BRPI0410680A - processo para a recuperação de 1,3-propanodiol de um caldo de fermentação - Google Patents
processo para a recuperação de 1,3-propanodiol de um caldo de fermentaçãoInfo
- Publication number
- BRPI0410680A BRPI0410680A BRPI0410680-6A BRPI0410680A BRPI0410680A BR PI0410680 A BRPI0410680 A BR PI0410680A BR PI0410680 A BRPI0410680 A BR PI0410680A BR PI0410680 A BRPI0410680 A BR PI0410680A
- Authority
- BR
- Brazil
- Prior art keywords
- propanediol
- phase
- feed stream
- aqueous feed
- recovery
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0446—Juxtaposition of mixers-settlers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0488—Flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0492—Applications, solvents used
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/26—Treatment of water, waste water, or sewage by extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
"PROCESSO PARA A RECUPERAçãO DE 1,3-PROPANODIOL DE UM CALDO DE FERMENTAçãO". São divulgados aqui processos para a recuperação de 1,3-propanodiol de uma corrente de alimentação aquosa. A presente invenção envolve contatar uma corrente de alimentação aquosa que compreende água, 1,3-propanodiol, e pelo menos um contaminante com pelo menos um solvente extrator para formar uma mistura. A mistura é separada em uma primeira fase e uma segunda fase. A segunda fase compreende uma maioria da água da corrente de alimentação aquosa. A primeira fase compreende solvente extrator e pelo menos parte do 1,3-propanodiol que estava presente na corrente de alimentação aquosa. A razão em peso na primeira fase de 1,3-propanodiol para qualquer contaminante presente é maior do que a razão em peso de 1,3-propanodiol para o mesmo contaminante na corrente de alimentação aquosa antes da corrente de alimentação aquosa ser contatada com o solvente extrator. A primeira fase pode ser removida da segunda fase separada para recuperar o 1,3-propanodiol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BR122014002952A BR122014002952B1 (pt) | 2003-05-06 | 2004-05-06 | processo para a recuperação de 1,3-propanodiol de um caldo de fermentação |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/430,498 | 2003-05-06 | ||
| US10/430,498 US7056439B2 (en) | 2003-05-06 | 2003-05-06 | Process for producing 1, 3-propanediol |
| PCT/US2004/013905 WO2004101437A2 (en) | 2003-05-06 | 2004-05-06 | Process for producing 1, 3-propanediol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BRPI0410680A true BRPI0410680A (pt) | 2006-06-20 |
| BRPI0410680B1 BRPI0410680B1 (pt) | 2014-07-08 |
Family
ID=33416251
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR122014002952A BR122014002952B1 (pt) | 2003-05-06 | 2004-05-06 | processo para a recuperação de 1,3-propanodiol de um caldo de fermentação |
| BRPI0410680-6B1A BRPI0410680B1 (pt) | 2003-05-06 | 2004-05-06 | Processo para a recuperação de 1,3-propanodiol de um caldo de fermentação |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR122014002952A BR122014002952B1 (pt) | 2003-05-06 | 2004-05-06 | processo para a recuperação de 1,3-propanodiol de um caldo de fermentação |
Country Status (17)
| Country | Link |
|---|---|
| US (2) | US7056439B2 (pt) |
| EP (3) | EP2327464B1 (pt) |
| JP (1) | JP4808624B2 (pt) |
| KR (1) | KR101094018B1 (pt) |
| CN (1) | CN100430111C (pt) |
| AU (1) | AU2004238804B2 (pt) |
| BR (2) | BR122014002952B1 (pt) |
| CA (1) | CA2524452C (pt) |
| ES (3) | ES2408344T3 (pt) |
| IL (1) | IL171693A (pt) |
| MX (1) | MXPA05011894A (pt) |
| NO (1) | NO20055383L (pt) |
| NZ (1) | NZ543388A (pt) |
| RU (1) | RU2323200C2 (pt) |
| UA (1) | UA84289C2 (pt) |
| WO (1) | WO2004101437A2 (pt) |
| ZA (1) | ZA200509090B (pt) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7056439B2 (en) * | 2003-05-06 | 2006-06-06 | Tate & Lyle Ingredidents Americas, Inc. | Process for producing 1, 3-propanediol |
| JP4837949B2 (ja) * | 2005-06-22 | 2011-12-14 | パナソニック電工株式会社 | グリコールの分離方法 |
| SE531424C2 (sv) * | 2007-06-18 | 2009-03-31 | Perstorp Specialty Chem Ab | Extraktionsförfarande i en process för framställning av di-, tri- och polyhydroxialkoholer |
| KR101543485B1 (ko) * | 2007-11-30 | 2015-08-10 | 메타볼릭 익스플로러 | 발효 브로쓰로부터 알콜을 정제하는 방법 |
| AR072446A1 (es) * | 2008-03-02 | 2010-09-01 | Dow Global Technologies Inc | Proceso de hidrogenacion mejorado |
| US8084651B2 (en) * | 2008-03-10 | 2011-12-27 | Tate & Lyle Ingredients Americas Llc | Process for purification of glycerol |
| CA2738452C (en) | 2008-10-03 | 2016-06-21 | Metabolic Explorer | Method for purifying an alcohol from a fermentation broth using a falling film, a wiped film, a thin film or a short path evaporator |
| ES2625623T3 (es) * | 2009-06-04 | 2017-07-20 | Genomatica, Inc. | Procedimiento de separación de componentes de un caldo de fermentación |
| US8367877B2 (en) * | 2009-11-17 | 2013-02-05 | Alliant Techsystems Inc. | Methods of purifying 1,2,4-butanetriol |
| KR101134619B1 (ko) * | 2009-12-10 | 2012-04-09 | 한국과학기술연구원 | 1,3-프로판다이올의 분리 방법 |
| WO2011076690A1 (en) | 2009-12-22 | 2011-06-30 | Metabolic Explorer | Method for purifying 1,2-propanediol from a fermentation broth |
| CN102140480B (zh) * | 2010-06-09 | 2013-07-17 | 河南天冠企业集团有限公司 | 一种发酵生产1,3-丙二醇的方法 |
| CN101898935A (zh) * | 2010-07-09 | 2010-12-01 | 华东理工大学 | 从发酵液中萃取分离1,3-丙二醇的方法 |
| US8829248B2 (en) | 2010-08-18 | 2014-09-09 | Eastman Chemical Company | Method for recovery and recycle of ruthenium homogeneous catalysts |
| US9227896B2 (en) | 2010-08-18 | 2016-01-05 | Eastman Chemical Company | Process for the separation and purification of a mixed diol stream |
| US8466328B2 (en) | 2010-08-18 | 2013-06-18 | Eastman Chemical Company | Method for recovery and recycle of ruthenium homogeneous catalysts |
| US8785686B2 (en) | 2010-09-23 | 2014-07-22 | Eastman Chemical Company | Process for recovering and recycling an acid catalyst |
| US8709376B2 (en) | 2010-09-23 | 2014-04-29 | Eastman Chemical Company | Process for recovering and recycling an acid catalyst |
| WO2012130316A1 (en) | 2011-03-31 | 2012-10-04 | Metabolic Explorer | Method for purifying mpg (monopropylene glycol) from a fermentation broth |
| WO2013019587A2 (en) * | 2011-07-29 | 2013-02-07 | Saudi Arabian Oil Company | Integrated hydrotreating and isomerization process with aromatic separation |
| US8703999B2 (en) | 2012-03-27 | 2014-04-22 | Eastman Chemical Company | Hydrocarboxylation of methylene dipropionate in the presence of propionic acid and a heterogeneous catalyst |
| US8765999B2 (en) | 2012-03-27 | 2014-07-01 | Eastman Chemical Company | Hydrocarboxylation of formaldehyde in the presence of a higher order carboxylic acid and a homogeneous catalyst |
| WO2013148505A1 (en) * | 2012-03-27 | 2013-10-03 | Eastman Chemical Company | Process for the separation and purification of a mixed diol stream |
| US8927766B2 (en) | 2012-03-27 | 2015-01-06 | Eastman Chemical Company | Hydrocarboxylation of methylene dipropionate in the presence of a propionic acid and a homogeneous catalyst |
| US8829234B2 (en) | 2012-03-27 | 2014-09-09 | Eastman Chemical Company | Hydrocarboxylation of formaldehyde in the presence of a higher order carboxylic acid and heterogeneous catalyst |
| CN102816048A (zh) * | 2012-09-04 | 2012-12-12 | 华东理工大学 | 萃取分离发酵液中1,3-丙二醇的方法 |
| PL222957B1 (pl) | 2012-09-28 | 2016-09-30 | Prochimia Surfaces Spółka Z Ograniczoną Odpowiedzialnością | Sposób izolacji propano-1,3-diolu z mieszaniny pofermentacyjnej |
| ES2826023T3 (es) * | 2012-12-21 | 2021-05-17 | Sulzer Management Ag | Un sistema de extracción líquido-líquido y procedimiento para su uso |
| CN104003844B (zh) * | 2014-05-23 | 2015-12-30 | 大连理工大学 | 萃取与发酵耦联分离发酵液中2,3-丁二醇的方法 |
| WO2016073351A1 (en) * | 2014-11-04 | 2016-05-12 | Shell Oil Company | Processes for reclaiming alcohols |
| US10086339B2 (en) | 2015-03-10 | 2018-10-02 | The University Of Connecticut | Polymers and membranes for separation of polar organic compounds from aqueous mixtures and methods of using |
| US10407453B2 (en) * | 2015-04-07 | 2019-09-10 | University Of Louisville Research Foundation, Inc. | Process for isolating C5 sugars from biomass hydrolyzate |
| FR3071172B1 (fr) * | 2017-09-18 | 2019-10-04 | IFP Energies Nouvelles | Procede de separation des composes furaniques, en particulier le 5- hydroxymethylfurfural, du dimethoxysulfoxyde par des extractions liquide-liquide |
| FR3073525A1 (fr) | 2017-11-13 | 2019-05-17 | Algobiotech | Procede d’extraction de carotenoides, composition et produits associes |
| US11710411B2 (en) * | 2020-05-08 | 2023-07-25 | The Travelers Indemnity Company | Systems and methods for autonomous hazardous area data collection |
| CN112920021B (zh) * | 2021-02-01 | 2022-04-29 | 大连理工大学 | 一种醇类混合溶剂萃取发酵液中1,3-丙二醇的方法 |
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| WO2001073097A2 (en) | 2000-03-29 | 2001-10-04 | Archer-Daniels-Midland Company | Method of recovering 1,3-propanediol from fermentation broth |
| AU2001275996B2 (en) * | 2000-07-21 | 2005-08-04 | Cj Cheiljedang Corporation | Production of polyhydroxyalkanoates from polyols |
| CN1204260C (zh) * | 2001-04-27 | 2005-06-01 | 大连理工大学 | 一种微生物微氧发酵生产1,3－丙二醇的方法 |
| US7311838B2 (en) * | 2001-11-13 | 2007-12-25 | Metanomics Gmbh & Co. Kgaa | Method for the extraction and analysis of contents made from organic material |
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| US7056439B2 (en) * | 2003-05-06 | 2006-06-06 | Tate & Lyle Ingredidents Americas, Inc. | Process for producing 1, 3-propanediol |
-
2003
- 2003-05-06 US US10/430,498 patent/US7056439B2/en not_active Expired - Lifetime
-
2004
- 2004-05-06 EP EP11158112A patent/EP2327464B1/en not_active Expired - Lifetime
- 2004-05-06 BR BR122014002952A patent/BR122014002952B1/pt not_active IP Right Cessation
- 2004-05-06 RU RU2005137867/04A patent/RU2323200C2/ru active
- 2004-05-06 WO PCT/US2004/013905 patent/WO2004101437A2/en not_active Ceased
- 2004-05-06 AU AU2004238804A patent/AU2004238804B2/en not_active Ceased
- 2004-05-06 EP EP11158110.4A patent/EP2327465B1/en not_active Expired - Lifetime
- 2004-05-06 ES ES04751324T patent/ES2408344T3/es not_active Expired - Lifetime
- 2004-05-06 BR BRPI0410680-6B1A patent/BRPI0410680B1/pt not_active IP Right Cessation
- 2004-05-06 MX MXPA05011894A patent/MXPA05011894A/es active IP Right Grant
- 2004-05-06 EP EP04751324.7A patent/EP1620362B1/en not_active Expired - Lifetime
- 2004-05-06 CN CNB2004800184635A patent/CN100430111C/zh not_active Expired - Fee Related
- 2004-05-06 NZ NZ543388A patent/NZ543388A/en not_active IP Right Cessation
- 2004-05-06 UA UAA200511455A patent/UA84289C2/ru unknown
- 2004-05-06 ES ES11158110.4T patent/ES2505541T3/es not_active Expired - Lifetime
- 2004-05-06 KR KR1020057021149A patent/KR101094018B1/ko not_active Expired - Fee Related
- 2004-05-06 JP JP2006532567A patent/JP4808624B2/ja not_active Expired - Fee Related
- 2004-05-06 CA CA2524452A patent/CA2524452C/en not_active Expired - Lifetime
- 2004-05-06 ES ES11158112T patent/ES2410057T3/es not_active Expired - Lifetime
-
2005
- 2005-10-31 IL IL171693A patent/IL171693A/en active IP Right Grant
- 2005-11-10 ZA ZA200509090A patent/ZA200509090B/en unknown
- 2005-11-14 NO NO20055383A patent/NO20055383L/no not_active Application Discontinuation
-
2006
- 2006-02-13 US US11/352,593 patent/US7572376B2/en not_active Expired - Lifetime
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| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 08/07/2014, OBSERVADAS AS CONDICOES LEGAIS. |
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| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 19A ANUIDADE. |
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| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2721 DE 28-02-2023 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |