CH197203A - Process for the production of an acidic wool dye. - Google Patents
Process for the production of an acidic wool dye.Info
- Publication number
- CH197203A CH197203A CH197203DA CH197203A CH 197203 A CH197203 A CH 197203A CH 197203D A CH197203D A CH 197203DA CH 197203 A CH197203 A CH 197203A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- dye
- acidic
- wool dye
- acidic wool
- Prior art date
Links
- 210000002268 wool Anatomy 0.000 title claims description 6
- 230000002378 acidificating effect Effects 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 4
- 239000000975 dye Substances 0.000 claims description 8
- DTVFGDRIXSZRIB-UHFFFAOYSA-N 6-amino-9-ethylcarbazole-3-sulfonic acid Chemical compound NC=1C=CC=2N(C3=CC=C(C=C3C2C1)S(=O)(=O)O)CC DTVFGDRIXSZRIB-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- -1 3-amino-N-ethylcarbazole-6-sulphonic acid sodium Chemical compound 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung eines sauren Wollfarbstoffes. Vorliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines sauren Woll- farbstoffes, dadurch gekennzeichnet, dass man 1-Chlor-2-nitrobenzol-4-propylsulfon mit 3-Amino-N-äthylcarbazol-6-sulfonsäure kon densiert.
Der so erhaltene Farbstoff färbt Wolle aus saurem Bade in orangegelben Tönen von guter Egalität und hervorragender Licht echtheit.
<I>Beispiel:</I> 31,2 Teile 3-amino-N-äthylcarbazol-6-sul- fonsaures Natrium werden in der zehnfachen Menge Wasser gelöst. Hierauf fügt man 26,3 Teile 1-Chlor-2-nitrobenzol-4-propylsul- fon in etwa 160 Teilen Alkohol und 10 Teile Natriumacetat zu und erhitzt die Mischung mehrere Stunden unter Rückfluss zum Sie- den.
Dann wird der Alkohol abdestilliert und der gebildete Farbstoff aus der wässe rigen Lösung durch Eindampfen oder Gus salzen abgeschieden.
Process for the production of an acidic wool dye. The present patent relates to a process for the production of an acidic wool dye, characterized in that 1-chloro-2-nitrobenzene-4-propylsulfone is condensed with 3-amino-N-ethylcarbazole-6-sulfonic acid.
The dye obtained in this way dyes wool from an acid bath in orange-yellow shades of good levelness and excellent light fastness.
<I> Example: </I> 31.2 parts of 3-amino-N-ethylcarbazole-6-sulphonic acid sodium are dissolved in ten times the amount of water. 26.3 parts of 1-chloro-2-nitrobenzene-4-propylsulphone in about 160 parts of alcohol and 10 parts of sodium acetate are then added and the mixture is refluxed for several hours.
The alcohol is then distilled off and the dyestuff formed is deposited from the aqueous solution by evaporation or casting salts.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE197203X | 1935-09-17 | ||
| CH193627T | 1937-12-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH197203A true CH197203A (en) | 1938-04-15 |
Family
ID=25722564
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH197203D CH197203A (en) | 1935-09-17 | 1936-08-31 | Process for the production of an acidic wool dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH197203A (en) |
-
1936
- 1936-08-31 CH CH197203D patent/CH197203A/en unknown
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