CL2018001844A1 - Método de preparación de isótopos - Google Patents

Método de preparación de isótopos

Info

Publication number
CL2018001844A1
CL2018001844A1 CL2018001844A CL2018001844A CL2018001844A1 CL 2018001844 A1 CL2018001844 A1 CL 2018001844A1 CL 2018001844 A CL2018001844 A CL 2018001844A CL 2018001844 A CL2018001844 A CL 2018001844A CL 2018001844 A1 CL2018001844 A1 CL 2018001844A1
Authority
CL
Chile
Prior art keywords
solution
exchange resin
levigate
strong
acid
Prior art date
Application number
CL2018001844A
Other languages
English (en)
Inventor
Dimitrios Mantzilas
Jan Roger Karlson
Judit Tjelmeland Østby
Original Assignee
Bayer As
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer As filed Critical Bayer As
Publication of CL2018001844A1 publication Critical patent/CL2018001844A1/es

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/10Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1864Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using two or more columns
    • B01D15/1871Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using two or more columns placed in series
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K51/00Preparations containing radioactive substances for use in therapy or testing in vivo
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P35/00Antineoplastic agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
    • B01D15/361Ion-exchange
    • B01D15/362Cation-exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
    • B01D15/361Ion-exchange
    • B01D15/363Anion-exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04Processes using organic exchangers
    • B01J39/05Processes using organic exchangers in the strongly acidic form
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/04Processes using organic exchangers
    • B01J41/05Processes using organic exchangers in the strongly basic form
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/60Cleaning or rinsing ion-exchange beds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F15/00Compounds of thorium
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21GCONVERSION OF CHEMICAL ELEMENTS; RADIOACTIVE SOURCES
    • G21G1/00Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes
    • G21G1/001Recovery of specific isotopes from irradiated targets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • Medicinal Chemistry (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • Optics & Photonics (AREA)
  • Epidemiology (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Medicinal Preparation (AREA)
  • Indole Compounds (AREA)

Abstract

LA PRESENTE INVENCIÓN COMPRENDE UN MÉTODO PARA LA GENERACIÓN DE 227TH DE PUREZA FARMACÉUTICAMENTE TOLERABLE QUE COMPRENDE I) PREPARAR UNA MEZCLA GENERADORA QUE COMPRENDE 227AC, 227TH Y 223RA; II) CARGAR DICHA MEZCLA GENERADORA SOBRE UNA RESINA DE INTERCAMBIO ANIÓNICO DE BASE FUERTE; III) LEVIGAR UNA MEZCLA DE DICHOS 223RA Y 227AC DE DICHA RESINA DE INTERCAMBIO ANIÓNICO DE BASE FUERTE CON EL USO DE UN PRIMER ÁCIDO MINERAL EN UNA SOLUCIÓN ACUOSA; IV) LEVIGAR 227TH DE DICHA RESINA DE INTERCAMBIO ANIÓNICO DE BASE FUERTE CON EL USO DE UN SEGUNDO ÁCIDO MINERAL EN UNA SOLUCIÓN ACUOSA MEDIANTE LO CUAL SE GENERA UNA PRIMERA SOLUCIÓN DE 227TH QUE CONTIENE 223RA Y 227AC CONTAMINANTES; V) CARGAR LA PRIMERA SOLUCIÓN DE 227TH SOBRE UNA RESINA DE INTERCAMBIO CATIÓNICO DE ÁCIDO FUERTE; VI) LEVIGAR POR LO MENOS UNA PARTE DE LOS 223RA Y 227AC CONTAMINANTES DE DICHA RESINA DE INTERCAMBIO CATIÓNICO DE ÁCIDO FUERTE CON EL USO DE UN TERCER ÁCIDO MINERAL EN SOLUCIÓN ACUOSA; Y VII) LEVIGAR EL 227TH DE DICHA RESINA DE INTERCAMBIO CATIÓNICO DE ÁCIDO FUERTE CON EL USO DE UNA PRIMERA SOLUCIÓN DE TAMPÓN ACUOSA PARA PROPORCIONAR UNA SEGUNDA SOLUCIÓN DE 227TH. SE PROPORCIONAN ADEMÁS TORIO 227 PURIFICADO DE PUREZA FARMACÉUTICA Y UNA COMPOSICIÓN FARMACÉUTICA QUE LO COMPRENDE.
CL2018001844A 2016-01-05 2018-07-05 Método de preparación de isótopos CL2018001844A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB1600154.7A GB201600154D0 (en) 2016-01-05 2016-01-05 Isotope preparation method

Publications (1)

Publication Number Publication Date
CL2018001844A1 true CL2018001844A1 (es) 2018-10-26

Family

ID=55406715

Family Applications (1)

Application Number Title Priority Date Filing Date
CL2018001844A CL2018001844A1 (es) 2016-01-05 2018-07-05 Método de preparación de isótopos

Country Status (22)

Country Link
US (2) US20190009265A1 (es)
EP (1) EP3400082A1 (es)
JP (1) JP7017511B2 (es)
KR (1) KR20180099705A (es)
CN (1) CN108472555A (es)
AR (1) AR107299A1 (es)
AU (1) AU2016384271B2 (es)
BR (1) BR112018013829A2 (es)
CA (1) CA3010190C (es)
CL (1) CL2018001844A1 (es)
CO (1) CO2018007037A2 (es)
GB (1) GB201600154D0 (es)
IL (1) IL259644B (es)
MX (1) MX2018008340A (es)
MY (1) MY198655A (es)
PE (1) PE20181454A1 (es)
RU (1) RU2768732C2 (es)
SG (2) SG10202006429YA (es)
TW (1) TWI733732B (es)
UA (1) UA125583C2 (es)
UY (1) UY37066A (es)
WO (1) WO2017118591A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3682959A1 (en) * 2019-01-16 2020-07-22 Sck Cen Purification of actinium
KR102490805B1 (ko) * 2019-07-02 2023-01-20 니혼 메디피직스 가부시키가이샤 226Ra 함유 용액의 정제 방법, 226Ra 타깃의 제조 방법, 및 225Ac의 제조 방법
CN111398469B (zh) * 2020-04-09 2020-10-27 中国科学院地质与地球物理研究所 一种小样品量的第四纪土壤碳酸盐的定年方法
EP4260346A1 (en) * 2020-12-10 2023-10-18 Advanced Accelerator Applications Method for producing high purity and high specific activity radionuclides
CN117051271B (zh) * 2023-06-27 2026-02-10 国电投核素同创(重庆)科技有限公司 一种钍与散裂元素的分离方法
WO2026008841A1 (en) * 2024-07-05 2026-01-08 Thor Medical Asa Process for production of useful radionucleides

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5809394A (en) * 1996-12-13 1998-09-15 Battelle Memorial Institute Methods of separating short half-life radionuclides from a mixture of radionuclides
NO310544B1 (no) * 1999-01-04 2001-07-23 Algeta As Opparbeidelse og anvendelse av radium-223 til fremstilling av preparat samt kit til behandling av kalsifisert vev for palliasjon, benkreft-terapi og/eller overflatebehandling av ben
NO313180B1 (no) * 2000-07-04 2002-08-26 Anticancer Therapeutic Inv Sa Bensökende alfapartikkel emitterende radiofarmasöytika
US20060228297A1 (en) * 2003-04-15 2006-10-12 Roy Larsen Thorium-227 for use in radiotherapy of soft tissue disease
CA2522148C (en) * 2003-04-15 2010-07-13 Algeta As Thorium-227 for use in radiotherapy of soft tissue disease
TWI372763B (en) * 2005-06-17 2012-09-21 Wyeth Llc Methods of purifying anti a beta antibodies
GB201002508D0 (en) * 2010-02-12 2010-03-31 Algeta As Product
GB201007354D0 (en) * 2010-04-30 2010-06-16 Algeta Asa Method
GB201208309D0 (en) 2012-05-11 2012-06-27 Algeta As Complexes
US9951399B2 (en) 2014-04-09 2018-04-24 Los Alamos National Security, Llc Separation of protactinum, actinium, and other radionuclides from proton irradiated thorium target

Also Published As

Publication number Publication date
SG10202006429YA (en) 2020-08-28
IL259644B (en) 2022-08-01
CO2018007037A2 (es) 2018-07-19
BR112018013829A2 (pt) 2018-12-11
US20190009265A1 (en) 2019-01-10
TWI733732B (zh) 2021-07-21
RU2768732C2 (ru) 2022-03-24
KR20180099705A (ko) 2018-09-05
US11452999B2 (en) 2022-09-27
MX2018008340A (es) 2018-09-17
RU2018127822A3 (es) 2020-03-17
CA3010190C (en) 2023-07-11
CA3010190A1 (en) 2017-07-13
WO2017118591A1 (en) 2017-07-13
UY37066A (es) 2017-08-31
JP7017511B2 (ja) 2022-02-08
PE20181454A1 (es) 2018-09-12
AU2016384271B2 (en) 2022-05-12
AU2016384271A1 (en) 2018-06-21
GB201600154D0 (en) 2016-02-17
UA125583C2 (uk) 2022-04-27
AR107299A1 (es) 2018-04-18
TW201726586A (zh) 2017-08-01
MY198655A (en) 2023-09-13
RU2018127822A (ru) 2020-02-06
IL259644A (en) 2018-07-31
CN108472555A (zh) 2018-08-31
US20200406247A1 (en) 2020-12-31
SG11201805459UA (en) 2018-07-30
JP2019509467A (ja) 2019-04-04
EP3400082A1 (en) 2018-11-14

Similar Documents

Publication Publication Date Title
CL2018001844A1 (es) Método de preparación de isótopos
MX2022002990A (es) Producto oral con una amina basica y un agente de apareamiento de iones.
BR112015025172A2 (pt) composição farmacêutica
MX2014000367A (es) Sistema de inyeccion de una suspension de carbonato de calcio (caco3) micronizada para la remineralizacion del agua desalinizada y dulce.
MX2020003316A (es) Composición de champú compacto que contiene surfactantes libres de sulfato.
CL2016001287A1 (es) Benzamidas sustituidas y procedimiento para su uso
CL2018003504A1 (es) Derivados de carbonucleósidos sustituidos útiles como agentes antineoplasicos.
CO2018003134A2 (es) Composiciones para el cuidado bucal que comprenden un aminoácido básico, una combinación de fuentes de iones de zinc y un sistema quelante
CU20170172A7 (es) 4,6-diaminoquinolin-3-carbonitrilos sustituidos útiles como agentes analgésicos, antipiréticos o antiinflamatorios y antineoplásicos
BR112014029754B1 (pt) soluções de tensoativos que contêm n-metil-noleilglucaminas e n-metil-n-c12-c14 acilglucaminas e seu uso, processo para produzir composições cosméticas e composição
GT201400230A (es) Necleòsidos de espìrooxetano de uracilo
AR091039A1 (es) Composiciones farmaceuticas topicas que comprenden terbinafina, uso y metodo de tratamiento
BRPI0412059A (pt) método para a preparação de formulação de liberação controlada
CL2019001631A1 (es) Formulación de mezcla que comprende células y un ácido graso poliinsaturado que tiene al menos 20 átomos de carbono (lc-pufa).
BR112015024938A2 (pt) formulação, uso de formulações, e, processo para preparação de formulações
CO6761374A2 (es) Derivados de heteroarilo como moduladores de nachr alfa 7
BR112017015958A2 (pt) material de base transdermicamente absorvível contendo composto lípido-péptido
CL2021003228A1 (es) Compuestos tricíclicos y su uso
AR098588A1 (es) Composiciones para el cuidado oral
CL2018003110A1 (es) Preparación y dispersión de formulaciones de emulsión estable.
AR109795A1 (es) Cátsup de tomate que tiene estabilidad de almacenamiento mejorada
AR088213A1 (es) Formulacion granulada soluble en agua de sal 2,4-d y metodo para su preparacion
AR111760A1 (es) Compuestos y composiciones para el tratamiento de tumores sólidos mediante administración intratumoral
MX2019003884A (es) Composicion detergente para lavanderia con un ph bajo.
NI201200141A (es) Hidrato del hidrobromuro de agomelatina y preparación de éste