BRPI0513548A - processos de recuperação de amÈnia a partir de fluxo de vapor e de efluente de reator - Google Patents

processos de recuperação de amÈnia a partir de fluxo de vapor e de efluente de reator

Info

Publication number
BRPI0513548A
BRPI0513548A BRPI0513548-6A BRPI0513548A BRPI0513548A BR PI0513548 A BRPI0513548 A BR PI0513548A BR PI0513548 A BRPI0513548 A BR PI0513548A BR PI0513548 A BRPI0513548 A BR PI0513548A
Authority
BR
Brazil
Prior art keywords
ammonia
reactor effluent
recovery processes
effluent
aqueous ammonium
Prior art date
Application number
BRPI0513548-6A
Other languages
English (en)
Inventor
Albert R Shuki
Kenneth P Keckler
Thomas L Bowman
Thomas L Szabo
Original Assignee
Ineos Usa Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ineos Usa Llc filed Critical Ineos Usa Llc
Publication of BRPI0513548A publication Critical patent/BRPI0513548A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/24—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons
    • C07C253/26—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons containing carbon-to-carbon multiple bonds, e.g. unsaturated aldehydes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/12—Separation of ammonia from gases and vapours
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/54—Nitrogen compounds
    • B01D53/58—Ammonia
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/40—Nitrogen compounds
    • B01D2257/406—Ammonia
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S210/00—Liquid purification or separation
    • Y10S210/902—Materials removed
    • Y10S210/908—Organic

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Biomedical Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Water Treatments (AREA)
  • Degasification And Air Bubble Elimination (AREA)
  • Removal Of Specific Substances (AREA)
  • Gas Separation By Absorption (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

PROCESSOS DE RECUPERAçãO DE AMÈNIA A PARTIR DE FLUXO DE VAPOR E DE EFLUENTE DE REATOR. Um processo de recuperação de amónia não reagida a partir do efluente de uma zona de reação usada para produzir acrilonitrila ou metacrilonitrila que compreende arrefecer o efluente de reator com uma solução aquosa de fosfato de amónio em pelo menos duas fases, capturando, assim, o componente de amónia a partir do efluente. A amónia capturada pode ser recuperada aquecendo o fosfato de amónio aquoso, que pode, então, ser reciclado. Os contaminantes presentes no fosfato de amónio aquoso podem ser removidos, por exemplo, por extração de solvente ou oxidação por via úmida, antes do reciclo.
BRPI0513548-6A 2004-07-22 2005-07-21 processos de recuperação de amÈnia a partir de fluxo de vapor e de efluente de reator BRPI0513548A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US59014204P 2004-07-22 2004-07-22
PCT/US2005/026283 WO2006012606A2 (en) 2004-07-22 2005-07-21 Improved process for recovery and recycle of ammonia from a vapor stream

Publications (1)

Publication Number Publication Date
BRPI0513548A true BRPI0513548A (pt) 2008-08-26

Family

ID=35501307

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0513548-6A BRPI0513548A (pt) 2004-07-22 2005-07-21 processos de recuperação de amÈnia a partir de fluxo de vapor e de efluente de reator

Country Status (10)

Country Link
US (1) US7326391B2 (pt)
EP (1) EP1784357A2 (pt)
JP (1) JP2008507469A (pt)
KR (1) KR20070038559A (pt)
CN (1) CN101027252A (pt)
AU (1) AU2005266939A1 (pt)
BR (1) BRPI0513548A (pt)
MX (1) MX2007000871A (pt)
RU (1) RU2007106575A (pt)
WO (1) WO2006012606A2 (pt)

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JP5369423B2 (ja) * 2006-11-01 2013-12-18 三菱瓦斯化学株式会社 アンモニアの回収方法
US20090299087A1 (en) * 2008-05-28 2009-12-03 Solutia, Inc. Process for manufacturing unsaturated mononitriles to improve on-stream time and reduce fouling
CN102452955A (zh) * 2010-10-21 2012-05-16 中国石油化工股份有限公司 丙烯腈反应装置中未反应氨回收再循环利用的方法
WO2012078218A1 (en) * 2010-12-07 2012-06-14 Exxonmobil Chemical Patents Inc. Processes utilizing solvent extraction
CN102530868B (zh) * 2010-12-28 2016-03-02 李宽义 氨氧化合成气除氨的环保工艺方法
CN103420531B (zh) * 2012-05-16 2015-11-18 中国石油化工股份有限公司 丙烯腈生产过程中废水综合处理方法
CN103420396A (zh) * 2012-05-16 2013-12-04 中国石油化工股份有限公司 丙烯腈无硫铵工艺铵盐解析的新方法
CN103524380A (zh) * 2012-07-03 2014-01-22 中国石油化工股份有限公司 丙烯腈无硫铵工艺中降低吸收液中有机物含量的方法
CN103521034A (zh) * 2012-07-03 2014-01-22 中国石油化工股份有限公司 丙烯腈无硫铵工艺铵盐解析的改进方法
CN104736481B (zh) * 2012-07-19 2018-03-02 英威达纺织（英国）有限公司 利用空气喷射控制氨提取中的腐蚀
WO2014014620A1 (en) * 2012-07-19 2014-01-23 Invista North America S.A R.L. Ammonia recovery with purge for corrosion control
CN103664693A (zh) * 2012-09-05 2014-03-26 中国石油化工股份有限公司 丙烯腈反应装置中无硫铵工艺铵盐解析的方法
CN103664694A (zh) * 2012-09-05 2014-03-26 中国石油化工股份有限公司 丙烯腈无硫铵工艺中降低吸收液中有机物含量的方法
CA2827933C (en) 2012-09-25 2018-09-18 Xiaomei Li Method and apparatus for recovering solids from water-based effluent
CN105664669B (zh) * 2014-11-20 2018-01-09 中国石油化工股份有限公司 丙烯腈反应装置中未反应氨的处理方法
CN105664683B (zh) * 2014-11-20 2018-01-09 中国石油化工股份有限公司 丙烯腈反应装置中催化湿式氧化处理氨氮的方法
CN104667558B (zh) * 2015-02-27 2018-02-13 英尼奥斯欧洲股份公司 轻有机物汽提器塔系统和工艺
TWI781916B (zh) 2016-01-09 2022-11-01 美商阿散德性能材料營運公司 用於在丙烯腈反應器饋入流中氰化氫之直接製備的催化劑組合物及方法
WO2017192350A1 (en) 2016-05-02 2017-11-09 Invista North America S.A R.L. Process for reducing cpi in a dinitrile stream
EP4041436A1 (de) * 2019-10-11 2022-08-17 thyssenkrupp Industrial Solutions AG Abgaswäscher mit energieintegration
CN110759529B (zh) * 2019-10-31 2022-03-29 新地环保技术有限公司 一种回用水脱气方法及其脱气系统
CN111623601B (zh) * 2020-05-29 2021-08-27 崇阳县青峰科技有限公司 一种偏钒酸铵脱水系统及偏钒酸铵的富氨脱水方法
CN112370939A (zh) * 2020-10-10 2021-02-19 金堆城钼业股份有限公司 一种钼酸铵结晶过程中的氨气回收方法
CN113816964B (zh) * 2021-10-14 2023-02-10 中国科学院兰州化学物理研究所 一种捕集二氧化碳的可逆离子液体及其合成方法

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US2797148A (en) * 1951-03-13 1957-06-25 Du Pont Recovery of nh3 from a gaseous mixture containing nh3 and hcn
GB1199697A (en) * 1967-11-13 1970-07-22 Nitto Chemical Industry Co Ltd Process for the Removal of Unreacted Ammonia in the Production of Acrylonitrile
US4009243A (en) * 1970-11-18 1977-02-22 Firma Carl Still Continuous process for scrubbing out hydrogen sulfide and ammonia from coke oven gas
US3985863A (en) * 1973-07-02 1976-10-12 United States Steel Corporation Process for the separation and recovery of ammonia and acid gases
US4259302A (en) * 1978-12-11 1981-03-31 United Technologies Corporation Regenerable ammonia scrubber
US4287162A (en) * 1979-07-18 1981-09-01 Suntech, Inc. Separation of ammonia from ammonia containing gases
US4341535A (en) * 1981-01-02 1982-07-27 The Standard Oil Co. Ammonium sulfate recovery process
TW382005B (en) * 1996-04-30 2000-02-11 Standard Oil Co Ohio Process for recovery and recycle of ammonia from an acrylonitrile reactor refluent stream using an ammonium phosphate quench system
US20010006614A1 (en) * 1998-12-23 2001-07-05 Nero Linda L. Process for recovery and recycle of ammonia from an acrylonitrile reactor effluent stream using an ammonium phosphate quench system
MXPA01005155A (es) * 2000-05-23 2003-08-20 Rohm & Haas Proceso para la recuperacion y el reciclaje de amoniaco proveniente de una corriente efluente de reactor.
US6872296B2 (en) * 2002-07-30 2005-03-29 INVISTA North America S.à.r.l. Method for removing ammonia from a gas comprising hydrogen cyanide, ammonia and water

Also Published As

Publication number Publication date
JP2008507469A (ja) 2008-03-13
CN101027252A (zh) 2007-08-29
AU2005266939A1 (en) 2006-02-02
WO2006012606A3 (en) 2006-12-07
KR20070038559A (ko) 2007-04-10
MX2007000871A (es) 2007-04-18
US20060088461A1 (en) 2006-04-27
WO2006012606A2 (en) 2006-02-02
RU2007106575A (ru) 2008-08-27
EP1784357A2 (en) 2007-05-16
US7326391B2 (en) 2008-02-05

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Legal Events

Date Code Title Description
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]

Free format text: CONFORME ARTIGO 10O DA RESOLUCAO 124/06, CABE SER ARQUIVADO REFERENTE AO NAO RECOLHIMENTO DA 6A ANUIDADE.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 2143 DE 31/01/2012.