CA1263765A - Procede et dispositif d'introduction d'echantillons pour spectrometre de masse - Google Patents

Procede et dispositif d'introduction d'echantillons pour spectrometre de masse

Info

Publication number: CA1263765A
Authority: CA; Canada
Prior art keywords: micro; sample; flow; tube; reactor
Prior art date: 1985-04-24
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA000507538A

Other languages

English (en)

French (fr)

Inventor

Robert Boyer

Jean-Pierre Journoux

Claude Duval

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Orano Demantelement SAS

Original Assignee

Compagnie Generale des Matieres Nucleaires SA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-04-24

Filing date

1986-04-24

Publication date

1989-12-05

1986-04-24 Application filed by Compagnie Generale des Matieres Nucleaires SA filed Critical Compagnie Generale des Matieres Nucleaires SA

1989-12-05 Application granted granted Critical

1989-12-05 Publication of CA1263765A publication Critical patent/CA1263765A/fr

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 17
230000008569 process Effects 0.000 title claims description 4
238000010438 heat treatment Methods 0.000 claims abstract description 13
150000001875 compounds Chemical class 0.000 claims abstract description 12
238000000859 sublimation Methods 0.000 claims abstract description 9
230000008022 sublimation Effects 0.000 claims abstract description 8
239000003153 chemical reaction reagent Substances 0.000 claims abstract description 6
239000000523 sample Substances 0.000 claims description 29
230000000694 effects Effects 0.000 claims description 5
239000012530 fluid Substances 0.000 claims description 3
230000001105 regulatory effect Effects 0.000 claims description 3
240000008042 Zea mays Species 0.000 claims 1
235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims 1
235000002017 Zea mays subsp mays Nutrition 0.000 claims 1
235000005822 corn Nutrition 0.000 claims 1
238000004519 manufacturing process Methods 0.000 claims 1
238000001819 mass spectrum Methods 0.000 claims 1
230000001131 transforming effect Effects 0.000 abstract 1
239000007789 gas Substances 0.000 description 19
150000002500 ions Chemical class 0.000 description 16
238000004458 analytical method Methods 0.000 description 9
238000005259 measurement Methods 0.000 description 8
230000000155 isotopic effect Effects 0.000 description 6
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
230000008901 benefit Effects 0.000 description 5
239000007788 liquid Substances 0.000 description 4
239000000047 product Substances 0.000 description 4
229910052770 Uranium Inorganic materials 0.000 description 3
238000010884 ion-beam technique Methods 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
239000000126 substance Substances 0.000 description 3
DNYWZCXLKNTFFI-UHFFFAOYSA-N uranium Chemical compound [U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U] DNYWZCXLKNTFFI-UHFFFAOYSA-N 0.000 description 3
SANRKQGLYCLAFE-UHFFFAOYSA-H uranium hexafluoride Chemical compound F[U](F)(F)(F)(F)F SANRKQGLYCLAFE-UHFFFAOYSA-H 0.000 description 3
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
230000009471 action Effects 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
230000001276 controlling effect Effects 0.000 description 2
238000010586 diagram Methods 0.000 description 2
238000005485 electric heating Methods 0.000 description 2
229910052731 fluorine Inorganic materials 0.000 description 2
239000011737 fluorine Substances 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
238000005086 pumping Methods 0.000 description 2
238000012546 transfer Methods 0.000 description 2
101100299656 Caenorhabditis elegans puf-6 gene Proteins 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
206010012289 Dementia Diseases 0.000 description 1
229910000792 Monel Inorganic materials 0.000 description 1
229910002651 NO3 Inorganic materials 0.000 description 1
229910052778 Plutonium Inorganic materials 0.000 description 1
239000012080 ambient air Substances 0.000 description 1
230000033228 biological regulation Effects 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
238000001816 cooling Methods 0.000 description 1
238000012937 correction Methods 0.000 description 1
239000013078 crystal Substances 0.000 description 1
230000009089 cytolysis Effects 0.000 description 1
230000007423 decrease Effects 0.000 description 1
238000007872 degassing Methods 0.000 description 1
238000013461 design Methods 0.000 description 1
230000009977 dual effect Effects 0.000 description 1
230000005684 electric field Effects 0.000 description 1
238000010894 electron beam technology Methods 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
239000012025 fluorinating agent Substances 0.000 description 1
238000003682 fluorination reaction Methods 0.000 description 1
230000004907 flux Effects 0.000 description 1
239000000446 fuel Substances 0.000 description 1
239000001307 helium Substances 0.000 description 1
229910052734 helium Inorganic materials 0.000 description 1
SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
230000003993 interaction Effects 0.000 description 1
239000000463 material Substances 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
239000000203 mixture Substances 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
229910001120 nichrome Inorganic materials 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
150000002829 nitrogen Chemical class 0.000 description 1
210000000056 organ Anatomy 0.000 description 1
239000002245 particle Substances 0.000 description 1
239000012071 phase Substances 0.000 description 1
OYEHPCDNVJXUIW-UHFFFAOYSA-N plutonium atom Chemical compound [Pu] OYEHPCDNVJXUIW-UHFFFAOYSA-N 0.000 description 1
230000002285 radioactive effect Effects 0.000 description 1
239000003870 refractory metal Substances 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000007790 solid phase Substances 0.000 description 1
238000007711 solidification Methods 0.000 description 1
238000004611 spectroscopical analysis Methods 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
230000006641 stabilisation Effects 0.000 description 1
238000011105 stabilization Methods 0.000 description 1
238000011144 upstream manufacturing Methods 0.000 description 1
239000003039 volatile agent Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
238000003466 welding Methods 0.000 description 1

Classifications

- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0422—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for gaseous samples
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0468—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0495—Vacuum locks; Valves

Landscapes

Chemical & Material Sciences (AREA)
Analytical Chemistry (AREA)
Other Investigation Or Analysis Of Materials By Electrical Means (AREA)

CA000507538A 1985-04-24 1986-04-24 Procede et dispositif d'introduction d'echantillons pour spectrometre de masse Expired CA1263765A (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
FR8506257		1985-04-24
FR8506257A FR2581246B1 (fr)	1985-04-24	1985-04-24	Procede et dispositif d'introduction d'echantillons pour spectrometre de masse

Publications (1)

Publication Number	Publication Date
CA1263765A true CA1263765A (fr)	1989-12-05

Family

ID=9318634

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA000507538A Expired CA1263765A (fr)	1985-04-24	1986-04-24	Procede et dispositif d'introduction d'echantillons pour spectrometre de masse

Country Status (5)

Country	Link
EP (1)	EP0200645B1 (de)
CA (1)	CA1263765A (de)
DE (1)	DE3664401D1 (de)
FR (1)	FR2581246B1 (de)
WO (1)	WO1986006545A1 (de)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2629270B2 (fr) *	1988-03-25	1990-12-28	Cogema	Dispositif d'introduction d'echantillons pour spectrometre de masse

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR1132049A (fr) *	1954-05-26	1957-03-04	Thomson Houston Comp Francaise	Dispositif d'introduction d'un échantillon dans un spectrographe de masse
US3888107A (en) *	1969-10-08	1975-06-10	Dow Chemical Co	Differential thermal analysis cell assembly
DE3269499D1 (en) *	1981-11-30	1986-04-03	Vg Instr Group	Automatic mass spectrometer inlet system

1985
- 1985-04-24 FR FR8506257A patent/FR2581246B1/fr not_active Expired
1986
- 1986-04-24 CA CA000507538A patent/CA1263765A/fr not_active Expired
- 1986-04-24 EP EP19860400902 patent/EP0200645B1/de not_active Expired
- 1986-04-24 WO PCT/FR1986/000140 patent/WO1986006545A1/fr not_active Ceased
- 1986-04-24 DE DE8686400902T patent/DE3664401D1/de not_active Expired

Also Published As

Publication number	Publication date
EP0200645B1 (de)	1989-07-12
DE3664401D1 (en)	1989-08-17
FR2581246A1 (fr)	1986-10-31
FR2581246B1 (fr)	1987-07-10
WO1986006545A1 (fr)	1986-11-06
EP0200645A1 (de)	1986-11-05

Legal Events

Date	Code	Title	Description
1994-06-05	MKLA	Lapsed

Publication	Publication Date	Title
Chan et al.	1991	Study of laser-material interactions using inductively coupled plasma-atomic emission spectrometry
US4902891A (en)	1990-02-20	Thermospray methods and apparatus for interfacing chromatography and mass spectrometry
FR2627863A1 (fr)	1989-09-01	Procede et dispositif pour l'analyse de gaz contenant du fluor et pour controler la concentration en fluor dans un gaz de laser excimeur
Ballance et al.	2018	A short response time atomic source for trapped ion experiments
US4933548A (en)	1990-06-12	Method and device for introducing samples for a mass spectrometer
CA1263765A (fr)	1989-12-05	Procede et dispositif d'introduction d'echantillons pour spectrometre de masse
Peruski et al.	2022	Cell design for laser-induced breakdown spectroscopy measurements on reactive gas samples
Buttersack et al.	2020	Deeply cooled and temperature controlled microjets: Liquid ammonia solutions released into vacuum for analysis by photoelectron spectroscopy
EP0104973B1 (de)	1987-05-27	Vorrichtung zur Ionisierung eines Materials durch Hochtemperaturheizung
FR2510761A1 (fr)	1983-02-04	Appareil de mesure des concentrations dans l'air des produits de filiation de radon et de thoron
Imai et al.	1995	Investigations of pyrolysed ascorbic acid in an electrothermal graphite furnace by inductively coupled argon plasma mass spectrometry and Raman spectrometry
JP2003247920A (ja)	2003-09-05	軽元素を含有する固体試料の組成比分析方法
JPH0331762A (ja)	1991-02-12	固体試料の分解方法
FR2629270A2 (fr)	1989-09-29	Dispositif d'introduction d'echantillons pour spectrometre de masse
JP2557435B2 (ja)	1996-11-27	誘導結合プラズマ質量分析用試料導入装置
JP2557473B2 (ja)	1996-11-27	誘導結合プラズマ質量分析用試料導入装置
Krause	1973	Apparatus for producing sticks of solid deuterium
JP2003075408A (ja)	2003-03-12	固体試料の金属元素分析方法およびその分析装置
WO1992015004A1 (fr)	1992-09-03	Appareil pour l'echantillonnage des liquides
Doyle	1995	A 1m normal incidence multi-channel spectrometer for laser plasma spectroscopy
Matos et al.	2012	Generation of an atomic beam by using laser ablation for isotope separation purposes
JP2623179B2 (ja)	1997-06-25	マススペクトロメータによる試料の気化分析方法
Goodfellow et al.	1995	Experimental verification of a high-current cathode thermal model
FR2684497A1 (fr)	1993-06-04	Laser impulsionnel.
JPS6296850A (ja)	1987-05-06	フア−ネスプラズマ発光分析装置