CA2034475C - Methode de cristallisation de fructose anhydre a partir de ses solutions aqueuses - Google Patents
Methode de cristallisation de fructose anhydre a partir de ses solutions aqueuses Download PDFInfo
- Publication number
- CA2034475C CA2034475C CA002034475A CA2034475A CA2034475C CA 2034475 C CA2034475 C CA 2034475C CA 002034475 A CA002034475 A CA 002034475A CA 2034475 A CA2034475 A CA 2034475A CA 2034475 C CA2034475 C CA 2034475C
- Authority
- CA
- Canada
- Prior art keywords
- crystallizer
- fructose
- cooling
- blades
- crystallization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229930091371 Fructose Natural products 0.000 title claims abstract description 56
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 title claims abstract description 56
- 239000005715 Fructose Substances 0.000 title claims abstract description 56
- 238000000034 method Methods 0.000 title claims abstract description 47
- 239000007864 aqueous solution Substances 0.000 title claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 48
- 239000000243 solution Substances 0.000 claims abstract description 28
- 238000012546 transfer Methods 0.000 claims abstract description 21
- 238000002156 mixing Methods 0.000 claims abstract description 18
- 239000000126 substance Substances 0.000 claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 claims abstract description 12
- 238000010899 nucleation Methods 0.000 claims abstract description 7
- 150000002231 fructose derivatives Chemical class 0.000 claims abstract description 4
- 239000006193 liquid solution Substances 0.000 claims abstract 3
- 238000002425 crystallisation Methods 0.000 claims description 51
- 230000008025 crystallization Effects 0.000 claims description 50
- 239000013078 crystal Substances 0.000 claims description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000000047 product Substances 0.000 description 14
- 239000007788 liquid Substances 0.000 description 11
- 239000006188 syrup Substances 0.000 description 11
- 235000020357 syrup Nutrition 0.000 description 11
- 239000000498 cooling water Substances 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- 239000003960 organic solvent Substances 0.000 description 6
- 238000001035 drying Methods 0.000 description 4
- 238000000227 grinding Methods 0.000 description 4
- 239000007787 solid Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 239000002178 crystalline material Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 235000021433 fructose syrup Nutrition 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000011031 large-scale manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 238000010979 pH adjustment Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000005029 sieve analysis Methods 0.000 description 2
- 230000002269 spontaneous effect Effects 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 235000009421 Myristica fragrans Nutrition 0.000 description 1
- LKDRXBCSQODPBY-ZXXMMSQZSA-N alpha-D-fructopyranose Chemical compound OC[C@]1(O)OC[C@@H](O)[C@@H](O)[C@@H]1O LKDRXBCSQODPBY-ZXXMMSQZSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 239000008121 dextrose Substances 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012527 feed solution Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 239000001115 mace Substances 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000011369 resultant mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000013341 scale-up Methods 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
- C07H3/02—Monosaccharides
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
- Seasonings (AREA)
- Jellies, Jams, And Syrups (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US46705590A | 1990-01-18 | 1990-01-18 | |
| US467,055 | 1990-01-18 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2034475A1 CA2034475A1 (fr) | 1991-07-19 |
| CA2034475C true CA2034475C (fr) | 2002-10-08 |
Family
ID=23854166
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002034475A Expired - Lifetime CA2034475C (fr) | 1990-01-18 | 1991-01-17 | Methode de cristallisation de fructose anhydre a partir de ses solutions aqueuses |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JP3165966B2 (fr) |
| KR (1) | KR0170405B1 (fr) |
| CA (1) | CA2034475C (fr) |
| DE (1) | DE4041317B4 (fr) |
| FI (1) | FI104738B (fr) |
| RU (1) | RU2050417C1 (fr) |
| UA (1) | UA10895A (fr) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP4352069A4 (fr) * | 2021-05-08 | 2025-03-26 | Petiva Private Limited | Système et procédé de cristallisation de d-allulose à partir d'une solution de d-allulose |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12590116B2 (en) | 2016-10-28 | 2026-03-31 | Tate & Lyle Solutions Usa Llc | Method for producing allulose crystals |
| US20200040023A1 (en) | 2016-10-28 | 2020-02-06 | Tate & Lyle Ingredients Americas Llc | Method for producing allulose crystals |
| DE102018131131B4 (de) | 2018-12-06 | 2025-10-16 | Bma Braunschweigische Maschinenbauanstalt Gmbh | Kontinuierliches Verfahren zur Gewinnung eines kristallinen Monosaccharides |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1456260A (en) * | 1974-01-28 | 1976-11-24 | Suomen Sokeri Oy | Method for crystallization of fructose from water solution |
| FR2582016B1 (fr) * | 1985-05-15 | 1987-09-18 | Roquette Freres | Procede et installation de production de fructose cristallise anhydre |
-
1990
- 1990-12-21 DE DE4041317A patent/DE4041317B4/de not_active Expired - Lifetime
-
1991
- 1991-01-09 FI FI910117A patent/FI104738B/fi active
- 1991-01-17 RU SU914894629A patent/RU2050417C1/ru not_active IP Right Cessation
- 1991-01-17 JP JP01716591A patent/JP3165966B2/ja not_active Expired - Lifetime
- 1991-01-17 UA UA4894629A patent/UA10895A/uk unknown
- 1991-01-17 CA CA002034475A patent/CA2034475C/fr not_active Expired - Lifetime
- 1991-01-18 KR KR1019910000824A patent/KR0170405B1/ko not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP4352069A4 (fr) * | 2021-05-08 | 2025-03-26 | Petiva Private Limited | Système et procédé de cristallisation de d-allulose à partir d'une solution de d-allulose |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH04325100A (ja) | 1992-11-13 |
| KR910014393A (ko) | 1991-08-31 |
| FI104738B (fi) | 2000-03-31 |
| DE4041317B4 (de) | 2005-09-08 |
| DE4041317A1 (de) | 1991-07-25 |
| UA10895A (uk) | 1996-12-25 |
| CA2034475A1 (fr) | 1991-07-19 |
| FI910117A0 (fi) | 1991-01-09 |
| KR0170405B1 (ko) | 1999-02-01 |
| JP3165966B2 (ja) | 2001-05-14 |
| FI910117L (fi) | 1991-07-19 |
| RU2050417C1 (ru) | 1995-12-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed | ||
| MKEC | Expiry (correction) |
Effective date: 20121202 |