BRPI0603210A - método de preparação de lìquidos iÈnicos isentos de halogenetos e lìquidos iÈnicos assim preparados - Google Patents
método de preparação de lìquidos iÈnicos isentos de halogenetos e lìquidos iÈnicos assim preparadosInfo
- Publication number
- BRPI0603210A BRPI0603210A BRPI0603210-9A BRPI0603210A BRPI0603210A BR PI0603210 A BRPI0603210 A BR PI0603210A BR PI0603210 A BRPI0603210 A BR PI0603210A BR PI0603210 A BRPI0603210 A BR PI0603210A
- Authority
- BR
- Brazil
- Prior art keywords
- ionic liquids
- anions
- free
- liquids
- room temperature
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
- C07D233/56—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms
- C07D233/60—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms with hydrocarbon radicals, substituted by oxygen or sulfur atoms, attached to ring nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
- C10N2020/01—Physico-chemical properties
- C10N2020/077—Ionic Liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
MéTODO DE PREPARAçãO DE LìQUIDOS IÈNICOS ISENTOS DE HALOGENETOS E LìQUIDOS INÈNICOS ASSIM PREPARADOS A reação de N-alquil-imidazol com sulfonatos de alquila, na temperatura ambiente, propicia alcano-sulfonatos de 1,3-dialquil imidazólio como sólidos cristalinos em altos rendimentos. Os ânions alcano- sulfonatos podem ser facilmente substituídos por uma série de outros anions (BF~4~, PF~6~, PF~3~(CF~2~CF~3~)~3~, CF~3~SO~3~ e (CF~3~SO~2~)~2~N! mediante simples reação de ânions, sais, ou ácidos em água na temperatura ambiente. A extração com diclorometano, filtração, e a evaporação do solvente, propiciam os desejados líquidos iónicos em rendimento de 80-95%. A pureza desses líquidos iónicos (em alguns casos >99,4%) pode ser determinada pela intensidade dos sinais de satélites ¬13¬C dos espectros de ressonância magnética do grupo N-metil imidazólio como um padrão interno.
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BRPI0603210-9A BRPI0603210A (pt) | 2006-08-15 | 2006-08-15 | método de preparação de lìquidos iÈnicos isentos de halogenetos e lìquidos iÈnicos assim preparados |
| US11/790,352 US7825259B2 (en) | 2006-08-15 | 2007-04-25 | Method of preparation of halogen-free ionic liquids and ionic liquids prepared in this manner |
| ARP070102074A AR060921A1 (es) | 2006-08-15 | 2007-05-14 | Proceso de preparacion de liquidos ionicos exentos de haluros y liquidos ionicos exentos de haluros |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BRPI0603210-9A BRPI0603210A (pt) | 2006-08-15 | 2006-08-15 | método de preparação de lìquidos iÈnicos isentos de halogenetos e lìquidos iÈnicos assim preparados |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BRPI0603210A true BRPI0603210A (pt) | 2008-04-08 |
Family
ID=39102215
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0603210-9A BRPI0603210A (pt) | 2006-08-15 | 2006-08-15 | método de preparação de lìquidos iÈnicos isentos de halogenetos e lìquidos iÈnicos assim preparados |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US7825259B2 (pt) |
| AR (1) | AR060921A1 (pt) |
| BR (1) | BRPI0603210A (pt) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101788578B1 (ko) | 2009-08-31 | 2017-11-15 | 와코 쥰야꾸 고교 가부시키가이샤 | 알릴술포네이트 음이온 함유 이온액체 |
| MX2010002574A (es) * | 2010-03-05 | 2011-09-21 | Mexicano Inst Petrol | Proceso de recuperacion de liquidos ionicos agotados por la desulfuracion extractiva de naftas. |
| SE535675C2 (sv) | 2011-03-22 | 2012-11-06 | Högprestandasmörjmedel och tillsatser till smörjmedel för järnhaltiga och icke järnhaltiga material | |
| US20130099156A1 (en) * | 2011-10-25 | 2013-04-25 | Christoph Stock | Use of liquid compositions comprising imidazolium salts as operating materials |
| KR102326396B1 (ko) | 2013-09-27 | 2021-11-12 | 레르 리키드 쏘시에떼 아노님 뿌르 레드 에렉스뿔라따시옹 데 프로세데 조르즈 클로드 | 아민 치환된 트리실릴아민 및 트리디실릴아민 화합물 |
| US11124876B2 (en) | 2015-03-30 | 2021-09-21 | L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Si-containing film forming precursors and methods of using the same |
| US9777025B2 (en) | 2015-03-30 | 2017-10-03 | L'Air Liquide, Société pour l'Etude et l'Exploitation des Procédés Georges Claude | Si-containing film forming precursors and methods of using the same |
| US10192734B2 (en) | 2016-12-11 | 2019-01-29 | L'Air Liquide, Société Anonyme pour l'Etude et l'Exploration des Procédés Georges Claude | Short inorganic trisilylamine-based polysilazanes for thin film deposition |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9928290D0 (en) | 1999-12-01 | 2000-01-26 | Univ Belfast | Process for preparing ambient temperature ionic liquids |
| DE10208822A1 (de) | 2002-03-01 | 2003-09-11 | Solvent Innovation Gmbh | Halogenfreie ionische Flüssigkeiten |
-
2006
- 2006-08-15 BR BRPI0603210-9A patent/BRPI0603210A/pt not_active Application Discontinuation
-
2007
- 2007-04-25 US US11/790,352 patent/US7825259B2/en not_active Expired - Fee Related
- 2007-05-14 AR ARP070102074A patent/AR060921A1/es active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| US20080045723A1 (en) | 2008-02-21 |
| AR060921A1 (es) | 2008-07-23 |
| US7825259B2 (en) | 2010-11-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
| B07A | Technical examination (opinion): publication of technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: INDEFIRO O PEDIDO DE ACORDO COM O(S) ARTIGO(S) 8 C/C 11, 24 E 25 DA LPI. |
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| B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL. |