CN104695114A - Linen-fabric anticorrosive and antibacterial treatment process - Google Patents
Linen-fabric anticorrosive and antibacterial treatment process Download PDFInfo
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- CN104695114A CN104695114A CN201510126874.6A CN201510126874A CN104695114A CN 104695114 A CN104695114 A CN 104695114A CN 201510126874 A CN201510126874 A CN 201510126874A CN 104695114 A CN104695114 A CN 104695114A
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- 239000004744 fabric Substances 0.000 title claims abstract description 91
- 238000000034 method Methods 0.000 title claims abstract description 58
- 230000008569 process Effects 0.000 title claims abstract description 56
- 230000000844 anti-bacterial effect Effects 0.000 title abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 43
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000000835 fiber Substances 0.000 claims abstract description 34
- 238000005406 washing Methods 0.000 claims abstract description 19
- 229960000583 acetic acid Drugs 0.000 claims abstract description 18
- 239000012362 glacial acetic acid Substances 0.000 claims abstract description 18
- 241000255789 Bombyx mori Species 0.000 claims abstract description 10
- 229920000742 Cotton Polymers 0.000 claims abstract description 10
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 10
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 9
- 241000208202 Linaceae Species 0.000 claims description 69
- 235000004431 Linum usitatissimum Nutrition 0.000 claims description 69
- 230000002421 anti-septic effect Effects 0.000 claims description 17
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims description 17
- 241000894006 Bacteria Species 0.000 claims description 12
- 230000002401 inhibitory effect Effects 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 9
- ATROHALUCMTWTB-OWBHPGMISA-N phoxim Chemical compound CCOP(=S)(OCC)O\N=C(\C#N)C1=CC=CC=C1 ATROHALUCMTWTB-OWBHPGMISA-N 0.000 claims description 9
- 229950001664 phoxim Drugs 0.000 claims description 9
- 238000007598 dipping method Methods 0.000 claims description 8
- 238000009413 insulation Methods 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 8
- 241000238631 Hexapoda Species 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 2
- 239000004902 Softening Agent Substances 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000007654 immersion Methods 0.000 abstract 1
- WBHQBSYUUJJSRZ-UHFFFAOYSA-M sodium bisulfate Chemical compound [Na+].OS([O-])(=O)=O WBHQBSYUUJJSRZ-UHFFFAOYSA-M 0.000 abstract 1
- 229910000342 sodium bisulfate Inorganic materials 0.000 abstract 1
- 239000004753 textile Substances 0.000 description 9
- 230000000845 anti-microbial effect Effects 0.000 description 3
- 230000003115 biocidal effect Effects 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- 230000002335 preservative effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000012209 synthetic fiber Substances 0.000 description 2
- 229920002994 synthetic fiber Polymers 0.000 description 2
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- 208000006877 Insect Bites and Stings Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000004599 antimicrobial Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a linen-fabric anticorrosive and antibacterial treatment process. The process specifically includes the steps of 1), selecting warp and weft materials including linen fibers, silkworm protein fibers, soft silk fibers and the rest of cotton fibers, boiling off linen fabric at normal pressure prior to cyclically washing the linen fabric with hot water and cold water and cleaning the same with the cold water; 2), performing immersion treatment on the linen fabric and then washing the same for 6-8 times; 3), treating the linen fabric in a solution containing sodium hydrogen sulfate and glacial acetic acid and then washing the linen fabric for 6-8 times; 4), immersing the linen fabric in a softening agent solution for treatment and drying. The linen-fabric anticorrosive and antibacterial treatment process is simple and easy to operate, safe, environment friendly and pollution free, and raw materials for treatment are easy to obtain; the linen fabric after treatment is good in anticorrosive and antibacterial performance, insect resisting and moth proofing and long in service life.
Description
Technical field
The invention belongs to textile technology field, relate to a kind of flax fabric antiseptic and inhibiting bacteria function treatment process.
Background technology
China is the big country of textile production and outlet, china textile industry self is through development for many years, competitive advantage is fairly obvious, possesses most complete industrial chain in the world, the highest process mating level, the capacity of self-regulation of the industry cluster ground reply market risk of numerous prosperity constantly strengthens, and the developing steps keeping sane to industry provide solid guarantee.From international environment, international market still has expands space more greatly and opportunity.Along with 2007 the end of the year Central European textiles limit expire, 2008 the end of the year China-America Textile quota to limit end, China Textile quota-free era is coming, account for the area all-round opening of global piece market more than 60% share, bring huge opportunity will to China Textile trade.And the coming years, World Economics will be in first transition, will promote the growth of international trade, this brings favourable international market to ensure by increasing to China Textile Clothing Export.
Chemical constitution and the aggregated structure of regeneration and native cellulose fibre are different from synthetic fiber, containing more hydrophilic radical (hydroxyl) in their molecular structure, strand and crystal orientation poor, degree of crystallinity is lower, there is more microgap between strand and between fiber, result in excellent hygroscopicity, gas permeability and snugness of fit.But cellulose base fiber fabric easily shrinks deformation when taking and wash, wrinkle resistance, resilience are poor.
The antibiotic finish of fabric is one of method eliminating pathogenic microorganisms on fabric, and antibiotic finish is called as antimicrobial finish in the U.S. etc.; Antibacterial deodourizing processing is called as in Japan; Someone is referred to as hygienic finishing at home.Weaving antiseptic can be divided into natural, organic and inorganic three major types.Every class antiseptic has its pluses and minuses, and organic antiseptic is effective, wide in variety, is a most widely used class antiseptic at present, but there is the problems such as heat-resistant stable difference, is difficult to use in synthetic fiber spinning technique; Natural antimicrobial agent has good security usually, but its range of application is narrow, and majority has a strong impact on the coloured light of fabric; Inorganic antiseptic good heat resistance, but be difficult to obtain durable effect for after-finishing of textile products, and there is the toxicity problem of heavy metal in most of kind.
Summary of the invention
Technical problem to be solved by this invention is, overcome the shortcoming of prior art, a kind of flax fabric antiseptic and inhibiting bacteria function treatment process is provided, present invention process is simple to operation, and process raw material are easy to get, with low cost, and safety and environmental protection is pollution-free, flax fabric Antimicrobial preservative performance after present invention process process is good, and insect protected is mothproof, long service life.
In order to solve above technical problem, the invention provides a kind of flax fabric antiseptic and inhibiting bacteria function treatment process, comprising following concrete steps:
Step one: the graticule material selected is according to the mass fraction: linen fibre: 68-82 part, silkworm protein fiber 8-12 part, soft silk fiber 5-7 part, all the other are cotton fiber, are placed on by described flax fabric and boil in yarn pot, normal pressure kiering, kiering 8-10h, boil rear vexed 2-3h, then the flax fabric after kiering is first washed with hot water and circulating chilled water in pot, after taking the dish out of the pot, use cold flow water fully clean again;
Step 2: preparation temperature is in the weak acid solution of 35-38 DEG C, pH value is 4-5, be warmed up to 40-42 DEG C, add phoxim, adjustment concentration is 0.06-0.08%, by the flax fabric dipping after above-mentioned kiering in the solution, be warmed up to 72-74 DEG C again, process 26-28min, then cool to 43-45 DEG C, insulation 10-14min, is then immersed in the flax fabric of above-mentioned process in the clear water of 38-40 DEG C and cleans 6-8 time;
Step 3: flax fabric good for above-mentioned washing is processed 25-35min in the solution containing niter cake and glacial acetic acid, wherein niter cake concentration is 1.8%, glacial acetic acid concentration is 1.5%, treatment temperature is 42-44 DEG C, processing time is 13-15min; bath raio is 1:30, is then immersed in by the flax fabric of above-mentioned process in the clear water of 41-43 DEG C and cleans 6-8 time;
Step 4: it is process 55-59min in the softener solution of 3% that the flax fabric after washing in step 3 is immersed in concentration, and wherein treatment temperature is 36-38 DEG C, and bath raio is 1:45, then dry oven dry 24-28min under temperature is 130-140 DEG C of condition.
The invention has the beneficial effects as follows:
Present invention process adopts in linen fibre, adds silkworm protein fiber, soft silk fiber and cotton fiber, reduce the integral hardness of flax fabric, flexible silk is sliding more to make it, on the basis of feature not changing the distinctive tough and tensile durable and Antimicrobial preservative of linen fibre, improve the comfort level of contact human skin, husband is soft more, improves its thermal property.
Normal pressure kiering is adopted in present invention process, not only simple and convenient with low cost, and toughness and the pliability of fabric count line can be increased, kill most of bacterium and parasite, Environmental Safety simultaneously; The present invention also makes finishing agent by adding phoxim in weak acid solution, the fabric after its process, can anticorrosive mildewproof, effectively avoids insect bite to damage by worms, improves the properties of fabric, extend its service life; And then process in solution fabric being placed on niter cake and glacial acetic acid, can in and in fabric, there is irritating chemical substance, reduce the injury to human body; Finally, by the use of softener, then dry, on the basis of the toughness and antiseptic property of not damaging fabric fibre itself, the mothproof performance of insect protected of fabric can be improved, strengthen flexibility and the comfort level of fabric, slow down its aging speed, extend its service life.
Detailed description of the invention
embodiment 1
The present embodiment provides a kind of flax fabric antiseptic and inhibiting bacteria function treatment process, comprises following concrete steps:
Step one: the graticule material selected is according to the mass fraction: linen fibre: 68 parts, silkworm protein fiber 8 parts, soft silk fiber 5 parts, all the other are cotton fiber, are placed on by described flax fabric and boil in yarn pot, normal pressure kiering, kiering 8h, boil rear vexed 2h, then the flax fabric after kiering is first washed with hot water and circulating chilled water in pot, after taking the dish out of the pot, use cold flow water fully clean again;
Step 2: preparation temperature is in the weak acid solution of 35 DEG C, pH value is 4, be warmed up to 40 DEG C, add phoxim, adjustment concentration is 0.06%, by the flax fabric dipping after above-mentioned kiering in the solution, be warmed up to 72 DEG C again, process 28min, then cool to 43 DEG C, insulation 14min, is then immersed in the flax fabric of above-mentioned process in the clear water of 38 DEG C and cleans 8 times;
Step 3: flax fabric good for above-mentioned washing is processed 25min in the solution containing niter cake and glacial acetic acid, wherein niter cake concentration is 1.8%, glacial acetic acid concentration is 1.5%, treatment temperature is 42 DEG C, processing time is 15min; bath raio is 1:30, is then immersed in by the flax fabric of above-mentioned process in the clear water of 41 DEG C and cleans 8 times;
Step 4: it is process 55min in the softener solution of 3% that the flax fabric after washing in step 3 is immersed in concentration, and wherein treatment temperature is 36 DEG C, and bath raio is 1:45, then dry oven dry 28min under temperature is 130 DEG C of conditions.
embodiment 2
The present embodiment provides a kind of flax fabric antiseptic and inhibiting bacteria function treatment process, comprises following concrete steps:
Step one: the graticule material selected is according to the mass fraction: linen fibre: 82 parts, silkworm protein fiber 12 parts, soft silk fiber 7 parts, all the other are cotton fiber, are placed on by described flax fabric and boil in yarn pot, normal pressure kiering, kiering 10h, boil rear vexed 3h, then the flax fabric after kiering is first washed with hot water and circulating chilled water in pot, after taking the dish out of the pot, use cold flow water fully clean again;
Step 2: preparation temperature is in the weak acid solution of 38 DEG C, pH value is 5, be warmed up to 42 DEG C, add phoxim, adjustment concentration is 0.08%, by the flax fabric dipping after above-mentioned kiering in the solution, be warmed up to 74 DEG C again, process 26min, then cool to 45 DEG C, insulation 10min, is then immersed in the flax fabric of above-mentioned process in the clear water of 40 DEG C and cleans 6 times;
Step 3: flax fabric good for above-mentioned washing is processed 35min in the solution containing niter cake and glacial acetic acid, wherein niter cake concentration is 1.8%, glacial acetic acid concentration is 1.5%, treatment temperature is 44 DEG C, processing time is 13min; bath raio is 1:30, is then immersed in by the flax fabric of above-mentioned process in the clear water of 43 DEG C and cleans 6 times;
Step 4: it is process 59min in the softener solution of 3% that the flax fabric after washing in step 3 is immersed in concentration, and wherein treatment temperature is 38 DEG C, and bath raio is 1:45, then dry oven dry 24min under temperature is 140 DEG C of conditions.
embodiment 3
The present embodiment provides a kind of flax fabric antiseptic and inhibiting bacteria function treatment process, comprises following concrete steps:
Step one: the graticule material selected is according to the mass fraction: linen fibre: 75 parts, silkworm protein fiber 10 parts, soft silk fiber 6 parts, all the other are cotton fiber, are placed on by described flax fabric and boil in yarn pot, normal pressure kiering, kiering 9h, boil rear vexed 2.5h, then the flax fabric after kiering is first washed with hot water and circulating chilled water in pot, after taking the dish out of the pot, use cold flow water fully clean again;
Step 2: preparation temperature is in the weak acid solution of 36 DEG C, pH value is 4.5, be warmed up to 41 DEG C, add phoxim, adjustment concentration is 0.07%, by the flax fabric dipping after above-mentioned kiering in the solution, be warmed up to 73 DEG C again, process 27min, then cool to 44 DEG C, insulation 12min, is then immersed in the flax fabric of above-mentioned process in the clear water of 39 DEG C and cleans 7 times;
Step 3: flax fabric good for above-mentioned washing is processed 30min in the solution containing niter cake and glacial acetic acid, wherein niter cake concentration is 1.8%, glacial acetic acid concentration is 1.5%, treatment temperature is 43 DEG C, processing time is 14min; bath raio is 1:30, is then immersed in by the flax fabric of above-mentioned process in the clear water of 42 DEG C and cleans 7 times;
Step 4: it is process 57min in the softener solution of 3% that the flax fabric after washing in step 3 is immersed in concentration, and wherein treatment temperature is 37 DEG C, and bath raio is 1:45, then dry oven dry 26min under temperature is 135 DEG C of conditions.
Above embodiment is only and technological thought of the present invention is described, can not limit protection scope of the present invention with this, and every technological thought proposed according to the present invention, any change that technical scheme basis is done, all falls within scope.
Claims (4)
1. a flax fabric antiseptic and inhibiting bacteria function treatment process, is characterized in that, comprises following concrete steps:
Step one: the graticule material selected is according to the mass fraction: linen fibre: 68-82 part, silkworm protein fiber 8-12 part, soft silk fiber 5-7 part, all the other are cotton fiber, are placed on by described flax fabric and boil in yarn pot, normal pressure kiering, kiering 8-10h, boil rear vexed 2-3h, then the flax fabric after kiering is first washed with hot water and circulating chilled water in pot, after taking the dish out of the pot, use cold flow water fully clean again;
Step 2: preparation temperature is in the weak acid solution of 35-38 DEG C, pH value is 4-5, be warmed up to 40-42 DEG C, add phoxim, adjustment concentration is 0.06-0.08%, by the flax fabric dipping after above-mentioned kiering in the solution, be warmed up to 72-74 DEG C again, process 26-28min, then cool to 43-45 DEG C, insulation 10-14min, is then immersed in the flax fabric of above-mentioned process in the clear water of 38-40 DEG C and cleans 6-8 time;
Step 3: flax fabric good for above-mentioned washing is processed 25-35min in the solution containing niter cake and glacial acetic acid, wherein niter cake concentration is 1.8%, glacial acetic acid concentration is 1.5%, treatment temperature is 42-44 DEG C, processing time is 13-15min; bath raio is 1:30, is then immersed in by the flax fabric of above-mentioned process in the clear water of 41-43 DEG C and cleans 6-8 time;
Step 4: it is process 55-59min in the softener solution of 3% that the flax fabric after washing in step 3 is immersed in concentration, and wherein treatment temperature is 36-38 DEG C, and bath raio is 1:45, then dry oven dry 24-28min under temperature is 130-140 DEG C of condition.
2. flax fabric antiseptic and inhibiting bacteria function treatment process according to claim 1, is characterized in that, comprise following concrete steps:
Step one: the graticule material selected is according to the mass fraction: linen fibre: 68 parts, silkworm protein fiber 8 parts, soft silk fiber 5 parts, all the other are cotton fiber, are placed on by described flax fabric and boil in yarn pot, normal pressure kiering, kiering 8h, boil rear vexed 2h, then the flax fabric after kiering is first washed with hot water and circulating chilled water in pot, after taking the dish out of the pot, use cold flow water fully clean again;
Step 2: preparation temperature is in the weak acid solution of 35 DEG C, pH value is 4, be warmed up to 40 DEG C, add phoxim, adjustment concentration is 0.06%, by the flax fabric dipping after above-mentioned kiering in the solution, be warmed up to 72 DEG C again, process 28min, then cool to 43 DEG C, insulation 14min, is then immersed in the flax fabric of above-mentioned process in the clear water of 38 DEG C and cleans 8 times;
Step 3: flax fabric good for above-mentioned washing is processed 25min in the solution containing niter cake and glacial acetic acid, wherein niter cake concentration is 1.8%, glacial acetic acid concentration is 1.5%, treatment temperature is 42 DEG C, processing time is 15min; bath raio is 1:30, is then immersed in by the flax fabric of above-mentioned process in the clear water of 41 DEG C and cleans 8 times;
Step 4: it is process 55min in the softener solution of 3% that the flax fabric after washing in step 3 is immersed in concentration, and wherein treatment temperature is 36 DEG C, and bath raio is 1:45, then dry oven dry 28min under temperature is 130 DEG C of conditions.
3. flax fabric antiseptic and inhibiting bacteria function treatment process according to claim 1, is characterized in that, comprise following concrete steps:
Step one: the graticule material selected is according to the mass fraction: linen fibre: 82 parts, silkworm protein fiber 12 parts, soft silk fiber 7 parts, all the other are cotton fiber, are placed on by described flax fabric and boil in yarn pot, normal pressure kiering, kiering 10h, boil rear vexed 3h, then the flax fabric after kiering is first washed with hot water and circulating chilled water in pot, after taking the dish out of the pot, use cold flow water fully clean again;
Step 2: preparation temperature is in the weak acid solution of 38 DEG C, pH value is 5, be warmed up to 42 DEG C, add phoxim, adjustment concentration is 0.08%, by the flax fabric dipping after above-mentioned kiering in the solution, be warmed up to 74 DEG C again, process 26min, then cool to 45 DEG C, insulation 10min, is then immersed in the flax fabric of above-mentioned process in the clear water of 40 DEG C and cleans 6 times;
Step 3: flax fabric good for above-mentioned washing is processed 35min in the solution containing niter cake and glacial acetic acid, wherein niter cake concentration is 1.8%, glacial acetic acid concentration is 1.5%, treatment temperature is 44 DEG C, processing time is 13min; bath raio is 1:30, is then immersed in by the flax fabric of above-mentioned process in the clear water of 43 DEG C and cleans 6 times;
Step 4: it is process 59min in the softener solution of 3% that the flax fabric after washing in step 3 is immersed in concentration, and wherein treatment temperature is 38 DEG C, and bath raio is 1:45, then dry oven dry 24min under temperature is 140 DEG C of conditions.
4. flax fabric antiseptic and inhibiting bacteria function treatment process according to claim 1, is characterized in that, comprise following concrete steps:
Step one: the graticule material selected is according to the mass fraction: linen fibre: 75 parts, silkworm protein fiber 10 parts, soft silk fiber 6 parts, all the other are cotton fiber, are placed on by described flax fabric and boil in yarn pot, normal pressure kiering, kiering 9h, boil rear vexed 2.5h, then the flax fabric after kiering is first washed with hot water and circulating chilled water in pot, after taking the dish out of the pot, use cold flow water fully clean again;
Step 2: preparation temperature is in the weak acid solution of 36 DEG C, pH value is 4.5, be warmed up to 41 DEG C, add phoxim, adjustment concentration is 0.07%, by the flax fabric dipping after above-mentioned kiering in the solution, be warmed up to 73 DEG C again, process 27min, then cool to 44 DEG C, insulation 12min, is then immersed in the flax fabric of above-mentioned process in the clear water of 39 DEG C and cleans 7 times;
Step 3: flax fabric good for above-mentioned washing is processed 30min in the solution containing niter cake and glacial acetic acid, wherein niter cake concentration is 1.8%, glacial acetic acid concentration is 1.5%, treatment temperature is 43 DEG C, processing time is 14min; bath raio is 1:30, is then immersed in by the flax fabric of above-mentioned process in the clear water of 42 DEG C and cleans 7 times;
Step 4: it is process 57min in the softener solution of 3% that the flax fabric after washing in step 3 is immersed in concentration, and wherein treatment temperature is 37 DEG C, and bath raio is 1:45, then dry oven dry 26min under temperature is 135 DEG C of conditions.
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| CN201510126874.6A CN104695114B (en) | 2015-03-23 | 2015-03-23 | A kind of flax fabric antiseptic and inhibiting bacteria function treatment process |
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| CN201510126874.6A CN104695114B (en) | 2015-03-23 | 2015-03-23 | A kind of flax fabric antiseptic and inhibiting bacteria function treatment process |
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| CN107100005A (en) * | 2016-02-22 | 2017-08-29 | 阜阳奥宏纤维制品有限公司 | A kind of silk flosssilk wadding fabric antiseptic and inhibiting bacteria function handling process |
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