CH110409A - Preparation suitable for dye production. - Google Patents
Preparation suitable for dye production.Info
- Publication number
- CH110409A CH110409A CH110409DA CH110409A CH 110409 A CH110409 A CH 110409A CH 110409D A CH110409D A CH 110409DA CH 110409 A CH110409 A CH 110409A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation suitable
- dye production
- dye
- production
- nitrosamine
- Prior art date
Links
- 238000002360 preparation method Methods 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- XKLJHFLUAHKGGU-UHFFFAOYSA-N nitrous amide Chemical compound ON=N XKLJHFLUAHKGGU-UHFFFAOYSA-N 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 230000008878 coupling Effects 0.000 claims 1
- 238000010168 coupling process Methods 0.000 claims 1
- 238000005859 coupling reaction Methods 0.000 claims 1
- 125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 claims 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- DPJCXCZTLWNFOH-UHFFFAOYSA-N 2-nitroaniline Chemical compound NC1=CC=CC=C1[N+]([O-])=O DPJCXCZTLWNFOH-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- FCWUFSJRTXLBTH-UHFFFAOYSA-N 2-(2,5-dichlorophenyl)-5-methyl-4h-pyrazol-3-one Chemical compound O=C1CC(C)=NN1C1=CC(Cl)=CC=C1Cl FCWUFSJRTXLBTH-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Coloring (AREA)
Description
Zur Far bstoffher Stellung geeignetes Präparat. Es wurde die überraschende Beobachtung gemacht, (la.ss konzentrierte Mischungen des Nitrosaminalkalisa.lzes aus o-Nitroanilin und dem Natronsa,lz von 1-(2.5-Dichlorphenyl)- 3-metliyl-5-pyrazolon. das eine kupplungs fähige 11ethylenbruppe enthält, Präparate darstellen,
welche eine ausgezeichnete Halt barkeit besitzen und infolgedessen für .die Darstellung von Farbstoffen in verschiedener Hinsicht, zum Beispiel in der Druckerei, w ieht4g sind.
<I>Beispiel:</I> 32,8 Teile 2.5-Dichlorphenylmetliylpyr- azolon 74 /ig werden mit 9,3 Teilen Xtz- natron 94 %ig und 42,4 Teilen einer Paste des Nitrosa.minnatriurnsalzes von o-Nitroani- lin, 35,8 % Base und 3 % freies Ätznatron enthaltend, in .einer Kugelmühle zu einem homogenen Brei veimahlen. Man erhält eine braungelbe, in Wasser leicht lösliche Paste.
Preparation suitable for dye production. The surprising observation was made, (let us concentrate mixtures of the nitrosamine alkali from o-nitroaniline and soda, from 1- (2.5-dichlorophenyl) -3-methyl-5-pyrazolone. Which contains a coupling-capable ethylene group, Represent preparations,
which have an excellent shelf life and as a result are ideal for the representation of dyes in various respects, for example in printing.
<I> Example: </I> 32.8 parts of 2,5-dichlorophenylmetliylpyrazolon 74 / ig are mixed with 9.3 parts of xtic soda 94% and 42.4 parts of a paste of the nitrosa / minatrium salt of o-nitroaniline Containing 35.8% base and 3% free caustic soda, veimahlen in .ein ball mill to a homogeneous pulp. A brown-yellow paste which is easily soluble in water is obtained.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE110409X | 1923-06-11 | ||
| CH109482T | 1924-06-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH110409A true CH110409A (en) | 1925-06-01 |
Family
ID=25707572
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH110409D CH110409A (en) | 1923-06-11 | 1924-06-05 | Preparation suitable for dye production. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH110409A (en) |
-
1924
- 1924-06-05 CH CH110409D patent/CH110409A/en unknown
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