CH202170A - Process for the preparation of a nitro dye. - Google Patents
Process for the preparation of a nitro dye.Info
- Publication number
- CH202170A CH202170A CH202170DA CH202170A CH 202170 A CH202170 A CH 202170A CH 202170D A CH202170D A CH 202170DA CH 202170 A CH202170 A CH 202170A
- Authority
- CH
- Switzerland
- Prior art keywords
- nitro dye
- preparation
- brown
- dye
- methyltaurine
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 239000001005 nitro dye Substances 0.000 title claims description 4
- 239000000975 dye Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 2
- 239000010985 leather Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- -1 Aminophenyl Chemical group 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 238000005185 salting out Methods 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B51/00—Nitro or nitroso dyes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. <B>199466.</B> Verfahren zur Herstellung eines Nitrofarbstoffes. Gegenstand des vorliegenden Zusatzpaten tes ist ein Verfahren zur Herstellung eines Nitrofarbstoffes, welches dadurch gekenn zeichnet ist, dass man 4-Aminopheiiyl-l- methyltaurin mit 1-Chlor-4,6-dinitro-2-sulfoii- säure kondensiert.
<I>Beispiel:</I> <B>230</B> Gewichtsteile 4<B>-</B> Aminophenyl <B>- 1</B> - methyltaurin von der Formel:
EMI0001.0011
werden in wenig Wasser mit Natriumearbo- nat neutralisiert und in Gegenwart von<B>136</B> Gewichtsteilen kristallisiertem Natriumacetat mit<B>321</B> Gewichtsteilen 1-chlor-4,6-dinitro- 2-sulforisaurem Kalium einige Stunden zum Sieden erhitzt. Nach beendeterKondensation wird der Farbstoff durch Aussalzen isoliert.
Das so erhaltene Produkt stellt ein brau nes Pulver. dar, das in Wasser mit brauner Farbe leicht löslich ist und Leder in gelb braunen Tönen gleichmässig durchfärbt.
Additional patent to main patent no. <B> 199466. </B> Process for the production of a nitro dye. The subject of the present additional patent is a process for the production of a nitro dye which is characterized in that 4-aminopheiiyl-1-methyltaurine is condensed with 1-chloro-4,6-dinitro-2-sulfoic acid.
<I> Example: </I> <B> 230 </B> parts by weight 4 <B> - </B> Aminophenyl <B> - 1 </B> - methyltaurine of the formula:
EMI0001.0011
are neutralized in a little water with sodium carbonate and in the presence of 136 parts by weight of crystallized sodium acetate with 321 parts by weight of 1-chloro-4,6-dinitro-2-sulphurate for a few hours heated to boiling. After the condensation has ended, the dye is isolated by salting out.
The product obtained in this way is a brown powder. which is easily soluble in water with a brown color and evenly dyes leather in yellow-brown tones.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE202170X | 1936-05-02 | ||
| CH199466T | 1939-11-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH202170A true CH202170A (en) | 1938-12-31 |
Family
ID=25723314
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH202170D CH202170A (en) | 1936-05-02 | 1937-04-22 | Process for the preparation of a nitro dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH202170A (en) |
-
1937
- 1937-04-22 CH CH202170D patent/CH202170A/en unknown
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