BRPI0519528A2 - processo para reduÇço do teor de cloro hodrolisÁvel em isocianatos orgÂnicos ou em misturas de isocianatos orgÂnicos, emprego de isocianatos - Google Patents
processo para reduÇço do teor de cloro hodrolisÁvel em isocianatos orgÂnicos ou em misturas de isocianatos orgÂnicos, emprego de isocianatosInfo
- Publication number
- BRPI0519528A2 BRPI0519528A2 BRPI0519528-4A BRPI0519528A BRPI0519528A2 BR PI0519528 A2 BRPI0519528 A2 BR PI0519528A2 BR PI0519528 A BRPI0519528 A BR PI0519528A BR PI0519528 A2 BRPI0519528 A2 BR PI0519528A2
- Authority
- BR
- Brazil
- Prior art keywords
- isocyanates
- organic
- mixtures
- reducing
- organic isocyanates
- Prior art date
Links
- 239000012948 isocyanate Substances 0.000 title abstract 10
- 150000002513 isocyanates Chemical class 0.000 title abstract 10
- 238000000034 method Methods 0.000 title abstract 4
- 239000000203 mixture Substances 0.000 title abstract 4
- 229910052801 chlorine Inorganic materials 0.000 title abstract 3
- 239000000460 chlorine Substances 0.000 title abstract 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 title abstract 2
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 abstract 1
- 238000005341 cation exchange Methods 0.000 abstract 1
- 150000001805 chlorine compounds Chemical class 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 230000008030 elimination Effects 0.000 abstract 1
- 238000003379 elimination reaction Methods 0.000 abstract 1
- 239000011261 inert gas Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C07C263/20—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyurethanes Or Polyureas (AREA)
- Paints Or Removers (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
Abstract
PROCESSO PARA REDUÇçO DO TEOR DE CLORO HIDROLISÁVEL EM ISOCIANATOS ORGÂNICOS OU EM MISTURAS DE ISOCIANATOS ORGÂNICOS, EMPREGO DE ISOCIANATOS. A presente invenção se refere a um processo para uma eliminação considerável de compostos de cloro de isocianatos orgânicos ou de misturas de isocianatos orgânicos, colocando-se o isocianato ou a mistura de isocianatos em contato com uma corrente de gás inerte contendo água ou com um material orgânico que tem efeito trocador de cátions. O processo permite uma eliminação suave de compostos contendo cloro dos isocianatos e se presta especialmente bem para isocianatos sensíveis à temperatura.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE200410063221 DE102004063221A1 (de) | 2004-12-22 | 2004-12-22 | Verfahren zur Reinigung organischer Isocyanate |
| DE200410063222 DE102004063222A1 (de) | 2004-12-22 | 2004-12-22 | Verfahren zur Reduktion von chlorhaltigen Komponenten in organischen Isocyanaten |
| PCT/EP2005/013277 WO2006072360A1 (de) | 2004-12-22 | 2005-12-10 | Verfahren zur reduktion von chlorhaltigen komponenten in organischen isocyanaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BRPI0519528A2 true BRPI0519528A2 (pt) | 2009-02-17 |
Family
ID=35962153
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0519528-4A BRPI0519528A2 (pt) | 2004-12-22 | 2005-12-10 | processo para reduÇço do teor de cloro hodrolisÁvel em isocianatos orgÂnicos ou em misturas de isocianatos orgÂnicos, emprego de isocianatos |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20080228006A1 (pt) |
| EP (1) | EP1831155A1 (pt) |
| JP (1) | JP2008524273A (pt) |
| CN (1) | CN102351738A (pt) |
| BR (1) | BRPI0519528A2 (pt) |
| IL (1) | IL183874A0 (pt) |
| WO (1) | WO2006072360A1 (pt) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2925498B1 (fr) * | 2007-12-21 | 2010-04-02 | Rhodia Operations | Procede de reduction de l'acidite residuelle d'isocyanatosilanes |
| CN110396057B (zh) * | 2019-07-16 | 2022-02-18 | 万华化学集团股份有限公司 | 一种制备低氯含量的异氰酸酯的方法 |
| CN110982038B (zh) * | 2019-12-27 | 2021-05-14 | 万华化学(宁波)有限公司 | 一种聚氨酯树脂及其制备方法 |
| CN112098576B (zh) * | 2020-08-27 | 2022-07-05 | 广州广电计量检测无锡有限公司 | 一种气质联用检测胶黏剂中1,3-双(1-异氰酸根-1-甲基乙基)苯的方法 |
| CN116535334A (zh) * | 2023-05-22 | 2023-08-04 | 南京工业大学 | 一种降低异氰酸酯中水解氯含量的方法 |
| CN117736116B (zh) * | 2023-11-28 | 2026-03-10 | 宁夏瑞泰科技股份有限公司 | 六亚甲基二异氰酸酯的制备方法 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1113570B (de) * | 1957-04-20 | 1961-09-07 | Bayer Ag | Verfahren zur Herstellung von Kationenaustauschern auf Basis von nicht sprosspolymerisierten vernetzten Polymerisaten |
| DE1240849B (de) | 1962-10-31 | 1967-05-24 | Olin Mathieson | Verfahren zur Herabsetzung der Konzentration des hydrolysierbaren Chlorids in einem organischen Isocyanat |
| US3219678A (en) * | 1963-02-28 | 1965-11-23 | Olin Mathieson | Process for reducing the hydrolyzable chlorine content of organic isocyanates |
| US3458558A (en) * | 1963-10-25 | 1969-07-29 | Allied Chem | Purification of isocyanates by reducing the hydrolyzable chlorine content |
| US3264336A (en) * | 1964-09-11 | 1966-08-02 | Mobay Chemical Corp | Purification of isocyanates by reduction of the hydrolyzable chlorine and acid content |
| US3759971A (en) * | 1971-01-20 | 1973-09-18 | Jefferson Chem Co Inc | Purification of isocyanates |
| US3799963A (en) * | 1972-05-12 | 1974-03-26 | Olin Corp | Purification of isocyanates reducing the hydrolyzable chlorine and acid content |
| US3912600A (en) * | 1974-05-09 | 1975-10-14 | Upjohn Co | Recovery of polymethylene polyphenyl polyisocyanate from a phoshenosed polyamine feed |
| US4049894A (en) * | 1975-08-25 | 1977-09-20 | The B. F. Goodrich Company | Latex modified portland cement and use thereof in polymerization reactors |
| JPS5686146A (en) * | 1979-12-14 | 1981-07-13 | Mitsui Toatsu Chem Inc | Preparation of lower aliphatic isocyanate |
| US4996351A (en) * | 1987-01-27 | 1991-02-26 | The Dow Chemical Company | Process for reducing the quantity of hydrolyzable chlorides in isocyanates |
| US4904704A (en) * | 1988-12-22 | 1990-02-27 | The Dow Chemical Company | Rigid foams prepared from treated toluene diisocyanate residue |
| US4962272A (en) * | 1989-05-30 | 1990-10-09 | Aristech Chemical Corporation | Treatment of arsine removal catalysts |
| JP2875877B2 (ja) * | 1990-10-23 | 1999-03-31 | 三井化学株式会社 | メチレン架橋ポリフェニレンポリイソシアネートの製造方法 |
| DE4124318A1 (de) * | 1991-07-23 | 1993-01-28 | Bayer Ag | Verfahren zur reinigung von polyisocyanaten, die so gereinigten polyisocyanate und ihre verwendung |
| JP3229710B2 (ja) * | 1993-06-08 | 2001-11-19 | 三井化学株式会社 | 有機イソシアナート化合物の精製方法 |
| JPH1045700A (ja) * | 1996-07-29 | 1998-02-17 | Mitsubishi Gas Chem Co Inc | ジイソシアネート化合物およびそのオリゴマー |
| US6245935B1 (en) | 1998-02-06 | 2001-06-12 | Showa Denko Kabushiki Kaisha | Method for producing isocyanatoalkyl (meth)acrylate |
| DE19914292A1 (de) * | 1999-03-30 | 2000-10-05 | Bayer Ag | Verfahren zur Verringerung des Chlorgehaltes von organischen Isocyanaten |
| DE19922572A1 (de) * | 1999-05-17 | 2000-11-23 | Bayer Ag | Verfahren zur Reinigung von organischen Isocyanaten, die so gereinigten organischen Isocyanate und ihre Verwendung |
| US20060229464A1 (en) * | 2003-07-31 | 2006-10-12 | Katsutoshi Morinaka | Stabilized (meth)acryloyloxyalkyl isocyanate a process for stabilization thereof and a process for preparation of the same |
-
2005
- 2005-12-10 US US11/792,806 patent/US20080228006A1/en not_active Abandoned
- 2005-12-10 JP JP2007547251A patent/JP2008524273A/ja active Pending
- 2005-12-10 WO PCT/EP2005/013277 patent/WO2006072360A1/de not_active Ceased
- 2005-12-10 EP EP05815233A patent/EP1831155A1/de not_active Withdrawn
- 2005-12-10 BR BRPI0519528-4A patent/BRPI0519528A2/pt not_active IP Right Cessation
- 2005-12-10 CN CN2011102384159A patent/CN102351738A/zh active Pending
-
2007
- 2007-06-12 IL IL183874A patent/IL183874A0/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US20080228006A1 (en) | 2008-09-18 |
| WO2006072360A1 (de) | 2006-07-13 |
| JP2008524273A (ja) | 2008-07-10 |
| CN102351738A (zh) | 2012-02-15 |
| IL183874A0 (en) | 2007-10-31 |
| EP1831155A1 (de) | 2007-09-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 8A ANUIDADE. |
|
| B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 2260 DE 29/04/2014. |