CH161484A - Process for the production of a new azo dye. - Google Patents
Process for the production of a new azo dye.Info
- Publication number
- CH161484A CH161484A CH161484DA CH161484A CH 161484 A CH161484 A CH 161484A CH 161484D A CH161484D A CH 161484DA CH 161484 A CH161484 A CH 161484A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- azo dye
- mol
- new
- new azo
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 238000000034 method Methods 0.000 title claims description 3
- 239000000987 azo dye Substances 0.000 title description 3
- ORFSSYGWXNGVFB-UHFFFAOYSA-N sodium 4-amino-6-[[4-[4-[(8-amino-1-hydroxy-5,7-disulfonaphthalen-2-yl)diazenyl]-3-methoxyphenyl]-2-methoxyphenyl]diazenyl]-5-hydroxynaphthalene-1,3-disulfonic acid Chemical compound COC1=C(C=CC(=C1)C2=CC(=C(C=C2)N=NC3=C(C4=C(C=C3)C(=CC(=C4N)S(=O)(=O)O)S(=O)(=O)O)O)OC)N=NC5=C(C6=C(C=C5)C(=CC(=C6N)S(=O)(=O)O)S(=O)(=O)O)O.[Na+] ORFSSYGWXNGVFB-UHFFFAOYSA-N 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- 229920000742 Cotton Polymers 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000004627 regenerated cellulose Substances 0.000 claims description 2
- 229920002994 synthetic fiber Polymers 0.000 claims description 2
- 239000012209 synthetic fiber Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- 229920000297 Rayon Polymers 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000005185 salting out Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B35/00—Disazo and polyazo dyes of the type A<-D->B prepared by diazotising and coupling
- C09B35/02—Disazo dyes
- C09B35/039—Disazo dyes characterised by the tetrazo component
- C09B35/08—Disazo dyes characterised by the tetrazo component the tetrazo component being a derivative of biphenyl
- C09B35/20—Disazo dyes characterised by the tetrazo component the tetrazo component being a derivative of biphenyl from two coupling compounds of different types
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
<B>Zusatzpatent</B> zum Hauptpatent Nr. 159410. Verfahren zur Herstellung eines neuen Azofarbstoffes. Es wurde gefunden, dass man einen zur Herstellung von egalen Färbungen auf aus Viskoseseide bestehender Stückwäre besonders geeigneten neuen Azofarbstoff erhält, wenn man 1 Mol tetrazotiertes 4,4'-Diamino-3-3'- dimethoxydiplienyl mit 1 Mol der 1- Oxy- iiaphthalin-4,
8-disulfonsäure mit 1 .1!2o1 der 1- Ainino-8-oxynaplithalin-4-sulfonsäure kuppelt.
Der neue Farbstoff stellt ein dunkles Pulver dar, das sich in Wasser mit reiner blauer Farbe löst. Er erzeugt auf Baumwolle oder Kunstfasern aus regenerierter Zellulose reine blaue Töne.
<I>Beispiel:</I> Die in gewohnter Weise hergestellte Tetrazoverbindung aus 244 Gewichtsteilen 3,3'-Diinetlioxy-4,4'-diaminodiphenyl wird in sodaalkalischer Lösung vereinigt mit 304 Gewichtsteilen 1-Oxynaphthalin-4,8-disulfon- säure und nach stattgefundener Kupplung mit 239 Gewichtsteilen 1-Amino-8-oxynaph- thalin-4-sulfonsäure. Nach erfolgter Kupplung wird der gebildete Farbstoff durch Erwärmen und Aussalzen isoliert, filtriert und getrocknet.
<B> Additional patent </B> to main patent no. 159410. Process for the production of a new azo dye. It has been found that a new azo dye which is particularly suitable for producing level dyeings on pieces made of viscose silk is obtained if 1 mole of tetrazotized 4,4'-diamino-3-3'-dimethoxydiplienyl is obtained with 1 mole of 1-oxy-iiaphthalene -4,
8-disulfonic acid couples with 1 .1! 2o1 of 1-ainino-8-oxynaplithalin-4-sulfonic acid.
The new dye is a dark powder that dissolves in water with a pure blue color. It creates pure blue tones on cotton or synthetic fibers from regenerated cellulose.
<I> Example: </I> The tetrazo compound prepared in the usual way from 244 parts by weight of 3,3'-diinetlioxy-4,4'-diaminodiphenyl is combined in a soda-alkaline solution with 304 parts by weight of 1-oxynaphthalene-4,8-disulfonic acid and after coupling has taken place with 239 parts by weight of 1-amino-8-oxynaphthalene-4-sulfonic acid. After coupling has taken place, the dye formed is isolated by heating and salting out, filtered and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH159410T | 1932-03-02 | ||
| CH161484T | 1932-03-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH161484A true CH161484A (en) | 1933-04-30 |
Family
ID=25717230
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH161484D CH161484A (en) | 1932-03-02 | 1932-03-02 | Process for the production of a new azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH161484A (en) |
-
1932
- 1932-03-02 CH CH161484D patent/CH161484A/en unknown
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