CH86982A - Process for the production of an azo dye particularly suitable for cotton printing. - Google Patents
Process for the production of an azo dye particularly suitable for cotton printing.Info
- Publication number
- CH86982A CH86982A CH86982DA CH86982A CH 86982 A CH86982 A CH 86982A CH 86982D A CH86982D A CH 86982DA CH 86982 A CH86982 A CH 86982A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- particularly suitable
- azo dye
- cotton
- sulfo
- Prior art date
Links
- 229920000742 Cotton Polymers 0.000 title claims description 5
- 238000000034 method Methods 0.000 title claims description 5
- 239000000987 azo dye Substances 0.000 title claims description 3
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- ZYECOAILUNWEAL-NUDFZHEQSA-N (4z)-4-[[2-methoxy-5-(phenylcarbamoyl)phenyl]hydrazinylidene]-n-(3-nitrophenyl)-3-oxonaphthalene-2-carboxamide Chemical compound COC1=CC=C(C(=O)NC=2C=CC=CC=2)C=C1N\N=C(C1=CC=CC=C1C=1)/C(=O)C=1C(=O)NC1=CC=CC([N+]([O-])=O)=C1 ZYECOAILUNWEAL-NUDFZHEQSA-N 0.000 claims description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- 150000008049 diazo compounds Chemical class 0.000 claims description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000344 soap Substances 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical class [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/10—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
- C09B29/16—Naphthol-sulfonic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
verfahren zur Herstellung eines zum Baumwolldruck besonders geeigneten Azofarustoffes. Es wurde gefunden, dass man durch Kup peln von diazotierter 4-Sulfo-2-ainino-l-oxy- benzol-6-carbonsäure mit 1-Oxynaphtalin-3- sulfo-5-carbonsäure einen Azofarbstoff erhält, welcher sich in Wasser mit violettroter, in konzentrierter Schwefelsäure mit blauroter Farbe löst und auf Baumwolle, nach dein Chromdruckverfahren bedruckt, seifen-,
chlor- und lichtechte rotviolette Töne gibt.
<I>Beispiel:</I> Die auf bekannte Art aus 23,3 Teilen 4 -Sulfo- 2 -amino- 1 -oxybenzol- 6 -carbonsäure dargestellte Diazoverbindung gibt man unter Rühren zu einer möglichst konzentrierten Lösung von 29 Teilen des Mononatriumsalzes der 1-Oxynaphtalin-3-sulfo-5-carbonsäui-e, 40 Teilen Soda und 26 Teilen Natronlauge iL 30 %. Der kristallinisch ausfallende Farbstoff wird kalt filtriert, gepresst und getrocknet.
process for the production of an azo-fragrant substance particularly suitable for cotton printing. It has been found that coupling diazotized 4-sulfo-2-ainino-1-oxybenzene-6-carboxylic acid with 1-oxynaphthalene-3-sulfo-5-carboxylic acid gives an azo dye which turns violet-red in water , dissolves in concentrated sulfuric acid with a blue-red color and is printed on cotton using the chrome printing process, soapy,
gives chlorine and lightfast red-violet tones.
<I> Example: </I> The diazo compound prepared in a known manner from 23.3 parts of 4-sulfo-2-amino-1 -oxybenzene-6-carboxylic acid is added with stirring to a solution of 29 parts of the monosodium salt which is as concentrated as possible 1-Oxynaphtalin-3-sulfo-5-carbonsäui-e, 40 parts of soda and 26 parts of sodium hydroxide solution iL 30%. The dyestuff which precipitates in crystalline form is filtered cold, pressed and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH86026T | 1918-05-24 | ||
| CH86982T | 1918-05-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH86982A true CH86982A (en) | 1920-11-01 |
Family
ID=25703521
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH86982D CH86982A (en) | 1918-05-24 | 1918-05-24 | Process for the production of an azo dye particularly suitable for cotton printing. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH86982A (en) |
-
1918
- 1918-05-24 CH CH86982D patent/CH86982A/en unknown
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