CH90858A - Process for the preparation of an o-oxyazo dye. - Google Patents
Process for the preparation of an o-oxyazo dye.Info
- Publication number
- CH90858A CH90858A CH90858DA CH90858A CH 90858 A CH90858 A CH 90858A CH 90858D A CH90858D A CH 90858DA CH 90858 A CH90858 A CH 90858A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- dye
- oxyazo
- oxynaphthalene
- oxybenzene
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Natural products OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 1
- 239000000987 azo dye Substances 0.000 claims 1
- 239000004922 lacquer Substances 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
Landscapes
- Coloring (AREA)
- Paper (AREA)
- Non-Silver Salt Photosensitive Materials And Non-Silver Salt Photography (AREA)
Description
Verfahren zur Darstellung eines o-Oxyazofarbstoifes. Es wurde gefunden, dass durch Kuppeln von 4 # 6-Dinitro-2-diazo-l-oxybenzol mit - 8- Chlor-l-oxynaphtalin-5-sulfosäure ein Farb stoff erhalten wird, der auf urgebeizter Wolle ein Korinth gibt und dessen Chromlack dunkel grün ist.
<I>Beispiel:</I> Die aus 19,9 Teilen 4 # 6-Dinitro=2-amino- 1-oxybenzol, 50 Teilen Salzsäure von 12 <I>136</I> und 6,9 Teilen Natriumnitrit bereitete Diazo- verbindung lässt man in eine durch Soda alkälisch gehaltene Lösung von 25,9 Teilen 8-Chlor-l-oxynaphtalir-5-sulfosäure einlaufen. Nach beendeter Kupplung salzt man den Farbstoff aus und arbeitet ihn in der üb lichen Weise auf.
Process for the preparation of an o-oxyazo dye. It has been found that by coupling 4 # 6-dinitro-2-diazo-1-oxybenzene with - 8-chloro-1-oxynaphthalene-5-sulfonic acid, a dye is obtained which gives a corinth to originally stained wool and its chrome varnish is dark green.
<I> Example: </I> The diazo prepared from 19.9 parts of 4 # 6-dinitro = 2-amino-1-oxybenzene, 50 parts of hydrochloric acid of 12 <I> 136 </I> and 6.9 parts of sodium nitrite - The compound is allowed to run into a solution of 25.9 parts of 8-chloro-1-oxynaphthalene-5-sulfonic acid kept alkaline by soda. After the coupling has ended, the dye is salted out and worked up in the usual manner.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE89057X | 1917-08-28 | ||
| CH89057T | 1920-07-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH90858A true CH90858A (en) | 1921-10-01 |
Family
ID=25703948
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH90858D CH90858A (en) | 1917-08-28 | 1920-07-08 | Process for the preparation of an o-oxyazo dye. |
| CH90857D CH90857A (en) | 1917-08-28 | 1920-07-08 | Process for the preparation of an o-oxyazo dye. |
| CH90856D CH90856A (en) | 1917-08-28 | 1920-07-08 | Process for preparing an o-oxyazo dye. |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH90857D CH90857A (en) | 1917-08-28 | 1920-07-08 | Process for the preparation of an o-oxyazo dye. |
| CH90856D CH90856A (en) | 1917-08-28 | 1920-07-08 | Process for preparing an o-oxyazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (3) | CH90858A (en) |
-
1920
- 1920-07-08 CH CH90858D patent/CH90858A/en unknown
- 1920-07-08 CH CH90857D patent/CH90857A/en unknown
- 1920-07-08 CH CH90856D patent/CH90856A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CH90856A (en) | 1921-10-01 |
| CH90857A (en) | 1921-10-01 |
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