CA1128685A - Process for bonding inorganic materials - Google Patents

Process for bonding inorganic materials

Info

Publication number: CA1128685A
Authority: CA; Canada
Prior art keywords: composition; organic solvent; weight; bis; hydrolysis catalyst
Prior art date: 1976-07-21
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA281,446A

Other languages

English (en)

French (fr)

Inventor

Michael Roth

Konrad Gogolok

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Wacker Chemie AG

Original Assignee

Wacker Chemie AG

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1976-07-21

Filing date

1977-06-27

Publication date

1982-07-27

1977-06-27 Application filed by Wacker Chemie AG filed Critical Wacker Chemie AG

1982-07-27 Application granted granted Critical

1982-07-27 Publication of CA1128685A publication Critical patent/CA1128685A/en

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 31
229910010272 inorganic material Inorganic materials 0.000 title claims abstract description 30
239000011147 inorganic material Substances 0.000 title claims abstract description 30
239000000203 mixture Substances 0.000 claims abstract description 61
230000007062 hydrolysis Effects 0.000 claims abstract description 44
238000006460 hydrolysis reaction Methods 0.000 claims abstract description 44
239000003054 catalyst Substances 0.000 claims abstract description 38
125000003545 alkoxy group Chemical group 0.000 claims abstract description 30
230000002209 hydrophobic effect Effects 0.000 claims abstract description 30
150000003377 silicon compounds Chemical class 0.000 claims abstract description 28
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
-1 alkyl radical Chemical class 0.000 claims description 57
239000003960 organic solvent Substances 0.000 claims description 33
239000003795 chemical substances by application Substances 0.000 claims description 31
239000000463 material Substances 0.000 claims description 17
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 11
125000004432 carbon atom Chemical group C* 0.000 claims description 10
150000003839 salts Chemical class 0.000 claims description 7
239000004570 mortar (masonry) Substances 0.000 claims description 6
125000001931 aliphatic group Chemical group 0.000 claims description 5
150000001735 carboxylic acids Chemical class 0.000 claims description 5
229910052751 metal Inorganic materials 0.000 claims description 5
239000002184 metal Substances 0.000 claims description 5
239000004215 Carbon black (E152) Substances 0.000 claims description 4
229930195733 hydrocarbon Natural products 0.000 claims description 4
229920001296 polysiloxane Polymers 0.000 claims description 4
238000009835 boiling Methods 0.000 claims description 3
239000004568 cement Substances 0.000 claims description 3
239000004927 clay Substances 0.000 claims description 3
239000004567 concrete Substances 0.000 claims description 3
150000002576 ketones Chemical class 0.000 claims description 3
239000010445 mica Substances 0.000 claims description 3
229910052618 mica group Inorganic materials 0.000 claims description 3
GYTROFMCUJZKNA-UHFFFAOYSA-N triethyl triethoxysilyl silicate Chemical compound CCO[Si](OCC)(OCC)O[Si](OCC)(OCC)OCC GYTROFMCUJZKNA-UHFFFAOYSA-N 0.000 claims description 3
PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 2
229910052748 manganese Inorganic materials 0.000 claims description 2
239000011572 manganese Substances 0.000 claims description 2
125000002524 organometallic group Chemical group 0.000 claims 2
FOQJQXVUMYLJSU-UHFFFAOYSA-N triethoxy(1-triethoxysilylethyl)silane Chemical group CCO[Si](OCC)(OCC)C(C)[Si](OCC)(OCC)OCC FOQJQXVUMYLJSU-UHFFFAOYSA-N 0.000 claims 2
BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims 1
150000007942 carboxylates Chemical class 0.000 claims 1
QUPDWYMUPZLYJZ-UHFFFAOYSA-N ethyl Chemical group C[CH2] QUPDWYMUPZLYJZ-UHFFFAOYSA-N 0.000 claims 1
150000002430 hydrocarbons Chemical class 0.000 claims 1
150000001335 aliphatic alkanes Chemical class 0.000 abstract description 6
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
239000002904 solvent Substances 0.000 description 6
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
150000001875 compounds Chemical class 0.000 description 4
150000003254 radicals Chemical class 0.000 description 4
239000000126 substance Substances 0.000 description 4
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
239000002253 acid Substances 0.000 description 3
239000007767 bonding agent Substances 0.000 description 3
229910052710 silicon Inorganic materials 0.000 description 3
239000010703 silicon Substances 0.000 description 3
125000005369 trialkoxysilyl group Chemical group 0.000 description 3
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 description 2
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
150000001298 alcohols Chemical class 0.000 description 2
150000001337 aliphatic alkines Chemical class 0.000 description 2
150000001338 aliphatic hydrocarbons Chemical class 0.000 description 2
HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 2
125000001309 chloro group Chemical group Cl* 0.000 description 2
AYOHIQLKSOJJQH-UHFFFAOYSA-N dibutyltin Chemical compound CCCC[Sn]CCCC AYOHIQLKSOJJQH-UHFFFAOYSA-N 0.000 description 2
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 2
239000011521 glass Substances 0.000 description 2
239000012535 impurity Substances 0.000 description 2
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
150000003961 organosilicon compounds Chemical class 0.000 description 2
239000004575 stone Substances 0.000 description 2
238000005728 strengthening Methods 0.000 description 2
VOLGAXAGEUPBDM-UHFFFAOYSA-N $l^{1}-oxidanylethane Chemical compound CC[O] VOLGAXAGEUPBDM-UHFFFAOYSA-N 0.000 description 1
ODIGIKRIUKFKHP-UHFFFAOYSA-N (n-propan-2-yloxycarbonylanilino) acetate Chemical group CC(C)OC(=O)N(OC(C)=O)C1=CC=CC=C1 ODIGIKRIUKFKHP-UHFFFAOYSA-N 0.000 description 1
VIDOPANCAUPXNH-UHFFFAOYSA-N 1,2,3-triethylbenzene Chemical compound CCC1=CC=CC(CC)=C1CC VIDOPANCAUPXNH-UHFFFAOYSA-N 0.000 description 1
SLRMQYXOBQWXCR-UHFFFAOYSA-N 2154-56-5 Chemical compound [CH2]C1=CC=CC=C1 SLRMQYXOBQWXCR-UHFFFAOYSA-N 0.000 description 1
239000004593 Epoxy Substances 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
206010053317 Hydrophobia Diseases 0.000 description 1
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
229920002319 Poly(methyl acrylate) Polymers 0.000 description 1
239000011398 Portland cement Substances 0.000 description 1
XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
CIUQDSCDWFSTQR-UHFFFAOYSA-N [C]1=CC=CC=C1 Chemical compound [C]1=CC=CC=C1 CIUQDSCDWFSTQR-UHFFFAOYSA-N 0.000 description 1
JLHADLTXDDGZFX-UHFFFAOYSA-L [[acetyloxy(dibutyl)stannyl]oxy-dibutylstannyl] acetate Chemical compound CCCC[Sn](CCCC)(OC(C)=O)O[Sn](CCCC)(CCCC)OC(C)=O JLHADLTXDDGZFX-UHFFFAOYSA-L 0.000 description 1
UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 description 1
239000003513 alkali Substances 0.000 description 1
229910021529 ammonia Inorganic materials 0.000 description 1
150000005840 aryl radicals Chemical class 0.000 description 1
239000010425 asbestos Substances 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
238000000576 coating method Methods 0.000 description 1
239000012975 dibutyltin dilaurate Substances 0.000 description 1
238000004821 distillation Methods 0.000 description 1
229920001971 elastomer Polymers 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
229910000041 hydrogen chloride Inorganic materials 0.000 description 1
IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
230000003301 hydrolyzing effect Effects 0.000 description 1
238000007654 immersion Methods 0.000 description 1
230000001939 inductive effect Effects 0.000 description 1
VQPKAMAVKYTPLB-UHFFFAOYSA-N lead;octanoic acid Chemical compound [Pb].CCCCCCCC(O)=O VQPKAMAVKYTPLB-UHFFFAOYSA-N 0.000 description 1
238000002156 mixing Methods 0.000 description 1
GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 description 1
125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
150000002897 organic nitrogen compounds Chemical class 0.000 description 1
150000001282 organosilanes Chemical class 0.000 description 1
239000002245 particle Substances 0.000 description 1
230000035515 penetration Effects 0.000 description 1
125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 1
229920000058 polyacrylate Polymers 0.000 description 1
229920001225 polyester resin Polymers 0.000 description 1
239000004645 polyester resin Substances 0.000 description 1
229920000098 polyolefin Polymers 0.000 description 1
239000000843 powder Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
239000002994 raw material Substances 0.000 description 1
229920005989 resin Polymers 0.000 description 1
239000011347 resin Substances 0.000 description 1
229910052895 riebeckite Inorganic materials 0.000 description 1
238000005096 rolling process Methods 0.000 description 1
239000004576 sand Substances 0.000 description 1
238000005507 spraying Methods 0.000 description 1
UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 1
ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 1
239000005052 trichlorosilane Substances 0.000 description 1
239000002966 varnish Substances 0.000 description 1
239000008096 xylene Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/46—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with organic materials
- C04B41/49—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes
- C04B41/4905—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes containing silicon
- C04B41/4922—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes containing silicon applied to the substrate as monomers, i.e. as organosilanes RnSiX4-n, e.g. alkyltrialkoxysilane, dialkyldialkoxysilane

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Ceramic Engineering (AREA)
Materials Engineering (AREA)
Structural Engineering (AREA)
Organic Chemistry (AREA)
Catalysts (AREA)
Compositions Of Macromolecular Compounds (AREA)

CA281,446A 1976-07-21 1977-06-27 Process for bonding inorganic materials Expired CA1128685A (en)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DEP2632835.8		1976-07-21
DE19762632835 DE2632835C3 (de)	1976-07-21	1976-07-21	Verfahren zum Binden von anorganischen Stoffen

Publications (1)

Publication Number	Publication Date
CA1128685A true CA1128685A (en)	1982-07-27

Family

ID=5983600

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA281,446A Expired CA1128685A (en)	1976-07-21	1977-06-27	Process for bonding inorganic materials

Country Status (8)

Country	Link
AT (1)	AT369353B (it)
BE (1)	BE856926A (it)
CA (1)	CA1128685A (it)
CH (1)	CH631426A5 (it)
DE (1)	DE2632835C3 (it)
FR (1)	FR2359098A1 (it)
GB (1)	GB1524790A (it)
IT (1)	IT1079734B (it)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS5911374A (ja) *	1982-07-08	1984-01-20	Nippon Sheet Glass Co Ltd	コ−テイング組成物
DE3332001A1 (de) *	1983-09-05	1984-06-07	Rudolf 8000 München Johne	Verfahren zur entsorgung von kehrichtschlacke von in ihr enthaltenen, loeslichen schadstoffen
US4737562A (en) *	1986-10-15	1988-04-12	Dow Corning Corporation	Self-adhering polyorganosiloxane elastomer compositions and method for preparing same
DE19816973A1 (de) *	1998-04-17	1999-11-25	Degussa	Verfahren zur Imprägnierung von mineralischen Baustoffen und dafür geeignete Organosiliciumverbindungen

1976
- 1976-07-21 DE DE19762632835 patent/DE2632835C3/de not_active Expired
1977
- 1977-06-27 CA CA281,446A patent/CA1128685A/en not_active Expired
- 1977-07-01 IT IT5008277A patent/IT1079734B/it active
- 1977-07-01 GB GB2768077A patent/GB1524790A/en not_active Expired
- 1977-07-19 BE BE179448A patent/BE856926A/xx not_active IP Right Cessation
- 1977-07-20 AT AT524677A patent/AT369353B/de not_active IP Right Cessation
- 1977-07-20 CH CH901777A patent/CH631426A5/de not_active IP Right Cessation
- 1977-07-21 FR FR7722361A patent/FR2359098A1/fr active Granted

Also Published As

Publication number	Publication date
DE2632835A1 (de)	1978-01-26
ATA524677A (de)	1982-05-15
BE856926A (fr)	1978-01-19
DE2632835C3 (de)	1979-10-11
IT1079734B (it)	1985-05-13
AT369353B (de)	1982-12-27
DE2632835B2 (de)	1979-02-15
CH631426A5 (en)	1982-08-13
GB1524790A (en)	1978-09-13
FR2359098A1 (fr)	1978-02-17
FR2359098B1 (it)	1981-01-09

Legal Events

Date	Code	Title	Description
1999-07-27	MKEX	Expiry

Publication	Publication Date	Title
US4757106A (en)	1988-07-12	Aqueous organopolysiloxane emulsions
US6841197B2 (en)	2005-01-11	n-Propylethoxysiloxanes, their preparation and use
US4835014A (en)	1989-05-30	Method for imparting water repellency to absorbent inorganic building materials
US4284548A (en)	1981-08-18	Ambient temperature curable hydroxyl containing polymer/silicon compositions
US3817905A (en)	1974-06-18	Coating composition
US5178668A (en)	1993-01-12	Aqueous water repellent compositions
JP3000242B2 (ja)	2000-01-17	アセトアセテート基又はアセトアセトアミド基を含有するプラスチック前駆体用の硬化剤としてのアルコキシシリルアミン
JPH0737470B2 (ja)	1995-04-26	オルガノシラン
JPH0422945B2 (it)	1992-04-20
JPS61155449A (ja)	1986-07-15	シロキサン組成物
JP3389338B2 (ja)	2003-03-24	加水分解性官能基含有オルガノポリシロキサンの製造方法及び硬化性樹脂組成物
US4218354A (en)	1980-08-19	Binder composition and coating containing the same
CA1234943A (en)	1988-04-05	Curable silicone compositions for the protection of polyurethane foam
EP0068671B1 (en)	1986-04-16	Siloxane compositions and process for treatment of materials
JPS6149319B2 (it)	1986-10-29
US4552942A (en)	1985-11-12	Silanes and compositions prepared therefrom
US4717599A (en)	1988-01-05	Water repellent for masonry
US5336715A (en)	1994-08-09	Organopolysiloxane composition
JPH02284958A (ja)	1990-11-22	液体シリコーン樹脂組成物およびその製造方法
JP2509268B2 (ja)	1996-06-19	無機材料用疎水性改良剤
US3560442A (en)	1971-02-02	Organo - polysiloxane compositions convertible into elastomers at room temperature
US3956570A (en)	1976-05-11	Method for imparting water-repellency to construction materials
US2706723A (en)	1955-04-19	Water repellent treatment for masonry and siloxane composition
CA1128685A (en)	1982-07-27	Process for bonding inorganic materials
JPS62252456A (ja)	1987-11-04	室温硬化性オルガノポリシロキサン組成物