polyhydroxyalkanoate
water
pha
Prior art date
Application number
BRPI0512665-7A
Other languages
English (en)
Inventor
Karunakaran Narasimhan
Angella C Cearley
Michael Steven Gibson
Stanley James Welling
Original Assignee
Procter & Gamble
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=35159733&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BRPI0512665(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Procter & Gamble filed Critical Procter & Gamble
Publication of BRPI0512665A publication Critical patent/BRPI0512665A/pt

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0288—Applications, solvents
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/88—Post-polymerisation treatment
    • C08G63/89—Recovery of the polymer
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/06—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from hydroxycarboxylic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Biological Depolymerization Polymers (AREA)

Abstract

PROCESSO APRIMORADO PARA A EXTRAçãO POR SOLVENTE DE POLIHIDROXIALCANOATOS DE BIOMASSA Processos aprimorados para a extração de polihidroxialcanoato de uma biomassa seca que contém o polihidroxialcanoato, que compreende as etapas de: combinar a biomassa que contém o polihidroxialcanoato com um solvente selecionado entre cetonas de cadeia inferior e misturas destas cetonas para formar um licor de biomassa que compreende menos de cerca de 25 % de água; misturar o licor de biomassa com cerca de 10 a cerca de 300 minutos a uma temperatura na faixa de cerca de 70<198>C a cerca de 120<198>C; separar o polihidroxialcanoato do licor de biomassa para formar um licor rico em PHA, sendo que a separação ocorre a uma temperatura de pelo menos cerca de 40<198>C; misturar o licor rico em PHA com água para formar um polihidroxialcanoato precipitado e um licor de solvente impuro, sendo que a água é misturada com o licor rico em PHA à razão de cerca de 3 partes de água para uma parte de polihidroxialcanoato; e recuperar o polihidroxialcanoato precipitado do licor de solvente impuro. O tratamento opcional com agentes oxidantes ou com tensoativos suaves ou com alvejantes suaves é usado para melhorar a cor e o odor.
BRPI0512665-7A 2004-06-29 2005-06-29 processo aprimorado para a extração por solvente de polihidroxialcanoatos de biomassa BRPI0512665A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US58377304P 2004-06-29 2004-06-29
PCT/US2005/023221 WO2006004895A1 (en) 2004-06-29 2005-06-29 Improved process for the solvent-based extraction of polyhydroxyalkanoates from biomass

Publications (1)

Publication Number Publication Date
BRPI0512665A true BRPI0512665A (pt) 2008-04-01

Family

ID=35159733

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0512665-7A BRPI0512665A (pt) 2004-06-29 2005-06-29 processo aprimorado para a extração por solvente de polihidroxialcanoatos de biomassa

Country Status (11)

Country Link
US (1) US7378266B2 (pt)
EP (1) EP1781721B2 (pt)
JP (1) JP2008504035A (pt)
CN (1) CN1976973B (pt)
AT (1) ATE425201T1 (pt)
BR (1) BRPI0512665A (pt)
CA (1) CA2571118A1 (pt)
DE (1) DE602005013242D1 (pt)
MX (1) MXPA06015089A (pt)
TW (1) TW200617171A (pt)
WO (1) WO2006004895A1 (pt)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2579721C (en) * 2004-09-13 2012-11-27 Metabolix, Inc. Single solvent polymer extraction methods
CA2599467A1 (en) 2005-02-17 2006-08-24 The Procter & Gamble Company Fabric care composition
CN101024498A (zh) * 2006-02-21 2007-08-29 秦才东 无水钠或钾的硅酸盐的生产方法
JP2008189861A (ja) * 2007-02-07 2008-08-21 Tosoh Corp 色調に優れるポリ３−ヒドロキシブチレート系重合体及びポリ３−ヒドロキシブチレート系重合体の精製方法
US8016980B2 (en) 2008-11-25 2011-09-13 Dixie Consumer Products Llc Paper products
CN101980222B (zh) * 2010-11-03 2013-12-25 北京航空航天大学 一种基于拓扑优化的仿蜘蛛网夹层筋板复合结构设计方法
RU2014106676A (ru) * 2011-07-22 2015-08-27 Торэй Индастриз, Инк. Способ производства органической кислоты
ES2448823B1 (es) 2012-08-14 2014-10-13 Neol Biosolutions, S.A. Producción de bioplásticos
WO2016081902A1 (en) 2014-11-20 2016-05-26 Full Cycle Bioplastics Inc. Producing polyhydroxyalkanoate copolymers from organic waste products
JP6993980B2 (ja) * 2016-10-13 2022-02-04 株式会社カネカ ポリヒドロキシアルカン酸の製造方法
TWI717569B (zh) 2017-11-02 2021-02-01 國立暨南國際大學 萃取聚羥基烷基酸酯(PHAs)之方法
CN111019108B (zh) * 2020-01-07 2021-03-05 清华大学 一种提取并纯化聚羟基脂肪酸酯的方法
KR102905824B1 (ko) * 2022-04-26 2025-12-31 주식회사 윤바이오테크 폴리 하이드록시 알카노에이트의 생산 방법
CN116144046B (zh) * 2022-06-06 2024-01-23 北京蓝晶微生物科技有限公司 一种聚羟基脂肪酸酯凝集体的制备方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4140741A (en) * 1976-01-14 1979-02-20 Agroferm A.G. Use of cyclic carbonic acid esters as solvents for poly-(β-hydroxybutyric acid)
US4324907A (en) * 1979-05-08 1982-04-13 Imperial Chemical Industries Limited Extraction process
GB8311677D0 (en) * 1983-04-28 1983-06-02 Ici Plc Extraction process
GB9416690D0 (en) * 1994-08-18 1994-10-12 Zeneca Ltd Process for the recovery of polyhydroxyalkanoic acid
ES2177796T3 (es) † 1995-08-21 2002-12-16 Procter & Gamble Extraccion por disolvente de polihidroxialcanoatos a partir de biomasafacilitada por el uso de un no disolvente marginal para pha.
US5942597A (en) * 1995-08-21 1999-08-24 The Procter & Gamble Company Solvent extraction of polyhydroxyalkanoates from biomass
JPH09191893A (ja) 1996-01-22 1997-07-29 Taisei Corp ヒドロキシアルカン酸共重合体の製造方法
US5821299A (en) † 1996-02-16 1998-10-13 The Proctor & Gamble Company Solvent extraction of polyhydroxy-alkanoates from biomass facilitated by the use of marginal nonsolvent
AU6974398A (en) * 1997-04-15 1998-11-11 Monsanto Company High temperature pha extraction using pha-poor solvents
WO1998046782A1 (en) * 1997-04-15 1998-10-22 Monsanto Company Methods of pha extraction and recovery using non-halogenated solvents
EP0981381B1 (en) † 1997-05-12 2007-02-21 Metabolix, Inc. Polyhydroxyalkanoates for in vivo applications
JP4790912B2 (ja) * 1999-05-12 2011-10-12 メタボリックス，インコーポレイテッド ポリヒドロキシアルカノエートを精製するための方法
DE19955381C1 (de) * 1999-11-10 2001-02-22 Ufz Leipzighalle Gmbh Verfahren zur Gewinnung eines Homo- oder Copolymers einer Poly-ß-hydroxyalkansäure (PHA) aus Biomasse
CN102443159B (zh) * 2002-08-06 2015-04-08 梅塔博利克斯股份有限公司 聚合物的萃取方法

Also Published As

Publication number Publication date
US20050287654A1 (en) 2005-12-29
US7378266B2 (en) 2008-05-27
CN1976973A (zh) 2007-06-06
WO2006004895A1 (en) 2006-01-12
MXPA06015089A (es) 2007-03-01
DE602005013242D1 (de) 2009-04-23
EP1781721A1 (en) 2007-05-09
EP1781721B1 (en) 2009-03-11
EP1781721B2 (en) 2012-12-26
ATE425201T1 (de) 2009-03-15
JP2008504035A (ja) 2008-02-14
CN1976973B (zh) 2010-11-10
TW200617171A (en) 2006-06-01
CA2571118A1 (en) 2006-01-12

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Legal Events

Date Code Title Description
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]

Free format text: REFERENTE AS 5A, 6A E 7A ANUIDADES.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 2158 DE 15/05/2012.