CH625332A5 - Device for continuous manufacture of granulates - Google Patents
Device for continuous manufacture of granulates Download PDFInfo
- Publication number
- CH625332A5 CH625332A5 CH1609077A CH1609077A CH625332A5 CH 625332 A5 CH625332 A5 CH 625332A5 CH 1609077 A CH1609077 A CH 1609077A CH 1609077 A CH1609077 A CH 1609077A CH 625332 A5 CH625332 A5 CH 625332A5
- Authority
- CH
- Switzerland
- Prior art keywords
- granules
- coolant
- frozen
- freeze
- product
- Prior art date
Links
- 239000008187 granular material Substances 0.000 title claims description 27
- 238000004519 manufacturing process Methods 0.000 title claims 4
- 239000002826 coolant Substances 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 25
- 239000007788 liquid Substances 0.000 claims description 19
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 10
- 238000004108 freeze drying Methods 0.000 claims description 9
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 238000007710 freezing Methods 0.000 claims description 7
- 230000008014 freezing Effects 0.000 claims description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 4
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 claims description 3
- 230000005484 gravity Effects 0.000 claims description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 2
- 239000001569 carbon dioxide Substances 0.000 claims description 2
- 238000002347 injection Methods 0.000 claims description 2
- 239000007924 injection Substances 0.000 claims description 2
- 239000001272 nitrous oxide Substances 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- 238000010924 continuous production Methods 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- 241000251468 Actinopterygii Species 0.000 claims 1
- 241001122767 Theaceae Species 0.000 claims 1
- 238000004140 cleaning Methods 0.000 claims 1
- 235000016213 coffee Nutrition 0.000 claims 1
- 235000013353 coffee beverage Nutrition 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 239000000428 dust Substances 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 235000019688 fish Nutrition 0.000 claims 1
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 claims 1
- 235000013305 food Nutrition 0.000 claims 1
- 235000015203 fruit juice Nutrition 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 235000013372 meat Nutrition 0.000 claims 1
- 229940126601 medicinal product Drugs 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 235000021055 solid food Nutrition 0.000 claims 1
- 238000007711 solidification Methods 0.000 claims 1
- 230000008023 solidification Effects 0.000 claims 1
- 235000014347 soups Nutrition 0.000 claims 1
- 235000013616 tea Nutrition 0.000 claims 1
- 235000013311 vegetables Nutrition 0.000 claims 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 4
- 229930006000 Sucrose Natural products 0.000 description 4
- 239000005720 sucrose Substances 0.000 description 4
- -1 butane and propane Chemical class 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 125000002947 alkylene group Chemical group 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B5/00—Drying solid materials or objects by processes not involving the application of heat
- F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
- F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
- F26B5/065—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing the product to be freeze-dried being sprayed, dispersed or pulverised
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B2/00—Preservation of foods or foodstuffs, in general
- A23B2/80—Freezing; Subsequent thawing; Cooling
- A23B2/85—Freezing; Subsequent thawing; Cooling with addition of or treatment with chemicals
- A23B2/88—Freezing; Subsequent thawing; Cooling with addition of or treatment with chemicals with direct contact between the food and the chemical, e.g. liquid N2 at cryogenic temperature
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B2/00—Preservation of foods or foodstuffs, in general
- A23B2/90—Preservation of foods or foodstuffs, in general by drying or kilning; Subsequent reconstitution
- A23B2/92—Freeze drying
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B4/00—Preservation of meat, sausages, fish or fish products
- A23B4/03—Drying; Subsequent reconstitution
- A23B4/037—Freeze-drying, i.e. cryodesiccation or lyophilisation; Apparatus therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B4/00—Preservation of meat, sausages, fish or fish products
- A23B4/06—Freezing; Subsequent thawing; Cooling
- A23B4/062—Freezing; Subsequent thawing; Cooling the materials being transported through or in the apparatus with or without shaping, e.g. in the form of powder, granules or flakes
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25C—PRODUCING, WORKING OR HANDLING ICE
- F25C1/00—Producing ice
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25D—REFRIGERATORS; COLD ROOMS; ICE-BOXES; COOLING OR FREEZING APPARATUS NOT OTHERWISE PROVIDED FOR
- F25D3/00—Devices using other cold materials; Devices using cold-storage bodies
- F25D3/10—Devices using other cold materials; Devices using cold-storage bodies using liquefied gases, e.g. liquid air
Landscapes
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- General Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Molecular Biology (AREA)
- Health & Medical Sciences (AREA)
- Combustion & Propulsion (AREA)
- Drying Of Solid Materials (AREA)
- Freezing, Cooling And Drying Of Foods (AREA)
- Medical Preparation Storing Or Oral Administration Devices (AREA)
- Confectionery (AREA)
- Glanulating (AREA)
- Non-Alcoholic Beverages (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19762659546 DE2659546A1 (de) | 1976-12-30 | 1976-12-30 | Verfahren zur herstellung von gefrorenen granulaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH625332A5 true CH625332A5 (en) | 1981-09-15 |
Family
ID=5997030
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH1609077A CH625332A5 (en) | 1976-12-30 | 1977-12-27 | Device for continuous manufacture of granulates |
Country Status (18)
| Country | Link |
|---|---|
| JP (1) | JPS53114783A (fr) |
| AR (1) | AR214108A1 (fr) |
| AT (1) | AT356498B (fr) |
| AU (1) | AU506746B2 (fr) |
| BE (1) | BE862370A (fr) |
| CA (1) | CA1106686A (fr) |
| CH (1) | CH625332A5 (fr) |
| DD (1) | DD133295A5 (fr) |
| DE (1) | DE2659546A1 (fr) |
| FI (1) | FI773941A7 (fr) |
| FR (1) | FR2375901A1 (fr) |
| GB (1) | GB1559920A (fr) |
| IE (1) | IE46022B1 (fr) |
| IL (1) | IL53695A0 (fr) |
| IT (1) | IT1089419B (fr) |
| NL (1) | NL7714401A (fr) |
| SE (1) | SE7714822L (fr) |
| ZA (1) | ZA777184B (fr) |
Families Citing this family (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3042955A1 (de) * | 1980-11-14 | 1982-10-21 | Helmut 7702 Gottmadingen Ruh | Verfahren und vorrichtung zum aufbereiten frischer kraeuter oder kraeutermischungen sowie formkoerper daraus |
| FR2566515B1 (fr) * | 1984-06-22 | 1987-03-27 | Air Liquide | Procede et installation de refroidissement, au moyen d'un fluide frigorigene d'une poudre |
| US4704873A (en) * | 1985-11-14 | 1987-11-10 | Taiyo Sanso Co., Ltd. | Method and apparatus for producing microfine frozen particles |
| DE69034228T2 (de) * | 1989-03-01 | 2007-06-14 | Polar Technologies Holdings B.V. | Tragbare Vorrichtung zur Herstellung von Schnee |
| ES2062530T3 (es) * | 1989-05-01 | 1994-12-16 | Alkermes Inc | Procedimiento para producir particulas pequeñas de moleculas biologicamente activas. |
| JPH0753704Y2 (ja) * | 1989-06-05 | 1995-12-13 | 大陽酸素株式会社 | 凍結粒製造装置 |
| JPH089582Y2 (ja) * | 1990-08-31 | 1996-03-21 | 大陽酸素株式会社 | 凍結粒製造装置 |
| US5318636A (en) * | 1991-04-19 | 1994-06-07 | Eva Abony Szucs | Method for cleaning surfaces, in particular sensitive surfaces |
| DE4112890A1 (de) * | 1991-04-19 | 1992-10-22 | Abony Szuecs Eva | Verfahren und vorrichtung zum reinigen von oberflaechen, insbesondere von empfindlichen oberflaechen |
| JPH06323712A (ja) * | 1993-04-20 | 1994-11-25 | E I Du Pont De Nemours & Co | 霧化した極低温液滴の閉じ込め帯域を用いて凍結粒子を製造する方法および装置 |
| DE4344393C2 (de) * | 1993-12-24 | 1998-10-01 | Ftd Foam Tech Dev Gmbh | Einrichtung zum Herstellen von Speiseeis, gefrorenen Dessert- und Fruchtmassen, Tortenmassen, Teigmassen, aus mehreren schwer mischbaren fluiden Matrizes, welche aus wenigstens einer Stoffkomponente bestehen |
| US5737928A (en) * | 1995-03-09 | 1998-04-14 | The Boc Group, Inc. | Process fluid cooling means and apparatus |
| DE19813101A1 (de) * | 1998-03-25 | 1999-09-30 | Herbert Dressler | Vorrichtung zum Versprühen chemisch-technischer Produkte und Verfahren hierzu |
| NO311164B1 (no) * | 1998-06-02 | 2001-10-22 | Leiv Eiriksson Nyfotek As | Fremgangsmåte for frysetörking av lösninger |
| BR0014577A (pt) | 1999-09-30 | 2003-02-25 | Saitec Srl | Método e sistema para refrigerar e efetuar mudança no estado de uma mistura lìquida |
| DE10243483A1 (de) * | 2002-09-19 | 2004-04-08 | Messer Griesheim Gmbh | System zum Mikropelletieren von Lösungen bzw. Schmelzen |
| ITMI20032367A1 (it) * | 2003-12-03 | 2005-06-04 | Air Liquide Italia S P A | Metodo ed impianto per il raffreddamento di fluidi |
| EP1697035B1 (fr) | 2003-12-22 | 2017-11-15 | Warren H. Finlay | Fomation de poudre par lyophilisation par vaporisation atmospherique |
| AU2005263465B2 (en) | 2004-07-23 | 2010-07-29 | Bayer Healthcare Llc | Sterile freezing, drying, storing, assaying and filling process (SFD-SAF process) (pellet freeze-drying process for parenteral biopharmaceuticals) |
| NZ550563A (en) * | 2006-10-16 | 2009-01-31 | Agres Ltd | Improvements in spray freeze drying |
| US7861551B2 (en) * | 2007-11-30 | 2011-01-04 | Whirlpool Corporation | Method and device for producing ice droplets on demand |
| CN101959527B (zh) | 2008-03-05 | 2016-04-20 | 赛诺菲巴斯德有限公司 | 一种使含佐剂的疫苗组合物稳定的方法 |
| EP2143440A1 (fr) | 2008-07-09 | 2010-01-13 | Sanofi Pasteur | Agent stabilisant et composition vaccinale comprenant un ou plusieurs flavivirus vivants atténués |
| US9945611B2 (en) | 2010-08-04 | 2018-04-17 | Ima Life North America Inc. | Bulk freeze drying using spray freezing and agitated drying |
| ITBS20110076A1 (it) * | 2011-05-25 | 2012-11-26 | K190 S R L | Apparato e procedimento per la preparazione di gelato o prodotti alimentari affini |
| FR2983286B1 (fr) * | 2011-11-24 | 2018-04-13 | L'air Liquide,Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Dispositif de refroidissement de produits en vrac |
| CN103123196B (zh) * | 2013-02-06 | 2015-08-26 | 邹杰 | 一种蓄冷设备 |
| JP5837670B2 (ja) * | 2014-10-24 | 2015-12-24 | アイエムエー ライフ ノース アメリカ インコーポレーテッド | 噴霧凍結および撹拌乾燥を使用するバルク・フリーズドライ |
| CN105597622B (zh) * | 2016-03-09 | 2017-11-21 | 苏州大学 | 结冰温度可控的用于制备微米级冰球颗粒的喷雾冷冻塔 |
| CN106113314B (zh) * | 2016-08-15 | 2019-06-21 | 浙江心源科技有限公司 | 一种喷雾结晶造粒装置及其造粒方法 |
| DE202016106243U1 (de) | 2016-09-21 | 2016-11-17 | Dressler Group GmbH & Co. KG | Vorrichtung zur Herstellung von pulverförmigen Kunststoffen mit möglichst kugelförmiger Struktur |
| DE102018002750B8 (de) * | 2018-04-06 | 2020-09-24 | Messer France S.A.S. | Vorrichtung zum Kühlen von Produkten |
| CN108709369A (zh) * | 2018-04-20 | 2018-10-26 | 大连工业大学 | 一种超声波喷雾冷冻干燥装置 |
| CN109820130B (zh) * | 2019-04-03 | 2022-09-16 | 河南工业大学 | 一种可溶性膳食纤维提取装置 |
| EP4203703A4 (fr) * | 2020-08-31 | 2025-01-15 | Cornell University | Systèmes et procédés de congélation rapide d'un liquide |
| US20230320375A1 (en) * | 2020-08-31 | 2023-10-12 | Cornell University | Systems and methods for rapidly freezing a liquid |
| CN112774571A (zh) * | 2020-12-26 | 2021-05-11 | 深圳万和制药有限公司 | 高均匀性大粒径微丸的分散冷凝生产工艺 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2751687A (en) * | 1952-05-21 | 1956-06-26 | Proctor Drying And Freezing Co | Process and apparatus for producing stabilized products |
-
1976
- 1976-12-30 DE DE19762659546 patent/DE2659546A1/de not_active Withdrawn
-
1977
- 1977-12-02 ZA ZA00777184A patent/ZA777184B/xx unknown
- 1977-12-22 AU AU31922/77A patent/AU506746B2/en not_active Expired
- 1977-12-23 CA CA293,821A patent/CA1106686A/fr not_active Expired
- 1977-12-26 IL IL53695A patent/IL53695A0/xx unknown
- 1977-12-27 AR AR270534A patent/AR214108A1/es active
- 1977-12-27 NL NL7714401A patent/NL7714401A/xx not_active Application Discontinuation
- 1977-12-27 CH CH1609077A patent/CH625332A5/de not_active IP Right Cessation
- 1977-12-27 BE BE183889A patent/BE862370A/fr unknown
- 1977-12-28 GB GB53984/77A patent/GB1559920A/en not_active Expired
- 1977-12-28 SE SE7714822A patent/SE7714822L/xx not_active Application Discontinuation
- 1977-12-28 FI FI773941A patent/FI773941A7/fi not_active Application Discontinuation
- 1977-12-28 JP JP15864477A patent/JPS53114783A/ja active Pending
- 1977-12-28 IT IT31361/77A patent/IT1089419B/it active
- 1977-12-29 IE IE2638/77A patent/IE46022B1/en unknown
- 1977-12-29 DD DD7700203008A patent/DD133295A5/xx unknown
- 1977-12-29 AT AT940677A patent/AT356498B/de not_active IP Right Cessation
- 1977-12-29 FR FR7739583A patent/FR2375901A1/fr active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CA1106686A (fr) | 1981-08-11 |
| BE862370A (fr) | 1978-06-27 |
| SE7714822L (sv) | 1978-07-01 |
| JPS53114783A (en) | 1978-10-06 |
| DD133295A5 (de) | 1978-12-27 |
| IT1089419B (it) | 1985-06-18 |
| IE46022B1 (en) | 1983-01-26 |
| DE2659546A1 (de) | 1978-07-13 |
| ZA777184B (en) | 1978-10-25 |
| FR2375901A1 (fr) | 1978-07-28 |
| AR214108A1 (es) | 1979-04-30 |
| AU506746B2 (en) | 1980-01-24 |
| GB1559920A (en) | 1980-01-30 |
| IL53695A0 (en) | 1978-03-10 |
| NL7714401A (nl) | 1978-07-04 |
| IE46022L (en) | 1978-06-30 |
| AU3192277A (en) | 1979-06-28 |
| ATA940677A (de) | 1979-09-15 |
| AT356498B (de) | 1980-04-25 |
| FI773941A7 (fi) | 1978-07-01 |
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