CH199097A - Process for the preparation of an o-oxyazo dye. - Google Patents
Process for the preparation of an o-oxyazo dye.Info
- Publication number
- CH199097A CH199097A CH199097DA CH199097A CH 199097 A CH199097 A CH 199097A CH 199097D A CH199097D A CH 199097DA CH 199097 A CH199097 A CH 199097A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- oxyazo
- carboxylic acid
- preparation
- anilide
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 8
- 238000002360 preparation method Methods 0.000 title description 2
- 239000000975 dye Substances 0.000 claims description 10
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 4
- 150000008049 diazo compounds Chemical class 0.000 claims description 4
- 210000002268 wool Anatomy 0.000 claims description 4
- RWZYAGGXGHYGMB-UHFFFAOYSA-N anthranilic acid Chemical compound NC1=CC=CC=C1C(O)=O RWZYAGGXGHYGMB-UHFFFAOYSA-N 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- UIIMBOGNXHQVGW-UHFFFAOYSA-N sodium;hydron;carbonate Chemical compound [Na+].OC(O)=O UIIMBOGNXHQVGW-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Coloring (AREA)
Description
Verfahren zur Herstellung eines o-Ogyazofarbstoffes. Nach dem im Hauptpatent beschriebenen Verfahren erhält man einen Wolle nach dem Einbad-Chromverfahren in violettbraunen Tönen färbenden Farbstoff, indem man 4 Nitro-6-chlor-2-amino-l-oxybenzol diazotiert und die Diazoverbindung mit 2-Oxynaphtha- lin-6-sulfonsäureanilid-2'-carbonsäure kup pelt.
Wie nun -weiter gefunden wurde, erhält man einen Farbstoff von ähnlichen Echt heitseigenschaften, wenn man 2-Aminobenzol- 1--carbonsäure diazotiert und die Diazoverbin- dung mit 2-Oxynaphthalin-6-sulfonsäureani- lid-2'-carbonsäure kuppelt. Der Farbstoff färbt auf Wolle nach dem Chromverfahren gedeckte rote Töne von guten Echtheitseigen schaften.
<I>Beispiel:</I> 13,7 Teile 2-Aminobenzol-l-carbonsäure werden auf übliche Art diazotiert. Die Di- azoverbin,dung läuft zu einer mit Eis versetz ten Auflösung von 35 Teilen 2-Oxynaphtha- lin-6-sulfonsäureanilid-2'-carbonsäure und 30 Teilen Soda in etwa 1000 Teilen Wasser. Die Aufarbeitung des Farbstoffes erfolgt in üblicher Weise. Er bildet nach dem Trock nen ein rotes Pulver von guter Löslichkeit.
Wolle wird nach dem Chromverfahren in ge deckten roten Tönen von guter Wasch-, Walk- und Lichtechtheit angefärbt.
Process for the preparation of an o-ogyazo dye. According to the process described in the main patent, a dye is obtained which dyes wool by the single-bath chromium process in violet-brown shades by diazotizing 4 nitro-6-chloro-2-amino-1-oxybenzene and treating the diazo compound with 2-oxynaphthalin-6- sulfonic anilide-2'-carboxylic acid kup pelt.
As has now been found, a dye of similar authenticity properties is obtained if 2-aminobenzene-1-carboxylic acid is diazotized and the diazo compound is coupled with 2-oxynaphthalene-6-sulfonic acid anilide-2'-carboxylic acid. The dye dyes muted red shades with good fastness properties on wool using the chrome process.
<I> Example: </I> 13.7 parts of 2-aminobenzene-1-carboxylic acid are diazotized in the usual way. The diazo compound leads to a dissolution of 35 parts of 2-oxynaphthaline-6-sulfonic acid anilide-2'-carboxylic acid and 30 parts of soda in about 1000 parts of water. The dye is worked up in the customary manner. After drying it forms a red powder with good solubility.
Using the chrome process, wool is dyed in opaque red tones that are wash, milled and lightfast.
Claims (1)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE199097X | 1936-01-17 | ||
| DE30636X | 1936-06-03 | ||
| CH197281T | 1936-11-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH199097A true CH199097A (en) | 1938-07-31 |
Family
ID=27177840
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH199097D CH199097A (en) | 1936-01-17 | 1936-11-04 | Process for the preparation of an o-oxyazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH199097A (en) |
-
1936
- 1936-11-04 CH CH199097D patent/CH199097A/en unknown
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