CH141781A - Process for the preparation of an azo dye. - Google Patents
Process for the preparation of an azo dye.Info
- Publication number
- CH141781A CH141781A CH141781DA CH141781A CH 141781 A CH141781 A CH 141781A CH 141781D A CH141781D A CH 141781DA CH 141781 A CH141781 A CH 141781A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- azo dye
- dye
- anilide
- bromobenzene
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title claims description 4
- 239000000987 azo dye Substances 0.000 title description 3
- 150000008049 diazo compounds Chemical class 0.000 claims description 3
- CXPJJDQQLXEYPM-UHFFFAOYSA-N 4-bromo-2,5-dimethylaniline Chemical compound CC1=CC(Br)=C(C)C=C1N CXPJJDQQLXEYPM-UHFFFAOYSA-N 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000975 dye Substances 0.000 description 2
- QOGHRLGTXVMRLM-UHFFFAOYSA-N 4-bromo-1,2-dimethylbenzene Chemical compound CC1=CC=C(Br)C=C1C QOGHRLGTXVMRLM-UHFFFAOYSA-N 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001226 reprecipitation Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Darstellung -eines Azofarbstoffes. Gegenstand -der vorliegenden Erfindung ist ein Verfahren zur Darstellung eines Azo- farbstoffes der folgenden Formel:
EMI0001.0004
den man durch l#',uppliing der Diazoverbin- dung des 1-Amino-2.5=dimethyl-4-bromben- zol auf 2 - Oxynaphtalin - 3 - carbonsäure-4'- methoxy-1.'-anilid erhält.
Beispiel: Die aus 2 kg 1-Amino-2.5-:dimethyl-4- brombenzol in üblicher Weise dargestellte Diazoverbindung lässt man unter Rühren in eine wässerige Suspension von 3 kg 2-Oxy- narphta@lin-3-,carbonsäure-4'-meth@oxy-1'-anilid, bereitet durch Auflösen,derselben in Natron lauge und Wiederausfällen mit verdünnter Essigsäure, einlanfen, Der Farbstoff scheidet sich als roter Niederschlag aus. Er wird fil triert, gewaschen und getrocknet.
Der Farb stoff dient zur Erzeugung von sehr gut chlorechten, ganz hervorragend lichtechten roten Tönen.
Process for the preparation of an azo dye. The subject-matter of the present invention is a process for the preparation of an azo dye of the following formula:
EMI0001.0004
which is obtained by adding the diazo compound of 1-amino-2,5-dimethyl-4-bromobenzene to 2-oxynaphthalene-3-carboxylic acid 4'-methoxy-1'-anilide.
Example: The diazo compound prepared in the usual way from 2 kg of 1-amino-2.5-: dimethyl-4-bromobenzene is left with stirring in an aqueous suspension of 3 kg of 2-oxynarphta @ lin-3-, carboxylic acid-4'- meth @ oxy-1'-anilide, prepared by dissolving it in sodium hydroxide solution and reprecipitation with dilute acetic acid, run in. The dye separates out as a red precipitate. It is filtered, washed and dried.
The dye is used to produce very good chlorine-fast, very excellent lightfast red tones.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE141781X | 1927-10-13 | ||
| CH139505T | 1928-10-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH141781A true CH141781A (en) | 1930-08-15 |
Family
ID=25713366
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH141781D CH141781A (en) | 1927-10-13 | 1928-10-11 | Process for the preparation of an azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH141781A (en) |
-
1928
- 1928-10-11 CH CH141781D patent/CH141781A/en unknown
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