CN102634983B - Antibacterial and wrinkle finishing solution for denim garments and preparation method for denim garments - Google Patents
Antibacterial and wrinkle finishing solution for denim garments and preparation method for denim garments Download PDFInfo
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 91
- 230000037303 wrinkles Effects 0.000 title claims abstract description 55
- 238000002360 preparation method Methods 0.000 title claims abstract description 28
- 238000001035 drying Methods 0.000 claims abstract description 35
- 239000003242 anti bacterial agent Substances 0.000 claims abstract description 27
- 239000011347 resin Substances 0.000 claims abstract description 23
- 229920005989 resin Polymers 0.000 claims abstract description 23
- 239000000835 fiber Substances 0.000 claims abstract description 16
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 13
- 239000011814 protection agent Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000007493 shaping process Methods 0.000 claims abstract 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 20
- 229910052742 iron Inorganic materials 0.000 claims description 10
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical group [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 6
- 238000007654 immersion Methods 0.000 claims description 3
- 238000005406 washing Methods 0.000 abstract description 22
- 230000000694 effects Effects 0.000 abstract description 21
- 239000007788 liquid Substances 0.000 abstract description 16
- 238000000034 method Methods 0.000 abstract description 7
- 238000010521 absorption reaction Methods 0.000 abstract description 2
- 238000002788 crimping Methods 0.000 abstract description 2
- 208000018999 crinkle Diseases 0.000 abstract 1
- 238000005470 impregnation Methods 0.000 abstract 1
- 230000002045 lasting effect Effects 0.000 abstract 1
- 206010040954 Skin wrinkling Diseases 0.000 description 61
- 239000004753 textile Substances 0.000 description 16
- 241000191967 Staphylococcus aureus Species 0.000 description 9
- 239000003795 chemical substances by application Substances 0.000 description 6
- 230000000149 penetrating effect Effects 0.000 description 6
- 229920001661 Chitosan Polymers 0.000 description 4
- 238000009987 spinning Methods 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000007730 finishing process Methods 0.000 description 2
- 125000001453 quaternary ammonium group Chemical group 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- -1 1-10g of penetrant Substances 0.000 description 1
- 241000282693 Cercopithecidae Species 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000005541 medical transmission Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 230000037331 wrinkle reduction Effects 0.000 description 1
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Abstract
本发明涉及一种牛仔服装抗菌压皱的整理液，以及利用该整理液作为具有抗菌压皱一体化功能的牛仔服装制备方法，该制备方法包括：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干；其中，上述提及配制牛仔服装抗菌压皱一体化功能的整理液，其各组分及重量配比为：水 800-1200g、压皱树脂100-200g、渗透剂1-10g、抗菌剂3-10g、交联剂1-10g、纤维保护剂1-20g；本发明的牛仔服装，在赋予传统牛仔服装压皱效果的同时，也得到了具有高附加值的抗菌效果，且不影响其本身的吸湿透气性能，提供持久清新和舒适。
The invention relates to an antibacterial and wrinkle finishing solution for denim garments, and a method for preparing denim garments with integrated antibacterial and wrinkle functions using the finishing solution. ——Impregnation and finishing liquid for denim clothing——Pre-drying treatment—Crinkle treatment——High temperature curing and shaping treatment—Washing and drying; Among them, the preparation of the finishing liquid with integrated antibacterial and wrinkle functions for denim clothing mentioned above, its The components and weight ratio are: 800-1200g of water, 100-200g of crimping resin, 1-10g of penetrant, 3-10g of antibacterial agent, 1-10g of crosslinking agent, 1-20g of fiber protection agent; Denim clothing, while endowing traditional denim clothing with a wrinkled effect, also has a high value-added antibacterial effect without affecting its own moisture absorption and breathability, providing lasting freshness and comfort.
Description
技术领域 technical field
本发明涉及纺织面料及纺织品后整理技术领域，具体来说，系涉及一种牛仔服装抗菌压皱的整理液，以及该整理液作为牛仔服装的制备方法。 The invention relates to the technical field of finishing of textile fabrics and textiles, in particular to an antibacterial and wrinkle finishing solution for denim garments, and a method for preparing the finishing solution as a denim garment.
背景技术 Background technique
纺织品非常容易滋生病菌，是疾病的重要传播源。人们日常使用的各种纺织品，都是细菌滋生繁衍和传播的适宜场所，各种细菌在条件适宜时会迅速繁殖，不仅会使纤维制品变色、发霉、降解等，还会对人体皮肤产生异常的刺激并诱发各种皮肤病，造成对人类生活的种种危害，因此赋予纺织品抗菌功能是其服用性能升级的重要手段。牛仔服装因其本身独特的气质深受消费者的喜爱，成为了人们的一种主要消费品，其需求量相当可观。然而由于牛仔服装换洗频率不如内衣、裤，可能滋长的细菌、病毒数更加令人担忧。对牛仔布进行抗菌整理，可赋予牛仔服装抗菌功能性，提高牛仔服装的附加值。 Textiles are very susceptible to germs and are an important source of disease transmission. All kinds of textiles that people use every day are suitable places for bacteria to multiply and spread. When the conditions are suitable, various bacteria will multiply rapidly, which will not only cause discoloration, mildew, degradation, etc. of fiber products, but also cause abnormal damage to human skin. Stimulate and induce various skin diseases and cause various hazards to human life. Therefore, endowing textiles with antibacterial function is an important means to upgrade their wearing performance. Denim clothing is deeply loved by consumers because of its unique temperament, and has become a major consumer product for people, and its demand is considerable. However, because denim clothing is not as frequent as underwear and pants, the number of bacteria and viruses that may grow is even more worrying. Antibacterial finishing of denim can endow denim with antibacterial function and increase the added value of denim.
目前，抗菌纺织品可分为天然抗菌纺织品和人造抗菌纺织品。人造抗菌纺织品常见的制备工艺主要分为熔融共纺、后整理两大类。熔融共纺是将抗菌剂制成抗菌母粒加入普通基料中，通过共混、熔融、喷丝等工序，加工成抗菌纤维，并进一步加工成各类纺织品，通过此类方式加工的产品抗菌性能较为持久；后整理则是通过浸轧、喷涂等方法，用抗菌剂对纺织品进行后处理，在纺织品表面涂覆一层抗菌层，从而赋予其抗菌性能，此方式加工的抗菌纺织品，抗菌剂能较好地分布于产品表面，有利于体现产品的抗菌性能，尤其适用于天然纤维制成的纺织品的抗菌加工，但随着产品的磨损抗菌性能可能逐渐丧失。 At present, antibacterial textiles can be divided into natural antibacterial textiles and artificial antibacterial textiles. The common preparation processes of artificial antibacterial textiles are mainly divided into two categories: melt co-spinning and finishing. Melt co-spinning is to make antibacterial agents into antibacterial masterbatches and add them to ordinary base materials. Through blending, melting, spinning and other processes, they are processed into antibacterial fibers, and further processed into various textiles. Products processed in this way are antibacterial The performance is relatively long-lasting; the finishing is to post-treat the textile with an antibacterial agent by padding, spraying, etc., and coat a layer of antibacterial layer on the surface of the textile to endow it with antibacterial properties. Antibacterial textiles processed in this way, antibacterial agent It can be better distributed on the surface of the product, which is beneficial to reflect the antibacterial performance of the product, especially suitable for the antibacterial processing of textiles made of natural fibers, but the antibacterial performance may gradually lose as the product wears.
对于牛仔服装而言，其制作过程中，要经过各种复杂的水洗工艺，如：酵洗、喷马骝、压皱等，以及反复的水洗，在这一系列的整理过程中，天然抗菌纺织品及用熔融共纺制备的抗菌纺织品的抗菌性能可能被酸、碱、高锰酸钾等破坏，无法得到最终具有抗菌功能的牛仔服装。 For denim clothing, in the production process, it has to go through various complicated washing processes, such as: yeast washing, spraying monkeys, creasing, etc., and repeated washing. In this series of finishing processes, natural antibacterial textiles And the antibacterial properties of the antibacterial textiles prepared by melt co-spinning may be destroyed by acid, alkali, potassium permanganate, etc., and the final denim clothing with antibacterial function cannot be obtained.
故此，到目前为止，还没有发现关于制备抗菌压皱一体化功能的牛仔服装方面的技术申请专利。 Therefore, so far, no technical application patent has been found about the preparation of denim garments with antibacterial and wrinkle-integrated functions.
发明内容 Contents of the invention
本发明的目的在于克服上述现有技术存在的问题，而提供一种牛仔服装抗菌压皱的整理液，以及利用该整理液作为牛仔服装的制备方法；此整理液具有抗菌压皱一体化功能，而且，采用这种抗菌压皱一体化功能的整理液，运用高温固化工艺制备，使牛仔服装具有抗菌压皱一体化功能的效果。 The purpose of the present invention is to overcome the problems in the above-mentioned prior art, and provide a kind of antibacterial and wrinkled finishing solution for denim garments, and use the finishing solution as a preparation method for denim garments; this finishing solution has the integrated function of antibacterial and wrinkle, Moreover, the finishing solution with the integrated function of antibacterial and wrinkle is used to prepare the denim garment with the integrated function of antibacterial and wrinkle through high-temperature curing process.
本发明的整理液系采用以下技术措施解决： The finishing liquid system of the present invention adopts the following technical measures to solve:
一种牛仔服装抗菌压皱的整理液，其特征是，它包括以下组分及其重量配比：水 800-1200g、压皱树脂100-200g、渗透剂1-10g、抗菌剂3-10g、交联剂1-10g、纤维保护剂1-20g。 An antibacterial and wrinkle finishing solution for denim clothing, characterized in that it comprises the following components and their weight ratios: 800-1200g of water, 100-200g of wrinkle resin, 1-10g of penetrant, 3-10g of antibacterial agent, Crosslinking agent 1-10g, fiber protection agent 1-20g.
上述整理液，还可以有以下更佳的实施方案： Above-mentioned finishing solution, also can have following better embodiment:
所述压皱树脂可以系2D树脂，或改性2D树脂。 The crimping resin may be a 2D resin, or a modified 2D resin.
所述抗菌剂可以系纳米银抗菌剂，或壳聚糖类抗菌剂或季铵盐类抗菌剂等。 The antibacterial agent can be a nano-silver antibacterial agent, or a chitosan antibacterial agent or a quaternary ammonium salt antibacterial agent.
上述制成的整理液作为牛仔服装的制备方法，其特征是，它包括如下步骤： The above-mentioned finishing solution made as the preparation method of denim clothing is characterized in that it comprises the steps:
步骤A，按照各组分及质量百分比，配制牛仔服装抗菌压皱的整理液，备用； Step A, according to each component and mass percentage, prepare denim clothing antibacterial and wrinkle finishing liquid, set aside;
步骤B，将牛仔服装浸渍在上述配制好的整理液中，浸渍10-40分钟，浸渍温度控制在25~60℃，然后用甩干机甩干，时间控制在1-5分钟； Step B, immerse the denim garment in the above prepared finishing solution for 10-40 minutes, the immersion temperature is controlled at 25-60°C, and then dried with a spin dryer for 1-5 minutes;
步骤C，把上述甩干处理后的牛仔服装，放在烘道式烘炉中预烘干，其温度控制在60-80℃，时间为5-10分钟； Step C, pre-drying the above-mentioned denim garments after drying treatment in a drying tunnel oven, the temperature is controlled at 60-80°C, and the time is 5-10 minutes;
步骤D，把上述经预烘干处理的牛仔服装，采用烫斗压皱或圆筒压皱处理； Step D, the above-mentioned pre-dried denim garments are crumpled with an iron or cylinder;
步骤E，把压皱处理后的牛仔服装，放在焗炉中进行定型处理，其温度控制在120-180℃，时间为15-30分钟； Step E, putting the wrinkled denim garment in an oven for shaping treatment, the temperature is controlled at 120-180° C., and the time is 15-30 minutes;
步骤F，最后，将定型处理后的牛仔服装水洗、烘干。 Step F, finally, wash and dry the denim garment after the styling treatment.
本发明的有益效果如下： The beneficial effects of the present invention are as follows:
（1）本发明的牛仔服装抗菌压皱一体化功能整理液，具有压皱和抗菌的双重功能，在赋予牛仔服装良好的压皱效果的同时，也赋予了牛仔服装优异的抗菌效果。 (1) The antibacterial and wrinkle-integrated functional finishing solution for denim garments of the present invention has dual functions of wrinkle reduction and antibacterial, and can endow denim garments with excellent antibacterial effects while imparting a good creasing effect to denim garments.
（2）本发明还提供了一种具有抗菌压皱一体化功能的牛仔服装的制备方法，采用牛仔服装抗菌压皱一体化功能整理液，在传统的牛仔服装压皱工序中添加抗菌剂与压皱树脂同浴整理牛仔服装，采用一浴法整理工艺，制备出一种具有抗菌功能的压皱牛仔服装，从而赋予传统牛仔服装抗菌压皱双重功能。整理后的牛仔服装抗菌和压皱效果好，牛仔服装吸湿透气性好。该方法提高了生产效率，节约了生产成本，提高了牛仔服装的附加值。 (2) The present invention also provides a method for preparing denim garments with integrated functions of antibacterial and creasing, using the finishing liquid with integrated functions of antibacterial and creasing for denim garments, adding antibacterial agents and pressing One-bath finishing process for denim garments with wrinkle resin was adopted to prepare a wrinkled denim garment with antibacterial function, thus endowing traditional denim garments with antibacterial and wrinkle double functions. The finished denim garment has good antibacterial and wrinkle effects, and the denim garment has good moisture absorption and air permeability. The method improves production efficiency, saves production cost and increases the added value of denim clothing.
附图说明 Description of drawings
图1为本发明具有抗菌压皱一体化功能的牛仔服装制备方法的流程图。 Fig. 1 is a flow chart of the denim garment preparation method with integrated antibacterial and wrinkle functions of the present invention.
具体实施方式 Detailed ways
下面结合具体实施例对本发明做进一步详细描述。 The present invention will be further described in detail below in conjunction with specific embodiments.
牛仔服装抗菌压皱一体化功能整理液，它的各组分及其重量配比，以每升（即：1000 g）水中添加为例：压皱树脂100-200g，渗透剂1-10g，抗菌剂3-10g，交联剂1-10g，纤维保护剂1-20g；其中，所述压皱树脂为2D树脂或改性2D树脂；且，所述抗菌剂可以系纳米银抗菌剂，或壳聚糖类抗菌剂，或季铵盐类抗菌剂等。 Antibacterial and wrinkle integrated functional finishing fluid for denim clothing, its components and their weight ratios, taking per liter (ie: 1000 g) of water as an example: 100-200g of wrinkle resin, 1-10g of penetrant, antibacterial agent 3-10g, crosslinking agent 1-10g, fiber protection agent 1-20g; wherein, the crumpled resin is 2D resin or modified 2D resin; and, the antibacterial agent can be nano silver antibacterial agent, or shell Polysaccharide antibacterial agents, or quaternary ammonium salt antibacterial agents, etc.
如图1所示，系一种利用上述制备的整理液，作为牛仔服装的制备方法，它包括以下步骤： As shown in Figure 1, be a kind of finishing liquid that utilizes above-mentioned preparation, as the preparation method of denim garment, it comprises the following steps:
步骤A，按照各组分及质量百分比，配制牛仔服装抗菌压皱的整理液，备用； Step A, according to each component and mass percentage, prepare denim clothing antibacterial and wrinkle finishing liquid, set aside;
步骤B，将牛仔服装浸渍在上述配制好的整理液中，浸渍10-40分钟，浸渍温度控制在25~60℃，然后用甩干机甩干，时间控制在1-5分钟； Step B, immerse the denim garment in the above prepared finishing solution for 10-40 minutes, the immersion temperature is controlled at 25-60°C, and then dried with a spin dryer for 1-5 minutes;
步骤C，把上述甩干处理后的牛仔服装，放在烘道式烘炉中预烘干，其温度控制在60-80℃，时间为5-10分钟； Step C, pre-drying the above-mentioned denim garments after drying treatment in a drying tunnel oven, the temperature is controlled at 60-80°C, and the time is 5-10 minutes;
步骤D，把上述经预烘干处理的牛仔服装，采用烫斗压皱或圆筒压皱处理； Step D, the above-mentioned pre-dried denim garments are crumpled with an iron or cylinder;
步骤E，把压皱处理后的牛仔服装，放在焗炉中进行定型处理，其温度控制在120-180℃，时间为15-30分钟； Step E, putting the wrinkled denim garment in an oven for shaping treatment, the temperature is controlled at 120-180° C., and the time is 15-30 minutes;
步骤F，最后，将定型处理后的牛仔服装水洗、烘干。 Step F, finally, wash and dry the denim garment after the styling treatment.
以下用几个具体实施例，作进一步的详细说明。 Below with several specific examples, be described in further detail.
实施例1Example 1
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：2D树脂100g，渗透剂JFC 1g，纳米银抗菌剂3g，交联剂1g，纤维保护剂G-617 1g。将牛仔服装浸渍在整理液中，温度25℃，浸渍时间30分钟，然后在甩干机中甩5分钟，再在烘道式烘炉中预烘干10分钟，温度为60℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉高温固化30min，温度为120℃。 Among them, the weight ratio of each component of denim clothing functional finishing liquid is to add per liter of water: 100g of 2D resin, 1g of penetrating agent JFC, 3g of nano-silver antibacterial agent, 1g of crosslinking agent, and 1g of fiber protection agent G-617. Immerse denim garments in the finishing solution at a temperature of 25°C for 30 minutes, then spin them in a spin dryer for 5 minutes, then pre-dry them in a drying tunnel oven for 10 minutes at a temperature of 60°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to a high-temperature oven for high-temperature curing for 30 minutes at a temperature of 120°C.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可 The denim garment obtained has obvious wrinkle effect, and through the antibacterial test, the antibacterial rate to Staphylococcus aureus can reach
达91%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 Up to 91% or more. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
实施例2Example 2
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：2D树脂150g，渗透剂JFC 5g，纳米银抗菌剂5g，交联剂5g，纤维保护剂G-617 5g。将牛仔服装浸渍在整理液中，温度40℃，浸渍时间10分钟，然后在甩干机中甩1分钟，再在烘道式烘炉中预烘干5分钟，温度为70℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉，高温固化温度为140℃，时间为20min。 Among them, the weight ratio of each component of denim clothing functional finishing liquid is added per liter of water: 150g of 2D resin, 5g of penetrating agent JFC, 5g of nano-silver antibacterial agent, 5g of crosslinking agent, and 5g of fiber protection agent G-617. Immerse denim garments in the finishing solution at a temperature of 40°C for 10 minutes, then spin in a spin dryer for 1 minute, then pre-dry them in a tunnel oven for 5 minutes at a temperature of 70°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to high temperature oven, high temperature curing temperature is 140 ℃, time is 20min.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可达95%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 The obtained denim garment has obvious wrinkle effect, and after antibacterial test, the antibacterial rate against Staphylococcus aureus can reach more than 95%. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
实施例3Example 3
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：2D树脂200g，渗透剂JFC 10g，纳米银抗菌剂10g，交联剂10g，纤维保护剂AD-40 20g。将牛仔服装浸渍在整理液中，温度60℃，浸渍时间20分钟，然后在甩干机中甩1分钟，再在烘道式烘炉中预烘干8分钟，温度为80℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉，高温固化温度为180℃，时间为15min。 Among them, the weight ratio of each component of denim clothing functional finishing liquid is to add per liter of water: 200g of 2D resin, 10g of penetrating agent JFC, 10g of nano-silver antibacterial agent, 10g of crosslinking agent, and 20g of fiber protection agent AD-40. Immerse denim garments in the finishing solution at a temperature of 60°C for 20 minutes, then spin in a spin dryer for 1 minute, then pre-dry them in a drying tunnel oven for 8 minutes at a temperature of 80°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to high temperature oven, high temperature curing temperature is 180 ℃, time is 15min.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可达98%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 The obtained denim garment has obvious wrinkle effect, and after antibacterial test, the antibacterial rate against Staphylococcus aureus can reach more than 98%. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
实施例4Example 4
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：醚化2D树脂100g，渗透剂MCH-127 1g，壳聚糖类抗菌剂3g，交联剂1g，纤维保护剂HA-soft80 1g。将牛仔服装浸渍在整理液中，温度25℃，浸渍时间30分钟，然后在甩干机中甩5分钟，再在烘道式烘炉中预烘干10分钟，温度为60℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉高温固化30min，温度为120℃。 Wherein the weight ratio of each component of denim clothing functional finishing liquid is to add in every liter of water: etherified 2D resin 100g, penetrant MCH-127 1g, chitosan antibacterial agent 3g, crosslinking agent 1g, fiber protection agent HA -soft80 1g. Immerse denim garments in the finishing solution at a temperature of 25°C for 30 minutes, then spin them in a spin dryer for 5 minutes, then pre-dry them in a drying tunnel oven for 10 minutes at a temperature of 60°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to a high-temperature oven for high-temperature curing for 30 minutes at a temperature of 120°C.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可达90%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 The obtained denim garment has obvious wrinkle effect, and after antibacterial test, the antibacterial rate against Staphylococcus aureus can reach more than 90%. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
实施例5Example 5
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：醚化2D树脂150g，渗透剂MCH-127 5g，壳聚糖类抗菌剂5g，交联剂5g，纤维保护剂HA-soft80 5g。将牛仔服装浸渍在整理液中，温度40℃，浸渍时间10分钟，然后在甩干机中甩1分钟，再在烘道式烘炉中预烘干5分钟，温度为70℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉，高温固化温度为140℃，时间为20min。 Wherein the weight ratio of each component of denim clothing functional finishing liquid is to add in every liter of water: etherified 2D resin 150g, penetrant MCH-127 5g, chitosan antibacterial agent 5g, crosslinking agent 5g, fiber protection agent HA -soft80 5g. Immerse denim garments in the finishing solution at a temperature of 40°C for 10 minutes, then spin in a spin dryer for 1 minute, then pre-dry them in a tunnel oven for 5 minutes at a temperature of 70°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to high temperature oven, high temperature curing temperature is 140 ℃, time is 20min.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可达94%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 The obtained denim garment has obvious wrinkle effect, and after antibacterial test, the antibacterial rate against Staphylococcus aureus can reach more than 94%. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
实施例6Example 6
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：醚化2D树脂200g，渗透剂MCH-127 10g，壳聚糖类抗菌剂10g，交联剂10g，纤维保护剂HA-soft80 20g。将牛仔服装浸渍在整理液中，温度60℃，浸渍时间20分钟，然后在甩干机中甩1分钟，再在烘道式烘炉中预烘干8分钟，温度为80℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉，高温固化温度为180℃，时间为15min。 Wherein the weight ratio of each component of denim clothing functional finishing liquid is to add in every liter of water: etherified 2D resin 200g, penetrating agent MCH-127 10g, chitosan antibacterial agent 10g, crosslinking agent 10g, fiber protection agent HA -soft80 20g. Immerse denim garments in the finishing solution at a temperature of 60°C for 20 minutes, then spin in a spin dryer for 1 minute, then pre-dry them in a drying tunnel oven for 8 minutes at a temperature of 80°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to high temperature oven, high temperature curing temperature is 180 ℃, time is 15min.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可达95%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 The obtained denim garment has obvious wrinkle effect, and after antibacterial test, the antibacterial rate against Staphylococcus aureus can reach more than 95%. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
实施例7Example 7
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：醚化2D树脂100g，渗透剂JFC 1g，季铵盐类抗菌剂3g，交联剂1g，纤维保护剂PT3 1g。将牛仔服装浸渍在整理液中，温度25℃，浸渍时间30分钟，然后在甩干机中甩5分钟，再在烘道式烘炉中预烘干10分钟，温度为60℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉高温固化30min，温度为120℃。 Among them, the weight ratio of each component of denim clothing functional finishing liquid is to add per liter of water: etherified 2D resin 100g, penetrant JFC 1g, quaternary ammonium antibacterial agent 3g, crosslinking agent 1g, fiber protection agent PT3 1g. Immerse denim garments in the finishing solution at a temperature of 25°C for 30 minutes, then spin them in a spin dryer for 5 minutes, then pre-dry them in a drying tunnel oven for 10 minutes at a temperature of 60°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to a high-temperature oven for high-temperature curing for 30 minutes at a temperature of 120°C.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可达94%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 The obtained denim garment has obvious wrinkle effect, and after antibacterial test, the antibacterial rate against Staphylococcus aureus can reach more than 94%. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
实施例8Example 8
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：醚化2D树脂150g，渗透剂JFC 5g，季铵盐类抗菌剂5g，交联剂5g，纤维保护剂PT3 5g。将牛仔服装浸渍在整理液中，温度40℃，浸渍时间10分钟，然后在甩干机中甩1分钟，再在烘道式烘炉中预烘干5分钟，温度为70℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉，高温固化温度为140℃，时间为20min。 Wherein the weight ratio of each component of denim garment functional finishing liquid is to add per liter of water: etherified 2D resin 150g, penetrating agent JFC 5g, quaternary ammonium salt antibacterial agent 5g, crosslinking agent 5g, fiber protection agent PT3 5g. Immerse denim garments in the finishing solution at a temperature of 40°C for 10 minutes, then spin in a spin dryer for 1 minute, then pre-dry them in a tunnel oven for 5 minutes at a temperature of 70°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to high temperature oven, high temperature curing temperature is 140 ℃, time is 20min.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可达97%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 The obtained denim garment has obvious wrinkle effect, and after antibacterial test, the antibacterial rate against Staphylococcus aureus can reach more than 97%. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
实施例9Example 9
一种具有抗菌压皱一体化功能的牛仔服装的制备方法为：牛仔服装抗菌压皱一体化功能整理液的配制——牛仔服装浸渍整理液——预烘干处理——压皱处理——高温固化定型处理——水洗、烘干。 A preparation method for denim garments with antibacterial and wrinkle integrated functions: preparation of denim garment antibacterial and wrinkle integrated functional finishing solution—denim garment impregnated finishing solution—pre-drying treatment—wrinkle treatment—high temperature Curing and setting treatment - washing and drying.
其中牛仔服装功能整理液的各组分的重量配比为每升水中添加：醚化2D树脂200g，渗透剂JFC 10g，季铵盐类抗菌剂10g，交联剂10g，纤维保护剂PT3 20g。将牛仔服装浸渍在整理液中，温度60℃，浸渍时间20分钟，然后在甩干机中甩1分钟，再在烘道式烘炉中预烘干8分钟，温度为80℃，再经过烫斗压皱或圆筒压皱，送入高温焗炉，高温固化温度为180℃，时间为15min。 Among them, the weight ratio of each component of denim garment functional finishing liquid is to add per liter of water: 200g of etherified 2D resin, 10g of penetrating agent JFC, 10g of quaternary ammonium antibacterial agent, 10g of crosslinking agent, and 20g of fiber protection agent PT3. Immerse denim garments in the finishing solution at a temperature of 60°C for 20 minutes, then spin in a spin dryer for 1 minute, then pre-dry them in a drying tunnel oven for 8 minutes at a temperature of 80°C, and then iron them. Bucket crumpling or cylinder crumpling, sent to high temperature oven, high temperature curing temperature is 180 ℃, time is 15min.
所得的牛仔服装具有明显的压皱效果，且经过抗菌测试，对金黄色葡萄球菌的抑菌率可达98%以上。经过十次水洗后，其压皱效果无变化，抑菌效果优异。 The obtained denim garment has obvious wrinkle effect, and after antibacterial test, the antibacterial rate against Staphylococcus aureus can reach more than 98%. After ten times of washing, the wrinkle effect remains unchanged, and the antibacterial effect is excellent.
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