CH197191A - Process for the production of an acidic wool dye. - Google Patents
Process for the production of an acidic wool dye.Info
- Publication number
- CH197191A CH197191A CH197191DA CH197191A CH 197191 A CH197191 A CH 197191A CH 197191D A CH197191D A CH 197191DA CH 197191 A CH197191 A CH 197191A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- dye
- acidic
- wool dye
- acidic wool
- Prior art date
Links
- 210000002268 wool Anatomy 0.000 title claims description 6
- 230000002378 acidificating effect Effects 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 239000000975 dye Substances 0.000 claims description 8
- HYLOSPCJTPLXSF-UHFFFAOYSA-N 5-amino-2-anilinobenzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC(N)=CC=C1NC1=CC=CC=C1 HYLOSPCJTPLXSF-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000005185 salting out Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Coloring (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung eines sauren Wollfarbstoffes. Vorliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines sauren Woll- farbstoffes, dadurch gekennzeichnet, dass mau 1-Chlor-2-nitrobenzol-4-methylsulfon mit 4- Amirio-diphenylamiri-2-sulfonsäure konden siert.
Der so erhaltene Farbstoff färbt Wolle aus saurem Bade in gelbbraunen Tönen von sehr guter Egalität und hervorragender Lichtecht heit. <I>Beispiel:</I> 28,6 Teile 4-amirio-diphenylamin-2-sulfon- saures Natrium werden in der zehnfachen Menge Wasser gelöst. Dann fügt man 23,5 Teile 1-Chlor-2-niti,obenzol-4-methylsulfon in etwa 160 Teilen Alkohol und 10 Teile Na- triumacetat zu und erhitzt das Ganze mehrere Stunden unter Rückfuss zum Sieden. Hierauf wird der Alkohol abdestilliert und der gebil dete Farbstoff aus der wässerigen Lösung durchEindampfen oderAussalzenabgeschieden.
Process for the production of an acidic wool dye. The present patent relates to a process for the production of an acidic wool dye, characterized in that 1-chloro-2-nitrobenzene-4-methylsulfone condenses with 4-aminodiphenylamine-2-sulfonic acid.
The dye obtained in this way dyes wool from an acid bath in yellow-brown shades of very good levelness and excellent lightfastness. <I> Example: </I> 28.6 parts of 4-amirio-diphenylamine-2-sulfonic acid sodium are dissolved in ten times the amount of water. Then 23.5 parts of 1-chloro-2-niti, benzene-4-methylsulfone in about 160 parts of alcohol and 10 parts of sodium acetate are added, and the whole is refluxed for several hours. The alcohol is then distilled off and the dye formed is separated off from the aqueous solution by evaporation or salting out.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE197191X | 1935-08-13 | ||
| DE193627X | 1935-08-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH197191A true CH197191A (en) | 1938-04-15 |
Family
ID=25757655
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH197191D CH197191A (en) | 1935-08-13 | 1936-08-10 | Process for the production of an acidic wool dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH197191A (en) |
-
1936
- 1936-08-10 CH CH197191D patent/CH197191A/en unknown
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