BRPI0700642A - método para o tratamento de emulsões água/óleo com microondas - Google Patents

método para o tratamento de emulsões água/óleo com microondas

Info

Publication number
BRPI0700642A
BRPI0700642A BRPI0700642-0A BRPI0700642A BRPI0700642A BR PI0700642 A BRPI0700642 A BR PI0700642A BR PI0700642 A BRPI0700642 A BR PI0700642A BR PI0700642 A BRPI0700642 A BR PI0700642A
Authority
BR
Brazil
Prior art keywords
microwave
emulsion
conditions
analysis
water
Prior art date
Application number
BRPI0700642-0A
Other languages
English (en)
Inventor
Cauby Coutinho Raquel Campos
Heredia Montserrat Fortuny
Marcio Nele De Souza
Alexandre Ferreira Santos
Original Assignee
Petroleo Brasileiro Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Petroleo Brasileiro Sa filed Critical Petroleo Brasileiro Sa
Priority to BRPI0700642-0A priority Critical patent/BRPI0700642B1/pt
Priority to US12/007,082 priority patent/US7705058B2/en
Priority to ARP080100168A priority patent/AR064902A1/es
Priority to MX2009009546A priority patent/MX2009009546A/es
Priority to PCT/GB2008/000815 priority patent/WO2008107696A2/en
Priority to CA002680143A priority patent/CA2680143A1/en
Priority to EP08250775.7A priority patent/EP1977806B1/en
Publication of BRPI0700642A publication Critical patent/BRPI0700642A/pt
Publication of BRPI0700642B1 publication Critical patent/BRPI0700642B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G32/00—Refining of hydrocarbon oils by electric or magnetic means, by irradiation, or by using microorganisms
    • C10G32/02—Refining of hydrocarbon oils by electric or magnetic means, by irradiation, or by using microorganisms by electric or magnetic means
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/04—Breaking emulsions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/04—Breaking emulsions
    • B01D17/042—Breaking emulsions by changing the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/04—Breaking emulsions
    • B01D17/044—Breaking emulsions by changing the pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G33/00—Dewatering or demulsification of hydrocarbon oils
    • C10G33/02—Dewatering or demulsification of hydrocarbon oils with electrical or magnetic means

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Colloid Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

MéTODO PARA O TRATAMENTO DE EMULSõES áGUA/óLEO COM MICROONDAS. é descrito um método para o tratamento de emulsões com microondas que compreende as etapas de: a) em laboratório, determinar, para uma emulsão A/O (604), (705), (713), (805), (812) as condições ótimas das variáveis: teor de água, teor de sal, pH da fase aquosa, temperatura inicial, potência para aplicação das microondas, temperatura final e distribuição de tamanho de gotas a serem ajustados na planta industrial, em função de características do óleo cru em estudo como viscosidade, densidade, teor de asfaltenos, acidez total, tais condições sendo aquelas necessárias para obter pelo menos 90% de eficiência de separação da dita emulsão em presença de radiação de microondas; b) utilizar estas informações para o ajuste inicial de condições de aplicação do método em unidades de separação de fases (100), (200), (300) em refinarias e em unidades de produção;c) efetuar análises em linha das variáveis da etapa a) e da resposta do processo nas correntes efluentes das unidades de separação, sendo esta resposta as análises de teor de água e sais, de forma a retroalimentar as informações ao melhor ajuste das condições de processo para aplicação das microondas; e d) utilizar adicionalmente as análises em linha ou em laboratório do efeito do método como monitoramento da eficiência da quebra da emulsão A/O.
BRPI0700642-0A 2007-03-07 2007-03-07 Método para o tratamento de emulsões água/óleo com microondas BRPI0700642B1 (pt)

Priority Applications (7)

Application Number Priority Date Filing Date Title
BRPI0700642-0A BRPI0700642B1 (pt) 2007-03-07 2007-03-07 Método para o tratamento de emulsões água/óleo com microondas
US12/007,082 US7705058B2 (en) 2007-03-07 2008-01-07 Method for the microwave treatment of water-in-oil emulsions
ARP080100168A AR064902A1 (es) 2007-03-07 2008-01-14 Metodo para el tratamiento de emulsiones agua/aceite con microondas
MX2009009546A MX2009009546A (es) 2007-03-07 2008-03-07 Metodo para el tratamiento por microondas de emulsiones de agua en petroleo.
PCT/GB2008/000815 WO2008107696A2 (en) 2007-03-07 2008-03-07 Method for the microwave treatment of water-in-oil emulsions
CA002680143A CA2680143A1 (en) 2007-03-07 2008-03-07 Method for the microwave treatment of water-in-oil emulsions
EP08250775.7A EP1977806B1 (en) 2007-03-07 2008-03-07 Method for the microwave treatment of water-in-oil emulsions

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
BRPI0700642-0A BRPI0700642B1 (pt) 2007-03-07 2007-03-07 Método para o tratamento de emulsões água/óleo com microondas

Publications (2)

Publication Number Publication Date
BRPI0700642A true BRPI0700642A (pt) 2008-10-21
BRPI0700642B1 BRPI0700642B1 (pt) 2015-04-14

Family

ID=39672590

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0700642-0A BRPI0700642B1 (pt) 2007-03-07 2007-03-07 Método para o tratamento de emulsões água/óleo com microondas

Country Status (7)

Country Link
US (1) US7705058B2 (pt)
EP (1) EP1977806B1 (pt)
AR (1) AR064902A1 (pt)
BR (1) BRPI0700642B1 (pt)
CA (1) CA2680143A1 (pt)
MX (1) MX2009009546A (pt)
WO (1) WO2008107696A2 (pt)

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US8555970B2 (en) * 2009-05-20 2013-10-15 Conocophillips Company Accelerating the start-up phase for a steam assisted gravity drainage operation using radio frequency or microwave radiation
US8365823B2 (en) * 2009-05-20 2013-02-05 Conocophillips Company In-situ upgrading of heavy crude oil in a production well using radio frequency or microwave radiation and a catalyst
CA2704575C (en) 2009-05-20 2016-01-19 Conocophillips Company Wellhead hydrocarbon upgrading using microwaves
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BRPI0905253B1 (pt) * 2009-12-28 2020-02-18 Petroleo Brasileiro S.A. - Petrobras Processo para o tratamento de emulsões água/óleo
CN103813842B (zh) * 2011-07-26 2016-03-23 沙特阿拉伯石油公司 用于油-气分离装置的动态破乳系统
RU2536583C2 (ru) * 2011-08-04 2014-12-27 Александр Алексеевич Федотов Способ обезвоживания водонефтяной эмульсии
CA2903256C (en) * 2013-03-06 2022-09-06 Wilsa, Inc. Method and apparatus for conditioning fluids
RU2568980C2 (ru) * 2013-11-14 2015-11-20 Открытое акционерное общество "Татнефть" имени В.Д. Шашина Способ разделения водонефтяной эмульсии с применением ультразвукового воздействия
US9827540B2 (en) 2014-05-19 2017-11-28 Highland Fluid Technology, Ltd. Central entry dual rotor cavitation
US9677008B2 (en) 2014-12-04 2017-06-13 Harris Corporation Hydrocarbon emulsion separator system and related methods
CA3001458A1 (en) * 2015-12-07 2017-06-15 Halliburton Energy Services, Inc. Beneficiating weighting agents
US20180334621A1 (en) 2017-05-22 2018-11-22 Saudi Arabian Oil Company Crude hydrocarbon fluids demulsification system
CN108413827A (zh) * 2018-03-14 2018-08-17 安徽理工大学 一种废旧乳化炸药的销毁回收装置及方法
CN108379880A (zh) 2018-03-20 2018-08-10 中国科学院过程工程研究所 一种含焦粉的油水混合物的分离设备及分离方法
RU2698803C1 (ru) * 2018-12-28 2019-08-30 Общество с ограниченной ответственностью (ООО) "ЛУКОЙЛ-ПЕРМЬ" Технология разрушения стойких водонефтяных эмульсий ультразвуковым методом
RU2710181C1 (ru) * 2019-08-06 2019-12-24 Общество с ограниченной ответственностью "Газпромнефть Научно-Технический Центр" (ООО "Газпромнефть НТЦ") Система и способ электромагнитного фазоразделения водонефтяной эмульсии
US11090580B2 (en) 2019-08-08 2021-08-17 Saudi Arabian Oil Company Dewatering a hydrocarbon storage tank
US11161758B2 (en) 2019-12-02 2021-11-02 Saudi Arabian Oil Company Microwave based systems for bacteria removal from water cooling towers
CN111253968B (zh) * 2020-02-26 2021-12-24 西安石油大学 一种磁性纳米粒子-微波处理稠油水包油型乳状液的方法
RU2745993C1 (ru) * 2020-03-05 2021-04-05 Общество с ограниченной ответственностью (ООО) "ЛУКОЙЛ-ПЕРМЬ" Способ комбинированного обезвоживания стойких водонефтяных эмульсий
US11845902B2 (en) * 2020-06-23 2023-12-19 Saudi Arabian Oil Company Online analysis in a gas oil separation plant (GOSP)
US12196713B2 (en) 2021-08-24 2025-01-14 Saudi Arabian Oil Company Convex ultrasonic sensor for weld inspection
CN113680106B (zh) * 2021-10-25 2022-01-25 山东海吉雅环保设备有限公司 一种电子束辐照处理老化油工艺
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Also Published As

Publication number Publication date
CA2680143A1 (en) 2008-09-12
AR064902A1 (es) 2009-05-06
BRPI0700642B1 (pt) 2015-04-14
EP1977806A3 (en) 2008-10-22
EP1977806A2 (en) 2008-10-08
MX2009009546A (es) 2009-09-15
US7705058B2 (en) 2010-04-27
EP1977806B1 (en) 2014-06-04
WO2008107696A3 (en) 2008-11-06
WO2008107696A2 (en) 2008-09-12
US20080221226A1 (en) 2008-09-11

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Legal Events

Date Code Title Description
B03A Publication of a patent application or of a certificate of addition of invention [chapter 3.1 patent gazette]
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

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Free format text: CONDICOES CONTRATUAIS: 1) ROYALTIES: 15% SOBRE O PRECO DE VENDA, EXCLUINDO OS IMPOSTOS INCIDENTES NA EMISSAO DA NOTA FISCAL (IPI, ISS E ICMS), TAXA DE ACESSO E TAXA MINIMA ANUAL; 2) PRAZO: 5 ANOS, PODENDO SER PRORROGAVEL POR IGUAL PERIODO, ATE O FIM DA VIGENCIA DO ATIVO INTELECTUAL; 3) CONDICOES DE PAGAMENTO: TRIMESTRAL, A PARTIR DOS DADOS OBTIDOS NAS NOTAS FISCAIS SOLICITADAS; 4) DISPONIBILIDADE DE KNOW-HOW: NAO; 5) ASSISTENCIA TECNICA: NAO. - OBS: CONSULTA A CARTA PATENTE PODERA SER FEITA ATRAVES DO ENDERECO ELETRONICO WWW.INPI.GOV.BR - NO ACESSO RAPIDO = BUSCA DE PROCESSOS = FACA LOGIN COM SENHA OU TECLE CONTINUAR = PATENTE = DIGITE O NUMERO DO PROCESSO = PESQUISAR. PARA ACESSAR, CADASTRE-SE NO PORTAL DO INPI.

Free format text: CONDICOES CONTRATUAIS: 1) ROYALTIES: 15% SOBRE O PRECO DE VENDA, EXCLUINDO OS IMPOSTOS INCIDENTES NA EMISSAO DA NOTA FISCAL (IPI, ISS E ICMS), TAXA DE ACESSO E TAXA MINIMA ANUAL; 2) PRAZO: 5 ANOS, PODENDO SER PRORROGAVEL POR IGUAL PERIODO, ATE O FIM DA VIGENCIA DO ATIVO INTELECTUAL; 3) CONDICOES DE PAGAMENTO: TRIMESTRAL, A PARTIR DOS DADOS OBTIDOS NAS NOTAS FISCAIS SOLICITADAS; 4) DISPONIBILIDADE DE KNOW-HOW: NAO; 5) ASSISTENCIA TECNICA: NAO. - OBS: CONSULTA A CARTA PATENTE PODERA SER FEITA ATRAVES DO ENDERECO ELETRONICO WWW.INPI.GOV.BR - NO ACESSO RAPIDO = BUSCA DE PROCESSOS = FACA LOGIN COM SENHA OU TECLE CONTINUAR = PATENTE = DIGITE O NUMERO DO PROCESSO = PESQUISAR. PARA ACESSAR, CAD

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B22L Other matters related to patents and certificates of addition of invention: notification of licence offer (art 64 par 1 of lpi)

Free format text: CONDICOES CONTRATUAIS: 1) ROYALTIES: 15% SOBRE O PRECO DE VENDA, EXCLUINDO OS IMPOSTOS INCIDENTES NA EMISSAO DA NOTA FISCAL (IPI, ISS E ICMS), TAXA DE ACESSO E TAXA MINIMA ANUAL; 2) PRAZO: 5 ANOS, PODENDO SER PRORROGAVEL POR IGUAL PERIODO, ATE O FIM DA VIGENCIA DO ATIVO INTELECTUAL; 3) CONDICOES DE PAGAMENTO: TRIMESTRAL, A PARTIR DOS DADOS OBTIDOS NAS NOTAS FISCAIS SOLICITADAS; 4) DISPONIBILIDADE DE KNOW-HOW: NAO; 5) ASSISTENCIA TECNICA: NAO. - OBS: CONSULTA A CARTA PATENTE PODERA SER FEITA ATRAVES DO ENDERECO ELETRONICO WWW.INPI.GOV.BR - NO ACESSO RAPIDO = BUSCA DE PROCESSOS = FACA LOGIN COM SENHA OU TECLE CONTINUAR = PATENTE = DIGITE O NUMERO DO PROCESSO = PESQUISAR. PARA ACESSAR, CAD

B22L Other matters related to patents and certificates of addition of invention: notification of licence offer (art 64 par 1 of lpi)

Free format text: CONDICOES CONTRATUAIS: 1) ROYALTIES: 15% SOBRE O PRECO DE VENDA, EXCLUINDO OS IMPOSTOS INCIDENTES NA EMISSAO DA NOTA FISCAL (IPI, ISS E ICMS), TAXA DE ACESSO E TAXA MINIMA ANUAL; 2) PRAZO: 5 ANOS, PODENDO SER PRORROGAVEL POR IGUAL PERIODO, ATE O FIM DA VIGENCIA DO ATIVO INTELECTUAL; 3) CONDICOES DE PAGAMENTO: TRIMESTRAL, A PARTIR DOS DADOS OBTIDOS NAS NOTAS FISCAIS SOLICITADAS; 4) DISPONIBILIDADE DE KNOW-HOW: NAO; 5) ASSISTENCIA TECNICA: NAO. - OBS: CONSULTA A CARTA PATENTE PODERA SER FEITA ATRAVES DO ENDERECO ELETRONICO WWW.INPI.GOV.BR - NO ACESSO RAPIDO = BUSCA DE PROCESSOS = FACA LOGIN COM SENHA OU TECLE CONTINUAR = PATENTE = DIGITE O NUMERO DO PROCESSO = PESQUISAR. PARA ACESSAR, CAD