CA2592499C - Procede de preparation de zeolite a, un adjuvant pour detergent, a partir de residus de kimberlite - Google Patents

Procede de preparation de zeolite a, un adjuvant pour detergent, a partir de residus de kimberlite Download PDF

Info

Publication number: CA2592499C
Authority: CA; Canada
Prior art keywords: range; zeolite; kimberlite; product; acid
Prior art date: 2004-12-30
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA2592499A

Other languages

English (en)

Other versions

CA2592499A1 (fr

Inventor

Raksh Vir Jasra

R. S. Somani

H. M. Mody

H. C. Bajaj

J. R. Chunawala

Hemal Ranpara

Dipti Barochiya

Devendra Ghelani

Suresh Chandra

M. K. Dhar

Keshav Rao

Kamlesh Kumar

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Council of Scientific and Industrial Research CSIR

National Mineral Development Corp Ltd

Original Assignee

Council of Scientific and Industrial Research CSIR

National Mineral Development Corp Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2004-12-30

Filing date

2004-12-30

Publication date

2012-10-16

2004-12-30 Application filed by Council of Scientific and Industrial Research CSIR, National Mineral Development Corp Ltd filed Critical Council of Scientific and Industrial Research CSIR

2006-07-06 Publication of CA2592499A1 publication Critical patent/CA2592499A1/fr

2012-10-16 Application granted granted Critical

2012-10-16 Publication of CA2592499C publication Critical patent/CA2592499C/fr

2024-12-30 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

239000003599 detergent Substances 0.000 title claims abstract description 40
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title claims description 56
239000010457 zeolite Substances 0.000 title claims description 33
229910021536 Zeolite Inorganic materials 0.000 title claims description 26
238000004519 manufacturing process Methods 0.000 title claims description 16
JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 claims abstract description 93
238000000034 method Methods 0.000 claims abstract description 70
239000004115 Sodium Silicate Substances 0.000 claims abstract description 57
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 57
229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 57
239000002253 acid Substances 0.000 claims abstract description 56
239000000203 mixture Substances 0.000 claims abstract description 22
229910003460 diamond Inorganic materials 0.000 claims abstract description 21
239000010432 diamond Substances 0.000 claims abstract description 21
239000003513 alkali Substances 0.000 claims abstract description 18
238000005065 mining Methods 0.000 claims abstract description 18
239000002910 solid waste Substances 0.000 claims abstract description 12
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 138
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 118
239000000047 product Substances 0.000 claims description 65
229910001868 water Inorganic materials 0.000 claims description 54
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 53
229910052681 coesite Inorganic materials 0.000 claims description 51
229910052906 cristobalite Inorganic materials 0.000 claims description 51
229910052682 stishovite Inorganic materials 0.000 claims description 51
229910052905 tridymite Inorganic materials 0.000 claims description 51
KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 46
235000011121 sodium hydroxide Nutrition 0.000 claims description 46
ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 claims description 44
229910001388 sodium aluminate Inorganic materials 0.000 claims description 44
239000000377 silicon dioxide Substances 0.000 claims description 42
239000002002 slurry Substances 0.000 claims description 36
238000003756 stirring Methods 0.000 claims description 36
229910000323 aluminium silicate Inorganic materials 0.000 claims description 33
239000000706 filtrate Substances 0.000 claims description 23
239000000126 substance Substances 0.000 claims description 22
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 20
239000000843 powder Substances 0.000 claims description 19
238000001914 filtration Methods 0.000 claims description 18
239000012535 impurity Substances 0.000 claims description 18
239000000395 magnesium oxide Substances 0.000 claims description 18
229910001220 stainless steel Inorganic materials 0.000 claims description 18
239000010935 stainless steel Substances 0.000 claims description 18
235000012239 silicon dioxide Nutrition 0.000 claims description 17
RREGISFBPQOLTM-UHFFFAOYSA-N alumane;trihydrate Chemical compound O.O.O.[AlH3] RREGISFBPQOLTM-UHFFFAOYSA-N 0.000 claims description 16
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 15
238000010438 heat treatment Methods 0.000 claims description 14
239000002245 particle Substances 0.000 claims description 14
238000009835 boiling Methods 0.000 claims description 12
239000007787 solid Substances 0.000 claims description 12
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
238000011282 treatment Methods 0.000 claims description 10
229910052593 corundum Inorganic materials 0.000 claims description 9
229910052500 inorganic mineral Inorganic materials 0.000 claims description 9
235000010755 mineral Nutrition 0.000 claims description 9
239000011707 mineral Substances 0.000 claims description 9
238000005406 washing Methods 0.000 claims description 9
229910001845 yogo sapphire Inorganic materials 0.000 claims description 9
239000000470 constituent Substances 0.000 claims description 8
238000001035 drying Methods 0.000 claims description 8
JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 8
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 7
229910017604 nitric acid Inorganic materials 0.000 claims description 7
102000005701 Calcium-Binding Proteins Human genes 0.000 claims description 6
108010045403 Calcium-Binding Proteins Proteins 0.000 claims description 6
238000010306 acid treatment Methods 0.000 claims description 6
238000001816 cooling Methods 0.000 claims description 6
238000010298 pulverizing process Methods 0.000 claims description 6
239000007858 starting material Substances 0.000 claims description 5
229910052799 carbon Inorganic materials 0.000 claims description 4
238000004090 dissolution Methods 0.000 claims description 4
239000008394 flocculating agent Substances 0.000 claims description 4
150000004684 trihydrates Chemical class 0.000 claims description 3
238000002360 preparation method Methods 0.000 abstract description 24
229910052782 aluminium Inorganic materials 0.000 abstract description 8
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract description 7
239000004411 aluminium Substances 0.000 abstract 1
238000009472 formulation Methods 0.000 abstract 1
CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 28
238000002425 crystallisation Methods 0.000 description 17
230000008025 crystallization Effects 0.000 description 17
238000002441 X-ray diffraction Methods 0.000 description 15
230000015572 biosynthetic process Effects 0.000 description 14
239000008367 deionised water Substances 0.000 description 10
229910021641 deionized water Inorganic materials 0.000 description 10
239000008399 tap water Substances 0.000 description 10
235000020679 tap water Nutrition 0.000 description 10
239000000463 material Substances 0.000 description 9
239000011541 reaction mixture Substances 0.000 description 8
238000010992 reflux Methods 0.000 description 8
238000006243 chemical reaction Methods 0.000 description 7
239000013078 crystal Substances 0.000 description 7
238000002156 mixing Methods 0.000 description 7
238000003860 storage Methods 0.000 description 7
239000003054 catalyst Substances 0.000 description 6
239000012071 phase Substances 0.000 description 6
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 5
229910019142 PO4 Inorganic materials 0.000 description 5
239000011575 calcium Substances 0.000 description 5
230000004927 fusion Effects 0.000 description 5
239000007788 liquid Substances 0.000 description 5
235000021317 phosphate Nutrition 0.000 description 5
238000003786 synthesis reaction Methods 0.000 description 5
238000004458 analytical method Methods 0.000 description 4
229910052791 calcium Inorganic materials 0.000 description 4
230000029087 digestion Effects 0.000 description 4
239000002994 raw material Substances 0.000 description 4
235000019832 sodium triphosphate Nutrition 0.000 description 4
-1 Aluminum alkoxide Chemical class 0.000 description 3
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
WYTGDNHDOZPMIW-RCBQFDQVSA-N alstonine Natural products C1=CC2=C3C=CC=CC3=NC2=C2N1C[C@H]1[C@H](C)OC=C(C(=O)OC)[C@H]1C2 WYTGDNHDOZPMIW-RCBQFDQVSA-N 0.000 description 3
150000001768 cations Chemical class 0.000 description 3
239000010881 fly ash Substances 0.000 description 3
XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 3
229910052622 kaolinite Inorganic materials 0.000 description 3
239000011777 magnesium Substances 0.000 description 3
229910052749 magnesium Inorganic materials 0.000 description 3
150000002894 organic compounds Chemical class 0.000 description 3
150000003013 phosphoric acid derivatives Chemical class 0.000 description 3
238000000926 separation method Methods 0.000 description 3
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
101100348017 Drosophila melanogaster Nazo gene Proteins 0.000 description 2
241001659863 Panna Species 0.000 description 2
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
239000003463 adsorbent Substances 0.000 description 2
150000004645 aluminates Chemical class 0.000 description 2
238000005341 cation exchange Methods 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000004744 fabric Substances 0.000 description 2
238000000227 grinding Methods 0.000 description 2
239000008233 hard water Substances 0.000 description 2
239000003999 initiator Substances 0.000 description 2
229910052742 iron Inorganic materials 0.000 description 2
238000002386 leaching Methods 0.000 description 2
238000010899 nucleation Methods 0.000 description 2
150000007524 organic acids Chemical class 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
239000010452 phosphate Substances 0.000 description 2
238000000053 physical method Methods 0.000 description 2
238000000746 purification Methods 0.000 description 2
229910001948 sodium oxide Inorganic materials 0.000 description 2
239000010936 titanium Substances 0.000 description 2
229910052719 titanium Inorganic materials 0.000 description 2
229910016523 CuKa Inorganic materials 0.000 description 1
JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 description 1
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
229920000388 Polyphosphate Polymers 0.000 description 1
108091006629 SLC13A2 Proteins 0.000 description 1
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
239000004809 Teflon Substances 0.000 description 1
229920006362 Teflon® Polymers 0.000 description 1
BFRXZIMAUMUZJH-UHFFFAOYSA-M [OH-].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] Chemical compound [OH-].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] BFRXZIMAUMUZJH-UHFFFAOYSA-M 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
230000010933 acylation Effects 0.000 description 1
238000005917 acylation reaction Methods 0.000 description 1
230000032683 aging Effects 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
230000029936 alkylation Effects 0.000 description 1
238000005804 alkylation reaction Methods 0.000 description 1
229940037003 alum Drugs 0.000 description 1
WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
229910021502 aluminium hydroxide Inorganic materials 0.000 description 1
JEWHCPOELGJVCB-UHFFFAOYSA-N aluminum;calcium;oxido-[oxido(oxo)silyl]oxy-oxosilane;potassium;sodium;tridecahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.O.O.O.[Na].[Al].[K].[Ca].[O-][Si](=O)O[Si]([O-])=O JEWHCPOELGJVCB-UHFFFAOYSA-N 0.000 description 1
150000008064 anhydrides Chemical class 0.000 description 1
239000012736 aqueous medium Substances 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
230000009286 beneficial effect Effects 0.000 description 1
238000001354 calcination Methods 0.000 description 1
235000010216 calcium carbonate Nutrition 0.000 description 1
229910000019 calcium carbonate Inorganic materials 0.000 description 1
229910001424 calcium ion Inorganic materials 0.000 description 1
239000000919 ceramic Substances 0.000 description 1
238000009614 chemical analysis method Methods 0.000 description 1
239000008119 colloidal silica Substances 0.000 description 1
230000002860 competitive effect Effects 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
239000002274 desiccant Substances 0.000 description 1
239000012153 distilled water Substances 0.000 description 1
238000009837 dry grinding Methods 0.000 description 1
230000007613 environmental effect Effects 0.000 description 1
230000007717 exclusion Effects 0.000 description 1
230000003311 flocculating effect Effects 0.000 description 1
239000003517 fume Substances 0.000 description 1
125000000524 functional group Chemical group 0.000 description 1
ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
239000007789 gas Substances 0.000 description 1
229910001679 gibbsite Inorganic materials 0.000 description 1
229910001385 heavy metal Inorganic materials 0.000 description 1
230000007062 hydrolysis Effects 0.000 description 1
238000006460 hydrolysis reaction Methods 0.000 description 1
238000005216 hydrothermal crystallization Methods 0.000 description 1
238000010335 hydrothermal treatment Methods 0.000 description 1
229910010272 inorganic material Inorganic materials 0.000 description 1
239000011147 inorganic material Substances 0.000 description 1
229910052909 inorganic silicate Inorganic materials 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
159000000014 iron salts Chemical class 0.000 description 1
238000006317 isomerization reaction Methods 0.000 description 1
238000007561 laser diffraction method Methods 0.000 description 1
229910001425 magnesium ion Inorganic materials 0.000 description 1
159000000003 magnesium salts Chemical class 0.000 description 1
239000011738 major mineral Substances 0.000 description 1
235000011963 major mineral Nutrition 0.000 description 1
238000003801 milling Methods 0.000 description 1
239000002808 molecular sieve Substances 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
238000010979 pH adjustment Methods 0.000 description 1
238000005504 petroleum refining Methods 0.000 description 1
229910001743 phillipsite Inorganic materials 0.000 description 1
239000000049 pigment Substances 0.000 description 1
239000001205 polyphosphate Substances 0.000 description 1
235000011176 polyphosphates Nutrition 0.000 description 1
239000011148 porous material Substances 0.000 description 1
238000000634 powder X-ray diffraction Methods 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
239000011164 primary particle Substances 0.000 description 1
238000012545 processing Methods 0.000 description 1
238000011002 quantification Methods 0.000 description 1
239000000376 reactant Substances 0.000 description 1
239000012066 reaction slurry Substances 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
238000011160 research Methods 0.000 description 1
238000004062 sedimentation Methods 0.000 description 1
238000007873 sieving Methods 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
239000000344 soap Substances 0.000 description 1
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
229910001415 sodium ion Inorganic materials 0.000 description 1
GROMGGTZECPEKN-UHFFFAOYSA-N sodium metatitanate Chemical compound [Na+].[Na+].[O-][Ti](=O)O[Ti](=O)O[Ti]([O-])=O GROMGGTZECPEKN-UHFFFAOYSA-N 0.000 description 1
239000011973 solid acid Substances 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
241000894007 species Species 0.000 description 1
239000001117 sulphuric acid Substances 0.000 description 1
235000011149 sulphuric acid Nutrition 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
238000005320 surfactant adsorption Methods 0.000 description 1
230000002194 synthesizing effect Effects 0.000 description 1
230000009466 transformation Effects 0.000 description 1
238000000844 transformation Methods 0.000 description 1
230000007704 transition Effects 0.000 description 1
238000010977 unit operation Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/128—Aluminium silicates, e.g. zeolites

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Dispersion Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Silicates, Zeolites, And Molecular Sieves (AREA)

CA2592499A 2004-12-30 2004-12-30 Procede de preparation de zeolite a, un adjuvant pour detergent, a partir de residus de kimberlite Expired - Fee Related CA2592499C (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
PCT/IN2004/000436 WO2006070399A1 (fr)	2004-12-30	2004-12-30	Procédé de préparation de zéolite a, un adjuvant pour détergent, à partir de résidus de kimberlite

Publications (2)

Publication Number	Publication Date
CA2592499A1 CA2592499A1 (fr)	2006-07-06
CA2592499C true CA2592499C (fr)	2012-10-16

Family

ID=34960560

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA2592499A Expired - Fee Related CA2592499C (fr)	2004-12-30	2004-12-30	Procede de preparation de zeolite a, un adjuvant pour detergent, a partir de residus de kimberlite

Country Status (3)

Country	Link
CN (1)	CN101090864B (fr)
CA (1)	CA2592499C (fr)
WO (1)	WO2006070399A1 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB201406268D0 (en) *	2014-04-08	2014-05-21	Pq Silicas Uk Ltd	Particulate zeolite composition
CN105271297A (zh) *	2015-10-22	2016-01-27	北京科技大学	一种利用尾矿制备4a分子筛的方法及其应用
CN105858674B (zh) *	2016-03-28	2018-03-02	大唐国际发电股份有限公司高铝煤炭资源开发利用研发中心	一种利用高铝粉煤灰制备方钠石的方法
CN110814850B (zh) *	2019-12-19	2021-06-25	淮安展德光电科技有限公司	一种车床加工屑处理装置
CN117623325B (zh) *	2023-12-19	2025-08-29	南昌航空大学	一种以报废化铣液为原料制备沸石的方法
CN118634780B (zh) *	2024-06-12	2025-01-21	中电建路桥集团有限公司	一种石材矿山尾矿渣制备环境修复功能材料的方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP1351882B1 (fr) *	2000-12-19	2004-10-06	National Aluminium Company Limited	Procede de fabrication de zeolite a utile en tant qu'adjuvant pour detergent

2004
- 2004-12-30 CA CA2592499A patent/CA2592499C/fr not_active Expired - Fee Related
- 2004-12-30 CN CN2004800447908A patent/CN101090864B/zh not_active Expired - Fee Related
- 2004-12-30 WO PCT/IN2004/000436 patent/WO2006070399A1/fr not_active Ceased

Also Published As

Publication number	Publication date
CN101090864B (zh)	2010-12-22
CN101090864A (zh)	2007-12-19
CA2592499A1 (fr)	2006-07-06
WO2006070399A1 (fr)	2006-07-06

Legal Events

Date	Code	Title	Description
2009-12-17	EEER	Examination request
2019-02-11	MKLA	Lapsed	Effective date: 20181231

Publication	Publication Date	Title
US7560093B2 (en)	2009-07-14	Process for preparing detergent builder Zeolite-A from Kimberlite tailings
Ayele et al.	2015	Synthesis of zeolite A from Ethiopian kaolin
JPH05503065A (ja)	1993-05-27	結晶二珪酸ナトリウムの熱水製造方法
US20090022646A1 (en)	2009-01-22	Process for hydrothermal production of sodium silicate solutions and precipitated silicas
JP2022513266A (ja)	2022-02-07	ゼオライトおよびその製造方法
EP0720587A1 (fr)	1996-07-10	Procede de fabrication de billes de silice a partir d'olivine
CA2592499C (fr)	2012-10-16	Procede de preparation de zeolite a, un adjuvant pour detergent, a partir de residus de kimberlite
US5236681A (en)	1993-08-17	Layered silicate
CA2629083C (fr)	2014-05-27	Procede de fabrication de silicate de sodium a partir de trainees de kimberlite
US6054106A (en)	2000-04-25	Magnesiosilicates
La Iglesia et al.	2002	Zeolite synthesis employing alkaline waste effluents from the aluminum industry
EP1027285B1 (fr)	2002-03-27	Procede de production de zeolite a partir de matieres premieres renfermant des alumino hydro-silicates alcalins
CA2057588C (fr)	2000-03-28	Procede pour l'obtention de zeolite 4a a partir de bauxite
JPH06239612A (ja)	1994-08-30	下水汚泥焼却灰からのゼオライト系鉱物の製法
KR20100085606A (ko)	2010-07-29	메카노케미칼 반응에 의한 페로니켈슬래그로부터 제올라이트 제조
Rozhkovskaya	2021	Synthesis of high quality zeolite from alum sludge for water treatment applications
KR20060013227A (ko)	2006-02-09	제올라이트의 제조방법
KR100420104B1 (ko)	2004-03-02	소듐세스퀴카보네이트와 층상실리케이트로 구성된 분말을제조하는 방법
CN1743442A (zh)	2006-03-08	一种用凹凸棒粘土合成洗涤助剂的方法
US20060281659A1 (en)	2006-12-14	Process for producing a powder consisting of sodiumsesquicarbonate and layered silicate
KR100297321B1 (ko)	2001-09-22	사문석으로부터 제올라이트 에이의 합성방법
Sargent et al.	2024	A Comparative Study on the Synthesis of Type NaX Zeolite Prepared from Kaolin for Builder Application in Detergent Production
WO2002026627A1 (fr)	2002-04-04	Nouvelles compositions zeolithes de faujasite hexagonale a forte teneur en aluminium
JPH0581524B2 (fr)	1993-11-15
JPS6152082B2 (fr)	1986-11-12