CA2741736A1 - Epoxide-based structural foam having improved tenacity - Google Patents

Epoxide-based structural foam having improved tenacity Download PDF

Info

Publication number: CA2741736A1
Authority: CA; Canada
Prior art keywords: thermally expandable; curable compound; compound according; block; shell
Prior art date: 2008-10-28
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Abandoned

Application number

CA2741736A

Other languages

English (en)

French (fr)

Inventor

Emilie Barriau

Olaf Lammerschop

Thomas Engels

Xaver Muenz

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Henkel AG and Co KGaA

Original Assignee

Henkel AG and Co KGaA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2008-10-28

Filing date

2009-09-23

Publication date

2010-05-06

2009-09-23 Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA

2010-05-06 Publication of CA2741736A1 publication Critical patent/CA2741736A1/en

Status Abandoned legal-status Critical Current

Links

150000002118 epoxides Chemical class 0.000 title claims abstract description 5
239000004616 structural foam Substances 0.000 title description 9
239000004433 Thermoplastic polyurethane Substances 0.000 claims abstract description 30
229920002803 thermoplastic polyurethane Polymers 0.000 claims abstract description 30
229920001400 block copolymer Polymers 0.000 claims abstract description 27
239000012948 isocyanate Substances 0.000 claims abstract description 9
150000002513 isocyanates Chemical class 0.000 claims abstract description 9
150000001875 compounds Chemical class 0.000 claims description 40
239000002245 particle Substances 0.000 claims description 31
239000000126 substance Substances 0.000 claims description 31
229920000642 polymer Polymers 0.000 claims description 28
229920001971 elastomer Polymers 0.000 claims description 18
239000010954 inorganic particle Substances 0.000 claims description 18
239000004604 Blowing Agent Substances 0.000 claims description 17
229920000620 organic polymer Polymers 0.000 claims description 17
239000011258 core-shell material Substances 0.000 claims description 16
239000005060 rubber Substances 0.000 claims description 16
239000000945 filler Substances 0.000 claims description 15
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239000007787 solid Substances 0.000 claims description 14
230000009477 glass transition Effects 0.000 claims description 13
239000000835 fiber Substances 0.000 claims description 12
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239000004814 polyurethane Substances 0.000 claims description 11
238000002844 melting Methods 0.000 claims description 7
230000008018 melting Effects 0.000 claims description 7
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239000004926 polymethyl methacrylate Substances 0.000 claims description 5
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NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 3
229920001195 polyisoprene Polymers 0.000 claims description 3
IBARAOFMHIVQQI-UHFFFAOYSA-N butyl prop-2-enoate;methyl 2-methylprop-2-enoate Chemical compound COC(=O)C(C)=C.COC(=O)C(C)=C.CCCCOC(=O)C=C IBARAOFMHIVQQI-UHFFFAOYSA-N 0.000 claims description 2
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239000000463 material Substances 0.000 abstract description 20
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-1 e.g. Substances 0.000 description 29
239000011257 shell material Substances 0.000 description 26
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239000002253 acid Substances 0.000 description 4
230000004913 activation Effects 0.000 description 4
WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 4
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238000005187 foaming Methods 0.000 description 4
239000011325 microbead Substances 0.000 description 4
239000000377 silicon dioxide Substances 0.000 description 4
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 3
NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 3
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
239000004721 Polyphenylene oxide Substances 0.000 description 3
150000007513 acids Chemical class 0.000 description 3
239000011230 binding agent Substances 0.000 description 3
229910052799 carbon Inorganic materials 0.000 description 3
150000004649 carbonic acid derivatives Chemical class 0.000 description 3
238000001816 cooling Methods 0.000 description 3
238000013016 damping Methods 0.000 description 3
239000003085 diluting agent Substances 0.000 description 3
150000002009 diols Chemical class 0.000 description 3
125000003700 epoxy group Chemical group 0.000 description 3
XXOYNJXVWVNOOJ-UHFFFAOYSA-N fenuron Chemical compound CN(C)C(=O)NC1=CC=CC=C1 XXOYNJXVWVNOOJ-UHFFFAOYSA-N 0.000 description 3
239000006260 foam Substances 0.000 description 3
150000002357 guanidines Chemical class 0.000 description 3
150000004679 hydroxides Chemical class 0.000 description 3
239000011159 matrix material Substances 0.000 description 3
150000002739 metals Chemical class 0.000 description 3
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ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 3
OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 2
XMTQQYYKAHVGBJ-UHFFFAOYSA-N 3-(3,4-DICHLOROPHENYL)-1,1-DIMETHYLUREA Chemical compound CN(C)C(=O)NC1=CC=C(Cl)C(Cl)=C1 XMTQQYYKAHVGBJ-UHFFFAOYSA-N 0.000 description 2
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XAYDWGMOPRHLEP-UHFFFAOYSA-N 6-ethenyl-7-oxabicyclo[4.1.0]heptane Chemical compound C1CCCC2OC21C=C XAYDWGMOPRHLEP-UHFFFAOYSA-N 0.000 description 2
GZVHEAJQGPRDLQ-UHFFFAOYSA-N 6-phenyl-1,3,5-triazine-2,4-diamine Chemical class NC1=NC(N)=NC(C=2C=CC=CC=2)=N1 GZVHEAJQGPRDLQ-UHFFFAOYSA-N 0.000 description 2
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CTKINSOISVBQLD-UHFFFAOYSA-N Glycidol Chemical compound OCC1CO1 CTKINSOISVBQLD-UHFFFAOYSA-N 0.000 description 2
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Classifications

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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0066—Use of inorganic compounding ingredients
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- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/4007—Curing agents not provided for by the groups C08G59/42 - C08G59/66
- C08G59/4014—Nitrogen containing compounds
- C08G59/4021—Ureas; Thioureas; Guanidines; Dicyandiamides
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0061—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof characterized by the use of several polymeric components
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
- C08L75/04—Polyurethanes
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2201/00—Foams characterised by the foaming process
- C08J2201/02—Foams characterised by the foaming process characterised by mechanical pre- or post-treatments
- C08J2201/024—Preparation or use of a blowing agent concentrate, i.e. masterbatch in a foamable composition
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2363/00—Characterised by the use of epoxy resins; Derivatives of epoxy resins
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2453/00—Characterised by the use of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2475/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/14—Applications used for foams
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
- C08L53/02—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers of vinyl-aromatic monomers and conjugated dienes
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
- C08L75/04—Polyurethanes
- C08L75/06—Polyurethanes from polyesters

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Inorganic Chemistry (AREA)
Compositions Of Macromolecular Compounds (AREA)
Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
Epoxy Resins (AREA)

CA2741736A 2008-10-28 2009-09-23 Epoxide-based structural foam having improved tenacity Abandoned CA2741736A1 (en)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
DE102008053518A DE102008053518A1 (de)	2008-10-28	2008-10-28	Epoxid-basierter Strukturschaum mit verbesserter Zähigkeit
DE102008053518.4		2008-10-28
PCT/EP2009/062310 WO2010049220A1 (de)	2008-10-28	2009-09-23	Epoxid-basierter strukturschaum mit verbesserter zähigkeit

Publications (1)

Publication Number	Publication Date
CA2741736A1 true CA2741736A1 (en)	2010-05-06

Family

ID=41327272

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA2741736A Abandoned CA2741736A1 (en)	2008-10-28	2009-09-23	Epoxide-based structural foam having improved tenacity

Country Status (10)

Country	Link
US (1)	US20110257285A1 (de)
EP (1)	EP2350177B1 (de)
JP (1)	JP2012506918A (de)
KR (1)	KR20110079687A (de)
CN (1)	CN102197070B (de)
BR (1)	BRPI0920077A2 (de)
CA (1)	CA2741736A1 (de)
DE (1)	DE102008053518A1 (de)
ES (1)	ES2402757T3 (de)
WO (1)	WO2010049220A1 (de)

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BR112014032402A2 (pt)	2012-06-28	2017-06-27	Henkel Ag & Co Kgaa	método de produção de um inserto composto
DE102012221192A1 (de) *	2012-11-20	2014-05-22	Henkel Ag & Co. Kgaa	Thermisch expandierbare Zubereitungen
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2008
- 2008-10-28 DE DE102008053518A patent/DE102008053518A1/de not_active Withdrawn
2009
- 2009-09-23 KR KR1020117009605A patent/KR20110079687A/ko not_active Withdrawn
- 2009-09-23 BR BRPI0920077A patent/BRPI0920077A2/pt not_active IP Right Cessation
- 2009-09-23 EP EP09740074A patent/EP2350177B1/de not_active Not-in-force
- 2009-09-23 CN CN2009801424963A patent/CN102197070B/zh not_active Expired - Fee Related
- 2009-09-23 JP JP2011532558A patent/JP2012506918A/ja active Pending
- 2009-09-23 WO PCT/EP2009/062310 patent/WO2010049220A1/de not_active Ceased
- 2009-09-23 CA CA2741736A patent/CA2741736A1/en not_active Abandoned
- 2009-09-23 ES ES09740074T patent/ES2402757T3/es active Active
2011
- 2011-04-27 US US13/095,282 patent/US20110257285A1/en not_active Abandoned

Also Published As

Publication number	Publication date
EP2350177A1 (de)	2011-08-03
WO2010049220A1 (de)	2010-05-06
ES2402757T3 (es)	2013-05-08
JP2012506918A (ja)	2012-03-22
BRPI0920077A2 (pt)	2016-04-05
US20110257285A1 (en)	2011-10-20
CN102197070A (zh)	2011-09-21
EP2350177B1 (de)	2013-01-23
CN102197070B (zh)	2013-04-24
KR20110079687A (ko)	2011-07-07
DE102008053518A1 (de)	2010-06-02

Legal Events

Date	Code	Title	Description
2014-09-30	EEER	Examination request	Effective date: 20140922
2016-11-06	FZDE	Discontinued	Effective date: 20160923

Publication	Publication Date	Title
US20110257285A1 (en)	2011-10-20	Epoxide-based structural foam having improved tenacity
US20110301255A1 (en)	2011-12-08	Epoxide-based structural foam comprising thermoplastic polyurethanes
JP5519781B2 (ja)	2014-06-11	エポキシドに基づく接着フィルムまたは接着テープ
US9464153B2 (en)	2016-10-11	Premix and method for producing a thermally expandable and curable epoxy-based compound
CN102585439B (zh)	2016-06-15	固态可热膨胀材料
US20090298960A1 (en)	2009-12-03	Ductile structural foams
US20100273905A1 (en)	2010-10-28	Thermoplast-containing epoxy resins and the processing thereof by extrusion or injection molding
DE102006048739A1 (de)	2008-04-17	Expandierbare, thermisch härtbare Zusammensetzung auf Basis von Epoxidharzen mit verbesserten Fließeigenschaften