CH155018A - Process for the production of a new azo dye. - Google Patents
Process for the production of a new azo dye.Info
- Publication number
- CH155018A CH155018A CH155018DA CH155018A CH 155018 A CH155018 A CH 155018A CH 155018D A CH155018D A CH 155018DA CH 155018 A CH155018 A CH 155018A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- azo dye
- new azo
- new
- new dye
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title description 2
- 239000000975 dye Substances 0.000 claims description 7
- -1 phenoxyacetylamino-2.5-dimethyl-1-aminobenzene Chemical compound 0.000 claims description 3
- 239000000835 fiber Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- 235000013311 vegetables Nutrition 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- OCISOSJGBCQHHN-UHFFFAOYSA-N 3-hydroxynaphthalene-1-carboxylic acid Chemical compound C1=CC=C2C(C(=O)O)=CC(O)=CC2=C1 OCISOSJGBCQHHN-UHFFFAOYSA-N 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/10—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
- C09B29/18—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides
- C09B29/20—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides of the naphthalene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. 152881. Verfahren zur Herstellung eines neuen Azofarbstofies. Es wurde gefunden, dass man einen neuen Farbstoff erhält, welcher der Formel:
EMI0001.0004
entspricht, wenn man dianotiertes Phenoxy- acetylamino-2.5-dimethyl-l-aminobenzol mit dem 2-Methyl-4-methoxyanilid der 2. 3-Oxy- naphthoesäure kuppelt.
Der neue Farbstoff bildet ein dunkel rotes Pulver. Auf geeigneten Substraten, wie zum Beispiel pflanzlichen Fasern, her gestellt, färbt er diese in echten blauroten Tönen. <I>Beispiel:</I> 27 Teile Phenoxyacetylamino-2.5-di- methyl-l-aminobenzol werden wie üblich di- azotiert und in eine Lösung von 30,7 Teilen des 2-Methyl-4-methoxyanilids der 2 . 3-Oxy- naphthoesäure, 50 Teilen 30 o/oiger Natron lauge, 30 Teilen Soda und 2000 Teilen Wasser eingetragen. Der gebildete Farbstoff fällt sofort aus.
Der dunkelrote Niederschlag wird filtriert und getrocknet.
Additional patent to main patent No. 152881. Process for the production of a new azo dye. It has been found that a new dye is obtained which has the formula:
EMI0001.0004
corresponds if one couples dianotated phenoxyacetylamino-2,5-dimethyl-1-aminobenzene with the 2-methyl-4-methoxyanilide of the 2. 3-oxynaphthoic acid.
The new dye forms a dark red powder. Produced on suitable substrates such as vegetable fibers, he dyes them in real blue-red tones. <I> Example: </I> 27 parts of phenoxyacetylamino-2,5-dimethyl-1-aminobenzene are azotized as usual and dissolved in a solution of 30.7 parts of the 2-methyl-4-methoxyanilide of the 2. Entered 3-oxynaphthoic acid, 50 parts of 30% sodium hydroxide solution, 30 parts of soda and 2000 parts of water. The dye formed precipitates immediately.
The dark red precipitate is filtered and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH155018T | 1930-10-25 | ||
| CH152881T | 1930-10-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH155018A true CH155018A (en) | 1932-05-31 |
Family
ID=25716070
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH155018D CH155018A (en) | 1930-10-25 | 1930-10-25 | Process for the production of a new azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH155018A (en) |
-
1930
- 1930-10-25 CH CH155018D patent/CH155018A/en unknown
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