CA1202500A - Methode de preparation d'un herbicide granule soluble a l'eau, a stabilite accrue a la chaleur - Google Patents

Methode de preparation d'un herbicide granule soluble a l'eau, a stabilite accrue a la chaleur

Info

Publication number: CA1202500A
Authority: CA; Canada
Prior art keywords: weight; sodium; amount; dinitro; alpha
Prior art date: 1983-09-06
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000436081A

Other languages

English (en)

Inventor

Pradip K. Mookerjee

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Wyeth Holdings LLC

Original Assignee

American Cyanamid Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-09-06

Filing date

1983-09-06

Publication date

1986-04-01

1983-09-06 Application filed by American Cyanamid Co filed Critical American Cyanamid Co

1983-09-06 Priority to CA000436081A priority Critical patent/CA1202500A/fr

1986-04-01 Application granted granted Critical

1986-04-01 Publication of CA1202500A publication Critical patent/CA1202500A/fr

Status Expired legal-status Critical Current

Links

239000000203 mixture Substances 0.000 title claims abstract description 84
238000000034 method Methods 0.000 title claims abstract description 22
238000002360 preparation method Methods 0.000 title claims abstract description 16
230000002363 herbicidal effect Effects 0.000 title abstract description 29
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title abstract description 20
238000002844 melting Methods 0.000 claims abstract description 9
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 33
239000000843 powder Substances 0.000 claims description 15
239000008187 granular material Substances 0.000 claims description 14
239000002245 particle Substances 0.000 claims description 14
238000009472 formulation Methods 0.000 claims description 13
239000000377 silicon dioxide Substances 0.000 claims description 12
239000000440 bentonite Substances 0.000 claims description 11
229910000278 bentonite Inorganic materials 0.000 claims description 11
SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 11
235000019329 dioctyl sodium sulphosuccinate Nutrition 0.000 claims description 10
YHAIUSTWZPMYGG-UHFFFAOYSA-L disodium;2,2-dioctyl-3-sulfobutanedioate Chemical compound [Na+].[Na+].CCCCCCCCC(C([O-])=O)(C(C([O-])=O)S(O)(=O)=O)CCCCCCCC YHAIUSTWZPMYGG-UHFFFAOYSA-L 0.000 claims description 10
159000000000 sodium salts Chemical class 0.000 claims description 9
238000013019 agitation Methods 0.000 claims description 8
229910021485 fumed silica Inorganic materials 0.000 claims description 8
230000008018 melting Effects 0.000 claims description 8
IZWPGJFSBABFGL-GMFCBQQYSA-M sodium;2-[methyl-[(z)-octadec-9-enoyl]amino]ethanesulfonate Chemical group [Na+].CCCCCCCC\C=C/CCCCCCCC(=O)N(C)CCS([O-])(=O)=O IZWPGJFSBABFGL-GMFCBQQYSA-M 0.000 claims description 8
150000001875 compounds Chemical class 0.000 claims description 7
239000000155 melt Substances 0.000 claims description 7
125000003342 alkenyl group Chemical group 0.000 claims description 6
125000000217 alkyl group Chemical group 0.000 claims description 6
125000000304 alkynyl group Chemical group 0.000 claims description 6
239000002270 dispersing agent Substances 0.000 claims description 6
NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 claims description 6
239000000080 wetting agent Substances 0.000 claims description 6
239000005995 Aluminium silicate Substances 0.000 claims description 5
235000012211 aluminium silicate Nutrition 0.000 claims description 5
239000007864 aqueous solution Substances 0.000 claims description 5
229960000892 attapulgite Drugs 0.000 claims description 5
239000004927 clay Substances 0.000 claims description 5
229910052739 hydrogen Inorganic materials 0.000 claims description 5
230000002209 hydrophobic effect Effects 0.000 claims description 5
NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 5
UYDLBVPAAFVANX-UHFFFAOYSA-N octylphenoxy polyethoxyethanol Chemical compound CC(C)(C)CC(C)(C)C1=CC=C(OCCOCCOCCOCCO)C=C1 UYDLBVPAAFVANX-UHFFFAOYSA-N 0.000 claims description 5
229910052625 palygorskite Inorganic materials 0.000 claims description 5
CHIFOSRWCNZCFN-UHFFFAOYSA-N pendimethalin Chemical group CCC(CC)NC1=C([N+]([O-])=O)C=C(C)C(C)=C1[N+]([O-])=O CHIFOSRWCNZCFN-UHFFFAOYSA-N 0.000 claims description 5
238000003801 milling Methods 0.000 claims description 4
GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims description 3
YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 claims description 3
239000004615 ingredient Substances 0.000 claims description 3
229910052901 montmorillonite Inorganic materials 0.000 claims description 3
238000001816 cooling Methods 0.000 claims description 2
238000002156 mixing Methods 0.000 claims description 2
FBWNMEQMRUMQSO-UHFFFAOYSA-N tergitol NP-9 Chemical compound CCCCCCCCCC1=CC=C(OCCOCCOCCOCCOCCOCCOCCOCCOCCO)C=C1 FBWNMEQMRUMQSO-UHFFFAOYSA-N 0.000 claims description 2
235000012216 bentonite Nutrition 0.000 claims 6
229940092782 bentonite Drugs 0.000 claims 6
239000001257 hydrogen Substances 0.000 claims 4
125000004435 hydrogen atom Chemical group [H]* 0.000 claims 4
125000004178 (C1-C4) alkyl group Chemical group 0.000 claims 2
GXJQMKFJQFGQKV-KHPPLWFESA-N 2-[methyl-[(z)-octadec-9-enoyl]amino]ethanesulfonic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)N(C)CCS(O)(=O)=O GXJQMKFJQFGQKV-KHPPLWFESA-N 0.000 claims 2
239000000378 calcium silicate Substances 0.000 claims 2
229910052918 calcium silicate Inorganic materials 0.000 claims 2
OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 claims 2
125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 claims 2
SMDHCQAYESWHAE-UHFFFAOYSA-N benfluralin Chemical compound CCCCN(CC)C1=C([N+]([O-])=O)C=C(C(F)(F)F)C=C1[N+]([O-])=O SMDHCQAYESWHAE-UHFFFAOYSA-N 0.000 claims 1
238000005469 granulation Methods 0.000 claims 1
230000003179 granulation Effects 0.000 claims 1
238000010438 heat treatment Methods 0.000 claims 1
238000005507 spraying Methods 0.000 claims 1
ZSDSQXJSNMTJDA-UHFFFAOYSA-N trifluralin Chemical compound CCCN(CCC)C1=C([N+]([O-])=O)C=C(C(F)(F)F)C=C1[N+]([O-])=O ZSDSQXJSNMTJDA-UHFFFAOYSA-N 0.000 claims 1
LZGUHMNOBNWABZ-UHFFFAOYSA-N n-nitro-n-phenylnitramide Chemical class [O-][N+](=O)N([N+]([O-])=O)C1=CC=CC=C1 LZGUHMNOBNWABZ-UHFFFAOYSA-N 0.000 abstract description 16
239000004009 herbicide Substances 0.000 description 28
206010001497 Agitation Diseases 0.000 description 7
239000000523 sample Substances 0.000 description 7
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
239000007787 solid Substances 0.000 description 5
230000015572 biosynthetic process Effects 0.000 description 4
239000013078 crystal Substances 0.000 description 4
239000004094 surface-active agent Substances 0.000 description 4
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 3
239000001856 Ethyl cellulose Substances 0.000 description 3
ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 3
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
235000019325 ethyl cellulose Nutrition 0.000 description 3
229920001249 ethyl cellulose Polymers 0.000 description 3
PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 3
239000011734 sodium Substances 0.000 description 3
229910052708 sodium Inorganic materials 0.000 description 3
239000000725 suspension Substances 0.000 description 3
238000012360 testing method Methods 0.000 description 3
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical group C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
-1 Nonylphenoxy Chemical group 0.000 description 2
230000009102 absorption Effects 0.000 description 2
238000010521 absorption reaction Methods 0.000 description 2
239000004495 emulsifiable concentrate Substances 0.000 description 2
229960004279 formaldehyde Drugs 0.000 description 2
235000019256 formaldehyde Nutrition 0.000 description 2
230000005484 gravity Effects 0.000 description 2
239000008233 hard water Substances 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
238000010902 jet-milling Methods 0.000 description 2
239000000463 material Substances 0.000 description 2
230000000717 retained effect Effects 0.000 description 2
239000008234 soft water Substances 0.000 description 2
239000000243 solution Substances 0.000 description 2
239000000758 substrate Substances 0.000 description 2
239000004563 wettable powder Substances 0.000 description 2
MHTNLJYRURGLAC-UHFFFAOYSA-N 3,4-dimethyl-2,6-dinitroaniline Chemical group CC1=CC([N+]([O-])=O)=C(N)C([N+]([O-])=O)=C1C MHTNLJYRURGLAC-UHFFFAOYSA-N 0.000 description 1
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
241000196324 Embryophyta Species 0.000 description 1
239000005909 Kieselgur Substances 0.000 description 1
241000209504 Poaceae Species 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
239000011575 calcium Substances 0.000 description 1
229910052791 calcium Inorganic materials 0.000 description 1
229910000019 calcium carbonate Inorganic materials 0.000 description 1
235000012241 calcium silicate Nutrition 0.000 description 1
239000000969 carrier Substances 0.000 description 1
239000013068 control sample Substances 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
230000000875 corresponding effect Effects 0.000 description 1
125000003963 dichloro group Chemical group Cl* 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000009826 distribution Methods 0.000 description 1
238000011156 evaluation Methods 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
230000009969 flowable effect Effects 0.000 description 1
239000003979 granulating agent Substances 0.000 description 1
125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
239000003701 inert diluent Substances 0.000 description 1
239000003112 inhibitor Substances 0.000 description 1
230000005764 inhibitory process Effects 0.000 description 1
230000014759 maintenance of location Effects 0.000 description 1
239000012768 molten material Substances 0.000 description 1
238000009828 non-uniform distribution Methods 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
239000011369 resultant mixture Substances 0.000 description 1
150000004760 silicates Chemical class 0.000 description 1
125000004469 siloxy group Chemical group [SiH3]O* 0.000 description 1
229920005552 sodium lignosulfonate Polymers 0.000 description 1
239000011343 solid material Substances 0.000 description 1
239000002904 solvent Substances 0.000 description 1
239000007921 spray Substances 0.000 description 1
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
231100000331 toxic Toxicity 0.000 description 1
230000002588 toxic effect Effects 0.000 description 1
238000009736 wetting Methods 0.000 description 1

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Agricultural Chemicals And Associated Chemicals (AREA)

CA000436081A 1983-09-06 1983-09-06 Methode de preparation d'un herbicide granule soluble a l'eau, a stabilite accrue a la chaleur Expired CA1202500A (fr)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CA000436081A CA1202500A (fr)	1983-09-06	1983-09-06	Methode de preparation d'un herbicide granule soluble a l'eau, a stabilite accrue a la chaleur

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CA000436081A CA1202500A (fr)	1983-09-06	1983-09-06	Methode de preparation d'un herbicide granule soluble a l'eau, a stabilite accrue a la chaleur

Publications (1)

Publication Number	Publication Date
CA1202500A true CA1202500A (fr)	1986-04-01

Family

ID=4126021

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000436081A Expired CA1202500A (fr)	1983-09-06	1983-09-06	Methode de preparation d'un herbicide granule soluble a l'eau, a stabilite accrue a la chaleur

Country Status (1)

Country	Link
CA (1)	CA1202500A (fr)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO1993016011A1 (fr) *	1992-02-11	1993-08-19	S.I.A.D. Societa' Italiana Acetilene & Derivati S.P.A.	Masse poreuse sans amiante pour bouteilles a acetylene
CN106332880A (zh) *	2016-08-26	2017-01-18	安徽久易农业股份有限公司	嗪草酮水分散粒剂
CN106332879A (zh) *	2016-08-26	2017-01-18	安徽久易农业股份有限公司	噁唑酰草胺水分散粒剂
CN106332878A (zh) *	2016-08-26	2017-01-18	安徽久易农业股份有限公司	含五氟磺草胺和噁嗪草酮的水分散粒剂
WO2022258424A1 (fr) *	2021-06-11	2022-12-15	Basf Se	Granulé dispersible dans l'eau de dimpropyridaz

1983
- 1983-09-06 CA CA000436081A patent/CA1202500A/fr not_active Expired

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO1993016011A1 (fr) *	1992-02-11	1993-08-19	S.I.A.D. Societa' Italiana Acetilene & Derivati S.P.A.	Masse poreuse sans amiante pour bouteilles a acetylene
CN106332880A (zh) *	2016-08-26	2017-01-18	安徽久易农业股份有限公司	嗪草酮水分散粒剂
CN106332879A (zh) *	2016-08-26	2017-01-18	安徽久易农业股份有限公司	噁唑酰草胺水分散粒剂
CN106332878A (zh) *	2016-08-26	2017-01-18	安徽久易农业股份有限公司	含五氟磺草胺和噁嗪草酮的水分散粒剂
WO2022258424A1 (fr) *	2021-06-11	2022-12-15	Basf Se	Granulé dispersible dans l'eau de dimpropyridaz

Legal Events

Date	Code	Title	Description
2003-09-06	MKEX	Expiry

Publication	Publication Date	Title
EP0112438B1 (fr)	1987-09-09	Procédé pour la préparation de compositions herbicides granulaires dispersibles dans l'eau avec une stabilité thermique augmentée
AU651335B2 (en)	1994-07-21	Water-dispersible or water-soluble pesticide granules from heat-activated binders
US5180420A (en)	1993-01-19	Water dispersible granules
CN108849952B (zh)	2020-11-17	一种吡唑醚菌酯水分散固体组合物及其制备方法
EP0853883A1 (fr)	1998-07-22	Composition chimique a usage agricole a resistance amelioree aux gouttes de pluie
CA1202500A (fr)	1986-04-01	Methode de preparation d'un herbicide granule soluble a l'eau, a stabilite accrue a la chaleur
EP0843964B1 (fr)	2002-10-16	Agent hydratant granulaire
CN102131388B (zh)	2015-01-14	水分散粒剂
US5296450A (en)	1994-03-22	Water dispersible granular herbicidal compositions comprising dinitroaniline herbicides, montmorillonite carrier, and a base
US5294594A (en)	1994-03-15	Water dispersible granular herbicidal compositions comprising dinitroaniline herbicides, montmorillonite carrier and water-swellable polymer
JP3598228B2 (ja)	2004-12-08	粒状農薬水和剤
US5393731A (en)	1995-02-28	Water dispersible granular herbicidal compositions comprising dinitroaniline and imidazolinone herbicides with montmorillonite carriers
JPH04327507A (ja)	1992-11-17	オキシフルオルフエンを含有する分散性粒体
US4197112A (en)	1980-04-08	Water-dispersible herbicide compositions
EP1887865B1 (fr)	2014-10-08	Melanges synergiques de sulfonates de condenses d'(alkyl) naphtalene formaldehyde et de lignosulfonates utiles dans des formulations agrochimiques
HU212609B (en)	1996-09-30	Plant protecting wettable powder compositions
PL170782B1 (en)	1997-01-31	Granulated product dispersible in water
JP4932096B2 (ja)	2012-05-16	除草活性成分を含有する顆粒水和剤及びその製造方法
US4776881A (en)	1988-10-11	Herbicide composition and process
IE48948B1 (en)	1985-06-26	Herbicidal compositions
US4209619A (en)	1980-06-24	Herbicidal complex and formulation
CA2112040C (fr)	2004-11-23	Herbicides pulverulents se dispersant dans l'eau
PL163382B1 (pl)	1994-03-31	Srodek chwastobójczy PL
JP2970666B2 (ja)	1999-11-02	農薬固型製剤
IL111895A (en)	2001-10-31	Water dispersible granular herbicidal compositions comprising dinitroanaline derivatives together with imidazolinone and their preparation

CA1202500A - Methode de preparation d'un herbicide granule soluble a l'eau, a stabilite accrue a la chaleur - Google Patents

Info

Links

Landscapes

Priority Applications (1)

Applications Claiming Priority (1)

Publications (1)

Family

ID=4126021

Family Applications (1)

Country Status (1)

Cited By (5)

Cited By (5)

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